Good supplier high quality 3,4-Dimethoxy phenyl acetonitrile 93-17-4 manufacturer Product Details Overview Quick Details Pro Name;3,4-Dimethoxy phenyl acetonitrile CAS NO:93-17-4 Purity:99% Application: API Appea
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inquiryCertificate of Analysis 产品 PRODUCT 3,4-二甲氧基苯乙腈3,4-Dimethoxybenzeneacetonitrile CAS No. 93-17-4 结构式 Formula
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inquiryItems Standard Result Assay 98%min ---------------------------------------------------------------------------------------------
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inquiry1. high purity; 2. able to provide COA/HNMR/HPLC; 3. High quality; 4. low price; 5. Best service; 6.direct supplier Appearance:yellow crtstalline powder Storage:rm Package:bag/bottle/drum Application:intermediate for cefuroxime Transp
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inquiryUnique advantages for (3,4-Dimethoxyphenyl)acetonitrile Cas 93-17-4 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White to light yellow powder Storage:N/A Package:25kg/dru
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inquiryHomoveratryl Amine[CAS:120-20-7] 2-(3,4-Dimethoxyphenyl) Ethylamine Homoveratryl Acid[CAS:93-40-3] (3,4-Dimethoxyphenyl) Acetic Acid HANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and con
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inquiry(3,4-Dimethoxyphenyl)acetonitrile Basic information Product Name: (3,4-Dimethoxyphenyl)acetonitrile Synonyms: TIMTEC-BB SBB005899;3,4-dimethoxy-benzeneacetonitril;3,4-dimethoxybenzeneace
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryProduct name (3 4-Dimethoxyphenyl)acetonitrile Synonyms Homoveratronitrite;3,4-Dimethoxylphenylacetonitrile;(3,4-Dimethoxyphenyl)acetonitrile, 3,4-Dimethoxybenzylcyanide, Homoveratronitrile;(3,4-
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inquiryAppearance:white to almost white crystals or cryst. needles Storage:Room temperature Package:25kg/drum Application:intermediate Transportation:Express/Sea/Air Port:Any port in china
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inquiry(3,4-Dimethoxyphenyl)acetonitrile Chemical Properties Melting point 54-57 °C(lit.) Boiling point 171-178 °C10 mm Hg(lit.) density 1.1607 (rough estimate) refractive index 1.5168 (estimate) Fp >230 °F storage temp.
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(3,4-Dimethoxyphenyl)acetonitrile CAS 93-17-4 Our advantage 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purch
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inquiryAppearance:white or yellowish white flaky crystal Storage:Keep the sun from direct sunlight ;prevention against high temperature Package:As customer request Application:Used for research and industrial manufacture. Transportatio
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inquiry(3,4-Dimethoxyphenyl)acetonitrile CAS 93-17-4 Description Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establish
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inquiryConditions | Yield |
---|---|
With ethyl phosphodichloridite; 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane at 20℃; for 2h; | 92% |
Conditions | Yield |
---|---|
With sodium cyanide | 91% |
α-(3,4-dimethoxyphenyl)-α-(methylthio)acetonitrile
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With acetic acid; zinc at 100℃; for 1h; | 90% |
2-(3,4-dimethoxyphenyl)acetaldehyde oxime
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With trimethylsilyl iodide; 1,1,1,3,3,3-hexamethyl-disilazane In chloroform at 56℃; for 4h; | 86% |
With trimethylsilyl iodide; 1,1,1,3,3,3-hexamethyl-disilazane In chloroform at 56℃; for 4h; Product distribution; other temperature, without hexamethyldisilazane (TMS2NH); | 86% |
With acetic anhydride | |
With trimethylsilyl iodide In chloroform for 2h; Ambient temperature; | 40 mg |
4-isoxazoleboronic acid pinacol ester
4-Bromoveratrole
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium fluoride; water In dimethyl sulfoxide at 130℃; for 16h; Domino Suzuki coupling and fragmentation reaction; Inert atmosphere; | 84% |
3,4-Dimethoxyphenylthioacetamid
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With 1-oxa-2-azaspiro[2.5]octane In toluene at 20 - 25℃; for 4h; | 82% |
4-Bromoveratrole
acetonitrile
A
3,4-dimethoxyphenylacetonitrile
B
bis(3,4-dimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
With ethoxyethoxyethanol; sodium amide In 1,2-dimethoxyethane 1.) 45 deg C, 2 h, 2.) -10 deg C, 2 h, 3.) -45 deg C, 4.5 h; | A 78% B 8% |
