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CHANGZHOU HANGYU PHARMACEUTICAL TECHNOLOGY CO., LTD

Good supplier high quality 3,4-Dimethoxy phenyl acetonitrile 93-17-4 manufacturer Product Details Overview Quick Details Pro Name;3,4-Dimethoxy phenyl acetonitrile CAS NO:93-17-4 Purity:99% Application: API Appea

good supplier high quality 3,4-Dimethoxy phenyl acetonitrile 93-17-4 manufacturer

Cas:93-17-4

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MS( MAOSHENG )Chemical CO.,LTD

Certificate of Analysis 产品 PRODUCT 3,4-二甲氧基苯乙腈3,4-Dimethoxybenzeneacetonitrile CAS No. 93-17-4 结构式 Formula

3, 4 - dimethoxy phenylacetonitrile

Cas:93-17-4

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

(3,4-Dimethoxyphenyl)acetonitrile Manufacturer/High quality/Best price/In stock

Cas:93-17-4

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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Assay 98%min ---------------------------------------------------------------------------------------------

High purity Various Specifications 3,4-Dimethoxy phenyl acetonitrile CAS:93-17-4

Cas:93-17-4

Min.Order:1 Gram

FOB Price: $100.0 / 500.0

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 3,4-Dimethoxy Phenyl Acetonitrile supplier in China

Cas:93-17-4

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Hubei Vanz Pharm Co.,Ltd

1. high purity; 2. able to provide COA/HNMR/HPLC; 3. High quality; 4. low price; 5. Best service; 6.direct supplier Appearance:yellow crtstalline powder Storage:rm Package:bag/bottle/drum Application:intermediate for cefuroxime Transp

(3,4-Dimethoxyphenyl)acetonitrile

Cas:93-17-4

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Wuhan Fortuna Chemical Co.,Ltd

Unique advantages for (3,4-Dimethoxyphenyl)acetonitrile Cas 93-17-4 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White to light yellow powder Storage:N/A Package:25kg/dru

High quality (3,4-Dimethoxyphenyl)acetonitrile Cas 93-17-4 with best price

Cas:93-17-4

Min.Order:25 Kilogram

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Hangzhou Think Chemical Co. Ltd

Homoveratryl Amine[CAS:120-20-7] 2-(3,4-Dimethoxyphenyl) Ethylamine Homoveratryl Acid[CAS:93-40-3] (3,4-Dimethoxyphenyl) Acetic Acid HANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and con

Supply Homoveratronitrile

Cas:93-17-4

Min.Order:1 Kilogram

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Type:Other

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 3,4-dimethoxyphenylacetonitrile

Cas:93-17-4

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

Veratryl cyanide

Cas:93-17-4

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

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Hebei yanxi chemical co.,LTD.

1 Factory price 2 High quality 3 Good service 4 Prompt service (3,4-Dimethoxyphenyl)acetonitrile (3,4-Dimethoxyphenyl)acetonitrile supplier 93-17-4 Quick Details ProName: (3,4-Dimethoxyphenyl)acetonitrile

(3,4-Dimethoxyphenyl)acetonitrile

Cas:93-17-4

Min.Order:500 Kilogram

FOB Price: $1600.0 / 1800.0

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Henan Tianfu Chemical Co., Ltd.

(3,4-Dimethoxyphenyl)acetonitrile Basic information Product Name: (3,4-Dimethoxyphenyl)acetonitrile Synonyms: TIMTEC-BB SBB005899;3,4-dimethoxy-benzeneacetonitril;3,4-dimethoxybenzeneace

TIANFU-CHEM CAS:93-17-4 (3,4-Dimethoxyphenyl)acetonitrile

Cas:93-17-4

Min.Order:1 Gram

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

3,4-Dimethoxy phenyl acetonitrile

Cas:93-17-4

Min.Order:1 Kilogram

FOB Price: $100.0 / 150.0

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 93-17-4 with best quality

Cas:93-17-4

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

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LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

