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Cas:3490-06-0
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Min.Order:1 Gram
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Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiry1-(3,4-dimethoxy-phenyl)-2-methylamino-ethanone; hydrochloride
A
N-methylhomoveratrylamine
B
1-(3,4-dimethoxyphenyl)-2-(methylamino)ethan-1-ol
Conditions | Yield |
---|---|
Stage #1: 1-(3,4-dimethoxy-phenyl)-2-methylamino-ethanone; hydrochloride With hydrogen; 5%-palladium/activated carbon In water at 75℃; under 2585.81 Torr; for 16 - 40h; Stage #2: With sodium hydroxide In water; toluene pH=12; Product distribution / selectivity; | A n/a B 95.1% |
N-[2-(3,4-dimethoxyphenyl)ethyl]formamide
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With sodium tetrahydroborate; boron trifluoride diethyl etherate In tetrahydrofuran 1) room temperature, 1 h; 2) reflux, 3 h; | 90% |
With tetrahydrofuran; lithium aluminium tetrahydride | |
With lithium aluminium tetrahydride In tetrahydrofuran; diethyl ether |
methanesulphonic acid,2-(3,4-dimethoxyphenyl)ethyl ester
methylamine
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
Stage #1: methanesulphonic acid,2-(3,4-dimethoxyphenyl)ethyl ester; methylamine In methanol; water at 140℃; under 15514.9 Torr; for 0.166667h; Flow reactor; Stage #2: With potassium hydroxide In water | 90% |
N-[2-(3,4-dimethoxyphenyl)ethyl]-2,2,2-trifluoroacetamide
methyl iodide
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran for 4h; Ambient temperature; | 82% |
3,4-dimethoxystyrene
N-methylhydroxylamine-O-sulphonic acid
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
Stage #1: 3,4-dimethoxystyrene With Schwartz's reagent In tetrahydrofuran at 25℃; Stage #2: N-methylhydroxylamine-O-sulphonic acid In tetrahydrofuran at 50℃; for 0.5h; | 71% |
2-(3,4-dimethoxyphenyl)-ethylchloride
methylamine
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
Stage #1: 2-(3,4-dimethoxyphenyl)-ethylchloride; methylamine In ethanol at 20℃; for 1h; Stage #2: With triisobutylaluminum In ethanol at 60℃; for 32h; | 68% |
(3,4-dimethoxy-phenyl)-thioacetic acid methylamide
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With hydrogenchloride an Blei-Elektroden; |
benzaldehyde
2-(3,4-dimethoxyphenyl)-ethylamine
dimethyl sulfate
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With benzene und Erwaermen des Reaktionsprodukts mit wss.Aethanol; |
benzaldehyde
2-(3,4-dimethoxyphenyl)-ethylamine
methyl iodide
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
und Erwaermen des Reaktionsprodukts mit wss.Aethanol; |
Conditions | Yield |
---|---|
With palladium; benzene Hydrogenation; |
N-[2-(3,4-dimethoxyphenyl)ethyl]-2,2,2-trifluoroacetamide
N-methylhomoveratrylamine
N-tert-Butyl-N'-[2-(3,4-dimethoxy-phenyl)-ethyl]-N'-methyl-methanediamine
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With hydrogenchloride In tetrahydrofuran for 2h; Ambient temperature; Yield given; |
A
N-methylhomoveratrylamine
B
(1R,5S,7R)-1,5,7-Trimethyl-2,4-dioxo-3-oxa-bicyclo[3.3.1]nonane-7-carboxylic acid methyl ester
Conditions | Yield |
---|---|
With water In acetonitrile at 22℃; Rate constant; buffer (pH 1.0-8.5); |
2-(3,4-dimethoxyphenyl)-ethylamine
methyl iodide
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With sodium hydroxide; benzaldehyde Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
Hydrogenation; |
N'-tert-Butyl-N-[(E)-2-(3,4-dimethoxy-phenyl)-vinyl]-N-methyl-formamidine
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium borohydride, 10percent HCl / aq. ethanol / 1 h / 0 °C / pH ca.6 2: 10percent HCl / tetrahydrofuran / 2 h / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 99 percent / CH2Cl2 / 1 h / 0 °C 2: 82 percent / NaH / tetrahydrofuran / 4 h / Ambient temperature View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: LiAlH4; diethyl ether 2: chloral 3: LiAlH4; THF View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: chloral 2: LiAlH4; THF View Scheme | |