sodium cyanide
1-(3,4-Dimethoxy-benzyl)-2-methylsulfanyl-4,6-diphenyl-pyridinium; iodide
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane for 24h; Heating; | 76% |
potassium cyanide
4-chloromethyl-1,2-dimethoxy-benzene
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
In dimethyl sulfoxide for 20h; | 67% |
With benzene | |
With hydrogenchloride |
Conditions | Yield |
---|---|
With iodine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide at 65℃; for 3h; | 64% |
2-bromo-4,5-dimethoxyphenylacetonitrile
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
Stage #1: 2-bromo-4,5-dimethoxyphenylacetonitrile With nickel(II) iodide; 1,4-bis(dicyclohexylphosphino)butane; sodium carbonate; cesium iodide In tetrahydrofuran for 0.25h; Schlenk technique; Glovebox; Stage #2: In tetrahydrofuran at 35℃; for 72h; Irradiation; | 54% |
(3,4-Dimethoxyphenyl)acetic acid
4-(methylsulfonyl)benzonitrile
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With riboflavin-2',3',4',5'-tetra-acetate In acetonitrile at 25℃; for 12h; Inert atmosphere; Irradiation; Sealed tube; | 45% |
Conditions | Yield |
---|---|
With acetic anhydride |
2-(3,4-dimethoxyphenyl)acetaldehyde oxime
acetic anhydride
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With p-menth-1-ene; palladium on activated charcoal |
sodium cyanide
(3,4-dimethoxyphenyl)methanol
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
(i) aq. HCl, CH2Cl2, (ii) /BRN= 3587243/, KI, acetone; Multistep reaction; | |
(i) aq. HCl, (ii) /BRN= 3587243/, DMSO; Multistep reaction; |
4-bromomethyl-1,2-dimethoxybenzene
sodium cyanide
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
In ethanol; water for 5h; Heating; |
ethyl 2-cyano-2-(3,4-dimethoxyphenyl)acetate
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With sodium hydroxide In water at 80 - 90℃; for 2h; Yield given; |
Phosphoric acid cyano-(3,4-dimethoxy-phenyl)-methyl ester diethyl ester
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethyl acetate for 2h; Ambient temperature; Yield given; |
3-hydroxy-4-methoxyphenylacetonitrile
dimethyl sulfate
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With sodium hydroxide at 0℃; for 1h; |
sodium cyanide
4-chloromethyl-1,2-dimethoxy-benzene
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
In 1,4-dioxane; water | |
In water; benzene for 6h; Heating; Yield given; |
sodium cyanide
4-chloromethyl-1,2-dimethoxy-benzene
A
3,4-dimethoxyphenylacetonitrile
B
(Z)-1,2-dicyano-1,2-bis(3,4-dimethoxyphenyl)ethene
Conditions | Yield |
---|---|
In tetrachloromethane; water Heating; |
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With p-menth-1-ene; palladium | |
With tetralin; palladium |
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
at 155℃; |
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With palladium; benzene Hydrogenation; |
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With acetic anhydride |
tetralin
2-benzoyloxy-2-(3',4'-dimethoxyphenyl)-acetonitrile
3,4-dimethoxyphenylacetonitrile
2-benzoyloxy-2-(3',4'-dimethoxyphenyl)-acetonitrile
3,4-dimethoxyphenylacetonitrile
4-bromomethyl-1,2-dimethoxybenzene
potassium cyanide
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
In ethanol; water for 4h; Substitution; Heating; |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In acetic acid for 4h; | 100% |
Stage #1: 3,4-dimethoxyphenylacetonitrile With diborane In tetrahydrofuran at 55℃; for 16h; Inert atmosphere; Stage #2: With hydrogenchloride; water In tetrahydrofuran at 0 - 20℃; Stage #3: With sodium hydroxide In tetrahydrofuran; water | 99% |
With hydrogen; nickel In ethanol at 40℃; electrocatalytic hydrogenation; | 98% |
Conditions | Yield |
---|---|
With hydrogenchloride; hydrogen In propan-1-ol; water at 60℃; under 375.038 Torr; for 18h; Flow reactor; | 100% |
Stage #1: 3,4-dimethoxyphenylacetonitrile With borane-ammonia complex; C17H16BrMnN2O3S In hexane at 60℃; for 12h; Stage #2: With hydrogenchloride In diethyl ether; water | 90% |
1-η**(5)-ferrocenyl-3,3-bis(methylthio)prop-2-en-1-one
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
Stage #1: 3,4-dimethoxyphenylacetonitrile With sodium hydride In N,N-dimethyl-formamide; mineral oil; benzene at 0℃; for 0.25h; Stage #2: 3,3-bis(methylsulfanyl)-1-η5-ferrocenyl-2-propen-1-one In N,N-dimethyl-formamide; mineral oil; benzene at 0 - 20℃; | 100% |
3,4-dimethoxyphenylacetonitrile
4-methoxy-benzaldehyde
(Z)-2-(3,4-dimethoxyphenyl)-3-(4-methoxyphenyl)acrylonitrile