(3,4-Dimethoxyphenyl)acetonitrile/ LIDE PHARMA- Factory supply / Best price

Cas:93-17-4

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Henan Sinotech Import&Export Corporation

Product name (3 4-Dimethoxyphenyl)acetonitrile Synonyms Homoveratronitrite;3,4-Dimethoxylphenylacetonitrile;(3,4-Dimethoxyphenyl)acetonitrile, 3,4-Dimethoxybenzylcyanide, Homoveratronitrile;(3,4-

(3,4-Dimethoxyphenyl)acetonitrile CAS: 93-17-4

Cas:93-17-4

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Hangzhou Sartort Biopharma Co., Ltd

Appearance:white to almost white crystals or cryst. needles Storage:Room temperature Package:25kg/drum Application:intermediate Transportation:Express/Sea/Air Port:Any port in china

High Quality 3,4-Dimethoxy phenyl acetonitrile (Verapamil intermediate)

Cas:93-17-4

Min.Order:25 Kilogram

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

(3,4-Dimethoxyphenyl)acetonitrile 93-17-4

Cas:93-17-4

Min.Order:1 Kilogram

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Shanghai Minstar Chemical Co., Ltd

(3,4-Dimethoxyphenyl)acetonitrile Chemical Properties Melting point 54-57 °C(lit.) Boiling point 171-178 °C10 mm Hg(lit.) density 1.1607 (rough estimate) refractive index 1.5168 (estimate) Fp >230 °F storage temp.

(3,4-Dimethoxyphenyl)acetonitrile.

Cas:93-17-4

Min.Order:1 Gram

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present,

(3,4-Dimethoxyphenyl)acetonitrile

Cas:93-17-4

Min.Order:1 Kilogram

FOB Price: $50.0

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Qingdao Beluga Import and Export Co., LTD

(3,4-Dimethoxyphenyl)acetonitrile CAS:93-17-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality or

(3,4-Dimethoxyphenyl)acetonitrile CAS:93-17-4

Cas:93-17-4

Min.Order:1 Gram

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

(3,4-Dimethoxyphenyl)acetonitrile

Cas:93-17-4

Min.Order:1 Kilogram

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:93-17-4

Cas:93-17-4

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

(3,4-Dimethoxyphenyl)Acetonitrile

Cas:93-17-4

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Hebei Miheng Trading Co., Ltd.

(3,4-Dimethoxyphenyl)acetonitrile CAS 93-17-4 Our advantage 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purch

(3,4-Dimethoxyphenyl)acetonitrile CAS 93-17-4

Cas:93-17-4

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Triumph International Development Limilted

Appearance:white or yellowish white flaky crystal Storage:Keep the sun from direct sunlight ;prevention against high temperature Package:As customer request Application:Used for research and industrial manufacture. Transportatio

3,4-Dimethoxy phenyl acetonitrile

Cas:93-17-4

Min.Order:0 Metric Ton

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

93-17-4 3,4-Dimethoxyphenyl)acetonitrile

Cas:93-17-4

Min.Order:10 Kilogram

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Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

CAS 93-17-4 (3,4-Dimethoxyphenyl)acetonitrile

Cas:93-17-4

Min.Order:1 Kilogram

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

(3,4-Dimethoxyphenyl)acetonitrile

Cas:93-17-4

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Hefei Zhaobo Technology Co., Ltd.

(3,4-Dimethoxyphenyl)acetonitrile CAS 93-17-4 Description Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establish

(3,4-Dimethoxyphenyl)acetonitrile CAS 93-17-4

Cas:93-17-4

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Synthetic route

2-(3,4-dimethoxyphenyl)acetamide
5663-56-9

2-(3,4-dimethoxyphenyl)acetamide

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With ethyl phosphodichloridite; 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 20℃; for 2h;92%
4-chloromethyl-1,2-dimethoxy-benzene
7306-46-9

4-chloromethyl-1,2-dimethoxy-benzene

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With sodium cyanide91%
α-(3,4-dimethoxyphenyl)-α-(methylthio)acetonitrile
84784-38-3