With LiAlH4; triethylamine In tetrahydrofuran; dichloromethane | |
Multi-step reaction with 2 steps 1: dichloromethane / 1 h / 20 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / 0 °C / Inert atmosphere; Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: -15 °C / anschliessendes Erhitzen mit Schwefel bis auf 150grad 2: aq.-ethanolic hydrochloric acid / an Blei-Elektroden View Scheme |
1-(4-nitrophenoxy)-2-[N-(3,4-dimethoxyphenethyl)-N-methylamino]ethane
A
N-methylhomoveratrylamine
B
1-(2-bromoethoxy)-4-nitrobenzene
Conditions | Yield |
---|---|
In benzyl-methyl-amine |
N-methyl-N-(2-(3',4'-dimethoxyphenyl)ethyl)trifluoroacetamide
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; dichloromethane |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: acetic acid; ammonium acetate / 20 - 120 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux 3: dichloromethane / 1 h / 20 °C 4: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / 0 °C / Inert atmosphere; Reflux View Scheme |
3,4-dimethoxynitrostyrene
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux 2: dichloromethane / 1 h / 20 °C 3: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / 0 °C / Inert atmosphere; Reflux View Scheme |
tert-butyl N-[2-(3,4-dimethoxyphenyl)ethyl]carbamate
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 6h; Inert atmosphere; Reflux; | 3.65 g |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: phosphorus pentachloride; calcium carbonate / toluene / 4.17 h / 0 - 20 °C / Inert atmosphere 2.1: ethanol / 1 h / 20 °C 2.2: 32 h / 60 °C View Scheme | |
Multi-step reaction with 2 steps 1: triethylamine / dichloromethane / 1.58 h / Inert atmosphere 2: methanol; water / 0.17 h / 140 °C / 15514.9 Torr / Flow reactor View Scheme |
methylamine
2-(3,4-dimethoxyphenyl)ethyl alcohol
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
Stage #1: 2-(3,4-dimethoxyphenyl)ethyl alcohol With thionyl chloride In N,N-dimethyl-formamide; toluene at 35 - 40℃; for 1h; Inert atmosphere; Stage #2: methylamine In water; N,N-dimethyl-formamide; toluene at 0 - 25℃; for 1h; Concentration; Temperature; |
N-methylhomoveratrylamine
2,3-Dimethoxy-7-methyl-bicyclo[4.2.0]octa-1(6),2,4-triene-7-carbonyl chloride
N-3,4-dimethoxyphenethyl-N-methyl-1-(3,4-dimethoxy-1-methylbenzocyclobutenyl)carboxamide
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In diethyl ether; water for 2h; 0 deg C -> r.t.; | 100% |
N-methylhomoveratrylamine
2-iodo-5-methoxybenzenepropanoyl chloride
N-<2-(3,4-dimethoxyphenyl)ethyl>-2-iodo-5-methoxy-N-methylbenzenepropanamide
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 3h; Ambient temperature; | 100% |
With hydrogenchloride; sodium hydroxide In dichloromethane; water; toluene | |
With hydrogenchloride; sodium hydroxide In dichloromethane; water; toluene | |
With hydrogenchloride; sodium hydroxide In dichloromethane; water; toluene |
N-methylhomoveratrylamine
(S)-verapamil
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
Stage #1: N-methylhomoveratrylamine; C16H21NO4*C8H11N With m-nitrobenzene boronic acid In 5,5-dimethyl-1,3-cyclohexadiene at 40℃; for 24h; Reflux; Stage #2: With hydrogenchloride; sodium hydrogencarbonate In water | 98.8% |
Conditions | Yield |
---|---|
With sodium hydroxide In chloroform; water | 98% |
N-methylhomoveratrylamine
4-hydroxyphenylpropionic acid
N-[2-(3,4-dimethoxyphenyl)ethyl]-3-(4-hydroxyphenyl)-N-methylpropanamide
Conditions | Yield |
---|---|
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In DMF (N,N-dimethyl-formamide) at 0 - 20℃; | 97% |
N-methylhomoveratrylamine
1-(azidosulfonyl)-2,3-dimethyl-1H-imidazol-3-ium trifluoromethanesulfonate
C11H16N4O4S
Conditions | Yield |
---|---|
In acetonitrile at 0℃; | 96% |
N-[4-(2,3-epoxypropoxy)phenyl]-5,6-dimethoxy-1-oxo-isoindoline
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