α-(3,4-dimethoxyphenyl)-α-(methylthio)acetonitrile

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With acetic acid; zinc at 100℃; for 1h;90%
2-(3,4-dimethoxyphenyl)acetaldehyde oxime
77733-60-9

2-(3,4-dimethoxyphenyl)acetaldehyde oxime

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With trimethylsilyl iodide; 1,1,1,3,3,3-hexamethyl-disilazane In chloroform at 56℃; for 4h;86%
With trimethylsilyl iodide; 1,1,1,3,3,3-hexamethyl-disilazane In chloroform at 56℃; for 4h; Product distribution; other temperature, without hexamethyldisilazane (TMS2NH);86%
With acetic anhydride
With trimethylsilyl iodide In chloroform for 2h; Ambient temperature;40 mg
4-isoxazoleboronic acid pinacol ester
928664-98-6

4-isoxazoleboronic acid pinacol ester

4-Bromoveratrole
2859-78-1

4-Bromoveratrole

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; water In dimethyl sulfoxide at 130℃; for 16h; Domino Suzuki coupling and fragmentation reaction; Inert atmosphere;84%
3,4-Dimethoxyphenylthioacetamid
145736-65-8

3,4-Dimethoxyphenylthioacetamid

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With 1-oxa-2-azaspiro[2.5]octane In toluene at 20 - 25℃; for 4h;82%
4-Bromoveratrole
2859-78-1

4-Bromoveratrole

acetonitrile
75-05-8

acetonitrile

A

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

B

bis(3,4-dimethoxyphenyl)acetonitrile
7250-04-6

bis(3,4-dimethoxyphenyl)acetonitrile

Conditions
ConditionsYield
With ethoxyethoxyethanol; sodium amide In 1,2-dimethoxyethane 1.) 45 deg C, 2 h, 2.) -10 deg C, 2 h, 3.) -45 deg C, 4.5 h;A 78%
B 8%
sodium cyanide
143-33-9

sodium cyanide

1-(3,4-Dimethoxy-benzyl)-2-methylsulfanyl-4,6-diphenyl-pyridinium; iodide
76950-82-8

1-(3,4-Dimethoxy-benzyl)-2-methylsulfanyl-4,6-diphenyl-pyridinium; iodide

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
In 1,2-dimethoxyethane for 24h; Heating;76%
potassium cyanide
151-50-8

potassium cyanide

4-chloromethyl-1,2-dimethoxy-benzene
7306-46-9

4-chloromethyl-1,2-dimethoxy-benzene

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
In dimethyl sulfoxide for 20h;67%
With benzene
With hydrogenchloride
2-(3,4-dimethoxyphenyl)-ethylamine
120-20-7

2-(3,4-dimethoxyphenyl)-ethylamine

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With iodine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide at 65℃; for 3h;64%
2-bromo-4,5-dimethoxyphenylacetonitrile
51655-39-1

2-bromo-4,5-dimethoxyphenylacetonitrile

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
Stage #1: 2-bromo-4,5-dimethoxyphenylacetonitrile With nickel(II) iodide; 1,4-bis(dicyclohexylphosphino)butane; sodium carbonate; cesium iodide In tetrahydrofuran for 0.25h; Schlenk technique; Glovebox;
Stage #2: In tetrahydrofuran at 35℃; for 72h; Irradiation;
54%
(3,4-Dimethoxyphenyl)acetic acid
93-40-3

(3,4-Dimethoxyphenyl)acetic acid

4-(methylsulfonyl)benzonitrile
22821-76-7

4-(methylsulfonyl)benzonitrile

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With riboflavin-2',3',4',5'-tetra-acetate In acetonitrile at 25℃; for 12h; Inert atmosphere; Irradiation; Sealed tube;45%
3,4-dimethoxyphenylpyruvic acid
2460-33-5

3,4-dimethoxyphenylpyruvic acid

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With acetic anhydride
2-(3,4-dimethoxyphenyl)acetaldehyde oxime
77733-60-9

2-(3,4-dimethoxyphenyl)acetaldehyde oxime

acetic anhydride
108-24-7

acetic anhydride

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

3,4-dimethoxy-α-ethoxycarbonyloxybenzyl cyanide
6443-67-0

3,4-dimethoxy-α-ethoxycarbonyloxybenzyl cyanide

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With p-menth-1-ene; palladium on activated charcoal
sodium cyanide
143-33-9

sodium cyanide

(3,4-dimethoxyphenyl)methanol
93-03-8

(3,4-dimethoxyphenyl)methanol

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
(i) aq. HCl, CH2Cl2, (ii) /BRN= 3587243/, KI, acetone; Multistep reaction;
(i) aq. HCl, (ii) /BRN= 3587243/, DMSO; Multistep reaction;
4-bromomethyl-1,2-dimethoxybenzene
21852-32-4

4-bromomethyl-1,2-dimethoxybenzene

sodium cyanide
143-33-9

sodium cyanide

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
In ethanol; water for 5h; Heating;
ethyl 2-cyano-2-(3,4-dimethoxyphenyl)acetate
36848-69-8

ethyl 2-cyano-2-(3,4-dimethoxyphenyl)acetate

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With sodium hydroxide In water at 80 - 90℃; for 2h; Yield given;
Phosphoric acid cyano-(3,4-dimethoxy-phenyl)-methyl ester diethyl ester
96824-26-9

Phosphoric acid cyano-(3,4-dimethoxy-phenyl)-methyl ester diethyl ester

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In ethyl acetate for 2h; Ambient temperature; Yield given;
3-hydroxy-4-methoxyphenylacetonitrile
4468-58-0

3-hydroxy-4-methoxyphenylacetonitrile

dimethyl sulfate
77-78-1

dimethyl sulfate

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With sodium hydroxide at 0℃; for 1h;
sodium cyanide
143-33-9

sodium cyanide

4-chloromethyl-1,2-dimethoxy-benzene
7306-46-9

4-chloromethyl-1,2-dimethoxy-benzene

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
In 1,4-dioxane; water
In water; benzene for 6h; Heating; Yield given;
sodium cyanide
143-33-9

sodium cyanide

4-chloromethyl-1,2-dimethoxy-benzene
7306-46-9

4-chloromethyl-1,2-dimethoxy-benzene

A

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

B

(Z)-1,2-dicyano-1,2-bis(3,4-dimethoxyphenyl)ethene
18656-85-4

(Z)-1,2-dicyano-1,2-bis(3,4-dimethoxyphenyl)ethene

Conditions
ConditionsYield
In tetrachloromethane; water Heating;
(+-)-benzoyloxy-<3.4-dimethoxy-phenyl>-acetonitrile

(+-)-benzoyloxy-<3.4-dimethoxy-phenyl>-acetonitrile

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With p-menth-1-ene; palladium
With tetralin; palladium
3.4-dimethoxy-phenylpyruvic acid-oxime

3.4-dimethoxy-phenylpyruvic acid-oxime

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
at 155℃;
ethoxycarbonyloxy-<3,4-dimethoxy-phenyl>-acetonitrile

ethoxycarbonyloxy-<3,4-dimethoxy-phenyl>-acetonitrile

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With palladium; benzene Hydrogenation;
oxime of homoveratraldehyde

oxime of homoveratraldehyde

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With acetic anhydride
tetralin
119-64-2

tetralin

2-benzoyloxy-2-(3',4'-dimethoxyphenyl)-acetonitrile
102327-45-7

2-benzoyloxy-2-(3',4'-dimethoxyphenyl)-acetonitrile

palladium

palladium

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

2-benzoyloxy-2-(3',4'-dimethoxyphenyl)-acetonitrile
102327-45-7

2-benzoyloxy-2-(3',4'-dimethoxyphenyl)-acetonitrile

(R)-p-menthene-(1)

(R)-p-menthene-(1)

palladium

palladium

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

4-bromomethyl-1,2-dimethoxybenzene
21852-32-4

4-bromomethyl-1,2-dimethoxybenzene

potassium cyanide
151-50-8

potassium cyanide

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
In ethanol; water for 4h; Substitution; Heating;
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