In ethanol Heating; | 95.42% |
N-methylhomoveratrylamine
hexamethylenetetramine
2-methyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
Conditions | Yield |
---|---|
In acetic acid; trifluoroacetic acid for 0.5h; Pictet-Spengler reaction; Heating; | 94% |
3-Chloropropionitrile
N-methylhomoveratrylamine
3-[[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino]propanenitrile
Conditions | Yield |
---|---|
With sodium carbonate; sodium iodide In tert-butyl alcohol for 24h; Heating; | 94% |
N-methylhomoveratrylamine
4-chloro-3-nitro-5-sulfamoylbenzoic acid
4-{[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino}-3-nitro-5-sulfamoylbenzoic acid
Conditions | Yield |
---|---|
Stage #1: N-methylhomoveratrylamine; 4-chloro-3-nitro-5-sulfamoylbenzoic acid In water for 11h; Reflux; Stage #2: With hydrogenchloride In water pH=Ca. 2; | 94% |
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With formic acid In toluene for 1h; Heating; | 93% |
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; | 93% |
N-methylhomoveratrylamine
(2R)-(+)-5-chloro-2-(3,4-dimethoxyphenyl)-2-isopropylpentanenitrile
dexverapamil
Conditions | Yield |
---|---|
at 130℃; for 1h; | 92% |
at 130℃; for 4h; |
N-methylhomoveratrylamine
(2S)-(-)-5-chloro-2-(3,4-dimethoxyphenyl)-2-isopropylpentanenitrile
(S)-verapamil
Conditions | Yield |
---|---|
at 130℃; for 1h; | 91% |
at 130℃; for 4h; |
N-methylhomoveratrylamine
1-(6,9-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-on-3-yl)-3-chloro-propane
1-[6,9-dimethoxy-1,3-dihydro-2H-3-benzazepin-2-on-3-yl]-3-[N-methyl-N-(2-{3,4-dimethoxy-phenyl}-ethyl)-amino]-propane
Conditions | Yield |
---|---|
90% |
N-methylhomoveratrylamine
δ-chlorovaleronitrile
5-[[2-(3,4-dimethoxyphenyl)ethyl](methyl)amino]pentanenitrile
Conditions | Yield |
---|---|
With sodium carbonate; sodium iodide In tert-butyl alcohol for 24h; Heating; | 89% |
With acetone; sodium iodide at 100℃; |
N-methylhomoveratrylamine
4-bromo-2-(dibromomethyl)-1-fluorobenzene
1-(5-bromo-2-fluorophenyl)-6,7-dimethoxy-2-methyl-1,2,3,4-tetrahydroisoquinoline
Conditions | Yield |
---|---|
With trifluoroacetic acid at 80℃; for 5h; Pictet-Spengler reaction; Inert atmosphere; neat (no solvent); | 89% |
N-methylhomoveratrylamine
formaldehyd
2-methyl-6,7-dimethoxy-1,2,3,4-tetrahydroisoquinoline
Conditions | Yield |
---|---|
With formic acid In water at 100℃; for 4h; | 88% |
With water und Erwaermen des Reaktionsprodukts mit konz. Salzsaeure; |
N-methylhomoveratrylamine
(+/-)-4-bromo-7,8-dimethoxyisochroman-3-one
4-(N-methyl-β-3',4'-dimethoxyphenylethylamino)-7,8-dimethoxyisochroman-3-one
Conditions | Yield |
---|---|
In benzene for 2h; Ambient temperature; | 88% |
N-methylhomoveratrylamine
1-[2-(3,4-dimethoxyphenyl)ethyl]-1,3-dimethylurea
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 18h; Inert atmosphere; | 88% |
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
In acetonitrile for 20h; Addition; Heating; | 87.7% |
N-methylhomoveratrylamine
N-[4-(3-chloropropoxy)phenyl]-5,6-dimethoxy-1-oxo-isoindoline
Conditions | Yield |
---|---|
at 80℃; for 6h; | 87.57% |
N-methylhomoveratrylamine
2,3-Dihydro-2-thioxo-1H-thieno[2,3-b][1,4]thiazin-6-carbonsaeuremethylester
Conditions | Yield |
---|---|
In tetrahydrofuran for 5h; Heating; | 87% |
N-methylhomoveratrylamine
methyl vinyl ketone
4-((N-(2-(3,4-dimethoxyphenyl)ethyl)-N-methyl)amino)-2-butanol
Conditions | Yield |
---|---|
With sodium borohydrid In methanol | 87% |
N-methylhomoveratrylamine
2-(4-benzyl-3,4-dihydro-2H-1,4-benzoxazin-2-yl)acetic acid
2-(4-Benzyl-3,4-dihydro-2H-benzo[1,4]oxazin-2-yl)-N-[2-(3,4-dimethoxy-phenyl)-ethyl]-N-methyl-acetamide
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane for 5h; Ambient temperature; | 86% |
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With triethylamine In ethanol for 48h; Substitution; Heating; | 86% |
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