2-(3,4-dimethoxyphenyl)-ethylamine
120-20-7

2-(3,4-dimethoxyphenyl)-ethylamine

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal In acetic acid for 4h;100%
Stage #1: 3,4-dimethoxyphenylacetonitrile With diborane In tetrahydrofuran at 55℃; for 16h; Inert atmosphere;
Stage #2: With hydrogenchloride; water In tetrahydrofuran at 0 - 20℃;
Stage #3: With sodium hydroxide In tetrahydrofuran; water
99%
With hydrogen; nickel In ethanol at 40℃; electrocatalytic hydrogenation;98%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

homoveratrylamine hydrochloride
635-85-8

homoveratrylamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride; hydrogen In propan-1-ol; water at 60℃; under 375.038 Torr; for 18h; Flow reactor;100%
Stage #1: 3,4-dimethoxyphenylacetonitrile With borane-ammonia complex; C17H16BrMnN2O3S In hexane at 60℃; for 12h;
Stage #2: With hydrogenchloride In diethyl ether; water
90%
1-η**(5)-ferrocenyl-3,3-bis(methylthio)prop-2-en-1-one
916322-38-8

1-η**(5)-ferrocenyl-3,3-bis(methylthio)prop-2-en-1-one

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

C24H23FeNO3S

C24H23FeNO3S

Conditions
ConditionsYield
Stage #1: 3,4-dimethoxyphenylacetonitrile With sodium hydride In N,N-dimethyl-formamide; mineral oil; benzene at 0℃; for 0.25h;
Stage #2: 3,3-bis(methylsulfanyl)-1-η5-ferrocenyl-2-propen-1-one In N,N-dimethyl-formamide; mineral oil; benzene at 0 - 20℃;
100%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

4-methoxy-benzaldehyde
123-11-5

4-methoxy-benzaldehyde

(Z)-2-(3,4-dimethoxyphenyl)-3-(4-methoxyphenyl)acrylonitrile
37629-77-9

(Z)-2-(3,4-dimethoxyphenyl)-3-(4-methoxyphenyl)acrylonitrile

Conditions
ConditionsYield
With sodium ethanolate In ethanol Reflux; Inert atmosphere;99%
With sodium methylate In ethanol at 20℃; for 3h;92%
With sodium ethanolate In ethanol at 85℃; for 1h; Knoevenagel Condensation; Inert atmosphere;90%
ethanol
64-17-5

ethanol

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

ethyl 2-(3,4-dimethoxyphenyl)acetoimidate hydrochloride
81316-62-3

ethyl 2-(3,4-dimethoxyphenyl)acetoimidate hydrochloride

Conditions
ConditionsYield
With hydrogenchloride at 0 - 5℃; Addition;99%
With hydrogenchloride88%
With hydrogenchloride In chloroform for 2h; Ambient temperature;
With hydrogenchloride In diethyl ether
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

3,4-dimethoxy-benzaldehyde
120-14-9

3,4-dimethoxy-benzaldehyde

(Z)-α-(3,4-dimethoxyphenyl)-3,4-dimethoxycinnamonitrile
37629-72-4

(Z)-α-(3,4-dimethoxyphenyl)-3,4-dimethoxycinnamonitrile

Conditions
ConditionsYield
With sodium ethanolate In ethanol at 85℃; for 1h;98%
With sodium ethanolate In ethanol for 1h; Reflux; Inert atmosphere;97%
With sodium ethanolate In ethanol at 85℃; for 1h; Knoevenagel Condensation; Inert atmosphere;97%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

N,N-dimethyl-formamide dimethyl acetal
4637-24-5

N,N-dimethyl-formamide dimethyl acetal

Z-2-(3,4-dimethoxyphenyl)-3-dimethylaminoacrylonitrile

Z-2-(3,4-dimethoxyphenyl)-3-dimethylaminoacrylonitrile

Conditions
ConditionsYield
In N,N-dimethyl-formamide for 4h; Reflux;98%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

2-(3,4-dimethoxyphenyl)ethan-1,1-d2-1-amine hydrochloride

2-(3,4-dimethoxyphenyl)ethan-1,1-d2-1-amine hydrochloride

Conditions
ConditionsYield
Stage #1: 3,4-dimethoxyphenylacetonitrile With samarium diiodide; water-d2; triethylamine In tetrahydrofuran at 20℃; for 0.25h; Inert atmosphere;
Stage #2: With hydrogenchloride In water regioselective reaction;
98%
Stage #1: 3,4-dimethoxyphenylacetonitrile With samarium diiodide; water-d2; triethylamine In tetrahydrofuran at 20℃; for 0.25h; Inert atmosphere;
Stage #2: With hydrogenchloride
98%
Stage #1: 3,4-dimethoxyphenylacetonitrile With ethyl [2]alcohol; sodium In hexane; mineral oil at 0℃; for 0.166667h; Inert atmosphere;
Stage #2: With hydrogenchloride In diethyl ether
92%
4-[(6-hydroxyhexyl)oxy]-3,5-dimethoxybenzaldehyde
154786-34-2

4-[(6-hydroxyhexyl)oxy]-3,5-dimethoxybenzaldehyde

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

(2Z)-2-(3,4-dimethoxyphenyl)-3-{4-[(6-hydroxyhexyl)oxy]-3,5-dimethoxyphenyl}prop-2-enenitrile
1425539-63-4

(2Z)-2-(3,4-dimethoxyphenyl)-3-{4-[(6-hydroxyhexyl)oxy]-3,5-dimethoxyphenyl}prop-2-enenitrile

Conditions
ConditionsYield
97%
Pentafluorobenzene
363-72-4

Pentafluorobenzene

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

α-(3',4'-Dimethoxyphenyl)-2,3,5,6-tetrafluorophenylacetonitrile

α-(3',4'-Dimethoxyphenyl)-2,3,5,6-tetrafluorophenylacetonitrile

Conditions
ConditionsYield
With lithium tert-butoxide In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere; regioselective reaction;97%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

hexan-1-ol
111-27-3

hexan-1-ol

α-<3.4-Dimethoxy-phenyl>-caprylsaeurenitril
93148-41-5

α-<3.4-Dimethoxy-phenyl>-caprylsaeurenitril

Conditions
ConditionsYield
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate In toluene at 135℃; for 4h; Inert atmosphere;97%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

O,N-bisbenzenesulfonyl-N-methylethanolamine
85753-64-6

O,N-bisbenzenesulfonyl-N-methylethanolamine

N-[3-Cyano-3-(3,4-dimethoxy-phenyl)-propyl]-N-methyl-benzenesulfonamide
85753-65-7

N-[3-Cyano-3-(3,4-dimethoxy-phenyl)-propyl]-N-methyl-benzenesulfonamide

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran for 1.5h; -78 deg C -> 25 deg C;96%
With n-butyllithium 1.) THF, -25 deg C; Yield given. Multistep reaction;
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

2-(2-iodo-4,5-dimethoxyphenyl)acetonitrile
58432-84-1

2-(2-iodo-4,5-dimethoxyphenyl)acetonitrile

Conditions
ConditionsYield
With iodine; silver trifluoroacetate In dichloromethane at -10 - -5℃;96%
With iodine; silver trifluoroacetate In dichloromethane at -5℃; for 0.1h;93%
With Iodine monochloride; acetic acid at 20℃;72%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

3,4-dimethoxy-N,N-dimethylbenzothioamide

3,4-dimethoxy-N,N-dimethylbenzothioamide

Conditions
ConditionsYield
With sulfur; copper acetylacetonate; potassium carbonate at 110℃; for 24h; Schlenk technique;96%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

3-ethoxy-4-[(6-hydroxyhexyl)oxy]benzaldehyde
1425539-56-5

3-ethoxy-4-[(6-hydroxyhexyl)oxy]benzaldehyde

(2Z)-2-(3,4-dimethoxyphenyl)-3-{3-ethoxy-4-[(6-hydroxyhexyl)oxy]phenyl}prop-2-enenitrile
1425539-57-6

(2Z)-2-(3,4-dimethoxyphenyl)-3-{3-ethoxy-4-[(6-hydroxyhexyl)oxy]phenyl}prop-2-enenitrile

Conditions
ConditionsYield
96%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

dimethyl amine
124-40-3

dimethyl amine

2-(3,4-dimethoxyphenyl)-N,N-dimethylacetamidine

2-(3,4-dimethoxyphenyl)-N,N-dimethylacetamidine

Conditions
ConditionsYield
With copper(l) chloride In ethanol; water at 20 - 70℃; for 24h; Inert atmosphere;96%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

Diethyl carbonate
105-58-8

Diethyl carbonate

ethyl 2-cyano-2-(3,4-dimethoxyphenyl)acetate
36848-69-8

ethyl 2-cyano-2-(3,4-dimethoxyphenyl)acetate

Conditions
ConditionsYield
Stage #1: With ethanol; sodium In toluene at 80 - 85℃; for 2h;
Stage #2: 3,4-dimethoxyphenylacetonitrile; Diethyl carbonate In toluene at 80℃; for 2h;
95.6%
With sodium at 110℃; for 1h;80%
Stage #1: 3,4-dimethoxyphenylacetonitrile With sodium In ethanol; toluene
Stage #2: Diethyl carbonate at 80℃;
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

2-bromo-4,5-dimethoxyphenylacetonitrile
51655-39-1

2-bromo-4,5-dimethoxyphenylacetonitrile

Conditions
ConditionsYield
With N-Bromosuccinimide; trifluoroacetic acid In acetonitrile at 20℃; for 6h;95%
With bromine; sodium acetate; acetic acid
With N-Bromosuccinimide; trifluoroacetic acid In acetonitrile at 20℃; for 16h;15.3 g
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

cyclohexanone
108-94-1

cyclohexanone

1-[cyano-(3,4-dimethoxyphenyl)-methyl]cyclohexanol

1-[cyano-(3,4-dimethoxyphenyl)-methyl]cyclohexanol

Conditions
ConditionsYield
With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate at 0 - 15℃; for 1h;95%
With sodium hydroxide; benzyltrimethylammonium chloride In water at 0 - 15℃;71%
2-Aminonicotinaldehyde
7521-41-7

2-Aminonicotinaldehyde

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

3-(3,4-dimethoxyphenyl)-[1,8]naphthyridin-2-ylamine
1075240-57-1

3-(3,4-dimethoxyphenyl)-[1,8]naphthyridin-2-ylamine

Conditions
ConditionsYield
With aminosulfonic acid for 0.05h; microwave irradiation;95%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

3,4,5-trimethoxy-benzaldehyde
86-81-7

3,4,5-trimethoxy-benzaldehyde

(Z)-3-(3,4,5-trimethoxyphenyl)-2-(3,4-dimethoxyphenyl)acrylonitrile

(Z)-3-(3,4,5-trimethoxyphenyl)-2-(3,4-dimethoxyphenyl)acrylonitrile

Conditions
ConditionsYield
With sodium ethanolate In ethanol at 85℃; for 1h; Knoevenagel Condensation; Inert atmosphere;95%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

5-(3',4'-dimethoxybenzyl)-1H-tetrazole

5-(3',4'-dimethoxybenzyl)-1H-tetrazole

Conditions
ConditionsYield
With sodium azide; ammonium chloride In N,N-dimethyl-formamide for 24h; Reflux;95%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

C10H9(2)H2NO2

C10H9(2)H2NO2

Conditions
ConditionsYield
With water-d2; triethylamine at 20℃; for 24h; Inert atmosphere;95%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

2-(3,4-dimethoxyphenyl)acetamide
5663-56-9

2-(3,4-dimethoxyphenyl)acetamide

Conditions
ConditionsYield
With potassium hydroxide In tert-butyl alcohol for 1h; Reagent/catalyst; Solvent; Reflux;94%
With hydrogenchloride
Multi-step reaction with 3 steps
1: aq.-ethanolic KOH-solution
2: hydrogen chloride
3: aqueous ammonia
View Scheme
With Rhodococcus rhodochrous ATCC BAA 870 cobalt nitrile hydratase In aq. buffer at 30℃; pH=7.6; Enzymatic reaction;
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

4-chlorobenzaldehyde
104-88-1

4-chlorobenzaldehyde

(Z)-3-(4-chlorophenyl)-2-(3,4-dimethoxyphenyl)acrylonitrile
37629-70-2

(Z)-3-(4-chlorophenyl)-2-(3,4-dimethoxyphenyl)acrylonitrile

Conditions
ConditionsYield
With sodium methylate In ethanol at 20℃; for 2h;94%
With ethanol; sodium ethanolate
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

benzaldehyde
100-52-7

benzaldehyde

(Z)-2-(3,4-dimethoxyphenyl)-3-phenylacrylonitrile
2958-55-6

(Z)-2-(3,4-dimethoxyphenyl)-3-phenylacrylonitrile

Conditions
ConditionsYield
With sodium methylate In ethanol at 20℃; for 2h;94%
With sodium ethanolate In ethanol at 85℃; for 1h; Knoevenagel condensation; Inert atmosphere;77%
With ethanol; sodium ethanolate
With sodium ethanolate In ethanol Heating;
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

2-azidobenzaldehyde
16714-25-3

2-azidobenzaldehyde

4-(3,4-Dimethoxy-phenyl)-1,2,3,9b-tetraaza-cyclopenta[a]naphthalene

4-(3,4-Dimethoxy-phenyl)-1,2,3,9b-tetraaza-cyclopenta[a]naphthalene

Conditions
ConditionsYield
With sodium ethanolate In ethanol; acetonitrile for 12h; Ambient temperature;94%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

methyl iodide
74-88-4

methyl iodide

2‐(3,4‐dimethoxyphenyl)‐2‐methylpropionitrile
23023-16-7

2‐(3,4‐dimethoxyphenyl)‐2‐methylpropionitrile

Conditions
ConditionsYield
Stage #1: 3,4-dimethoxyphenylacetonitrile With sodium hydride In tetrahydrofuran at 0℃; for 0.5h;
Stage #2: methyl iodide In tetrahydrofuran for 12h; Product distribution / selectivity;
94%
Stage #1: 3,4-dimethoxyphenylacetonitrile With sodium hydride In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere;
Stage #2: methyl iodide In tetrahydrofuran at 0 - 20℃; for 3h; Inert atmosphere;
93%
Stage #1: 3,4-dimethoxyphenylacetonitrile With sodium hydride In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere;
Stage #2: methyl iodide In tetrahydrofuran at 0 - 20℃; for 2.5h; Inert atmosphere;
93%
3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

2,3,4-trimethoxybenzaldehyde
2103-57-3

2,3,4-trimethoxybenzaldehyde

(Z)-3-(2,3,4-trimethoxyphenyl)-2-(3,4-dimethoxyphenyl)acrylonitrile
1151666-74-8

(Z)-3-(2,3,4-trimethoxyphenyl)-2-(3,4-dimethoxyphenyl)acrylonitrile

Conditions
ConditionsYield
With sodium ethanolate In ethanol at 85℃; for 1h; Knoevenagel Condensation; Inert atmosphere;94%
With sodium ethanolate In ethanol at 85℃; for 1h; Knoevenagel Condensation; Inert atmosphere;94%
N-Acetylimidazole
2466-76-4

N-Acetylimidazole

3,4-dimethoxyphenylacetonitrile
93-17-4

3,4-dimethoxyphenylacetonitrile

α-(3,4-dimethoxyphenyl)acetoacetonitrile
18133-46-5, 63895-79-4

α-(3,4-dimethoxyphenyl)acetoacetonitrile

Conditions
ConditionsYield
With lithium hydride In dimethyl sulfoxide at 20℃; for 0.5h;94%
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