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol Reflux; Inert atmosphere; | 99% |
With sodium methylate In ethanol at 20℃; for 3h; | 92% |
With sodium ethanolate In ethanol at 85℃; for 1h; Knoevenagel Condensation; Inert atmosphere; | 90% |
ethanol
3,4-dimethoxyphenylacetonitrile
ethyl 2-(3,4-dimethoxyphenyl)acetoimidate hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride at 0 - 5℃; Addition; | 99% |
With hydrogenchloride | 88% |
With hydrogenchloride In chloroform for 2h; Ambient temperature; | |
With hydrogenchloride In diethyl ether |
3,4-dimethoxyphenylacetonitrile
3,4-dimethoxy-benzaldehyde
(Z)-α-(3,4-dimethoxyphenyl)-3,4-dimethoxycinnamonitrile
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 85℃; for 1h; | 98% |
With sodium ethanolate In ethanol for 1h; Reflux; Inert atmosphere; | 97% |
With sodium ethanolate In ethanol at 85℃; for 1h; Knoevenagel Condensation; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide for 4h; Reflux; | 98% |
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
Stage #1: 3,4-dimethoxyphenylacetonitrile With samarium diiodide; water-d2; triethylamine In tetrahydrofuran at 20℃; for 0.25h; Inert atmosphere; Stage #2: With hydrogenchloride In water regioselective reaction; | 98% |
Stage #1: 3,4-dimethoxyphenylacetonitrile With samarium diiodide; water-d2; triethylamine In tetrahydrofuran at 20℃; for 0.25h; Inert atmosphere; Stage #2: With hydrogenchloride | 98% |
Stage #1: 3,4-dimethoxyphenylacetonitrile With ethyl [2]alcohol; sodium In hexane; mineral oil at 0℃; for 0.166667h; Inert atmosphere; Stage #2: With hydrogenchloride In diethyl ether | 92% |
4-[(6-hydroxyhexyl)oxy]-3,5-dimethoxybenzaldehyde
3,4-dimethoxyphenylacetonitrile
(2Z)-2-(3,4-dimethoxyphenyl)-3-{4-[(6-hydroxyhexyl)oxy]-3,5-dimethoxyphenyl}prop-2-enenitrile
Conditions | Yield |
---|---|
97% |
Conditions | Yield |
---|---|
With lithium tert-butoxide In N,N-dimethyl-formamide at 20℃; for 0.5h; Inert atmosphere; regioselective reaction; | 97% |
3,4-dimethoxyphenylacetonitrile
hexan-1-ol
α-<3.4-Dimethoxy-phenyl>-caprylsaeurenitril
Conditions | Yield |
---|---|
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate In toluene at 135℃; for 4h; Inert atmosphere; | 97% |
3,4-dimethoxyphenylacetonitrile
O,N-bisbenzenesulfonyl-N-methylethanolamine
N-[3-Cyano-3-(3,4-dimethoxy-phenyl)-propyl]-N-methyl-benzenesulfonamide
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran for 1.5h; -78 deg C -> 25 deg C; | 96% |
With n-butyllithium 1.) THF, -25 deg C; Yield given. Multistep reaction; |
3,4-dimethoxyphenylacetonitrile
2-(2-iodo-4,5-dimethoxyphenyl)acetonitrile
Conditions | Yield |
---|---|
With iodine; silver trifluoroacetate In dichloromethane at -10 - -5℃; | 96% |
With iodine; silver trifluoroacetate In dichloromethane at -5℃; for 0.1h; | 93% |
With Iodine monochloride; acetic acid at 20℃; | 72% |
3,4-dimethoxyphenylacetonitrile
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
With sulfur; copper acetylacetonate; potassium carbonate at 110℃; for 24h; Schlenk technique; | 96% |
3,4-dimethoxyphenylacetonitrile
3-ethoxy-4-[(6-hydroxyhexyl)oxy]benzaldehyde
(2Z)-2-(3,4-dimethoxyphenyl)-3-{3-ethoxy-4-[(6-hydroxyhexyl)oxy]phenyl}prop-2-enenitrile
Conditions | Yield |
---|---|
96% |
Conditions | Yield |
---|---|
With copper(l) chloride In ethanol; water at 20 - 70℃; for 24h; Inert atmosphere; | 96% |
3,4-dimethoxyphenylacetonitrile
Diethyl carbonate
ethyl 2-cyano-2-(3,4-dimethoxyphenyl)acetate
Conditions | Yield |
---|---|
Stage #1: With ethanol; sodium In toluene at 80 - 85℃; for 2h; Stage #2: 3,4-dimethoxyphenylacetonitrile; Diethyl carbonate In toluene at 80℃; for 2h; | 95.6% |
With sodium at 110℃; for 1h; | 80% |
Stage #1: 3,4-dimethoxyphenylacetonitrile With sodium In ethanol; toluene Stage #2: Diethyl carbonate at 80℃; |
3,4-dimethoxyphenylacetonitrile
2-bromo-4,5-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With N-Bromosuccinimide; trifluoroacetic acid In acetonitrile at 20℃; for 6h; | 95% |
With bromine; sodium acetate; acetic acid | |
With N-Bromosuccinimide; trifluoroacetic acid In acetonitrile at 20℃; for 16h; | 15.3 g |
Conditions | Yield |
---|---|
With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate at 0 - 15℃; for 1h; | 95% |
With sodium hydroxide; benzyltrimethylammonium chloride In water at 0 - 15℃; | 71% |
2-Aminonicotinaldehyde
3,4-dimethoxyphenylacetonitrile
3-(3,4-dimethoxyphenyl)-[1,8]naphthyridin-2-ylamine
Conditions | Yield |
---|---|
With aminosulfonic acid for 0.05h; microwave irradiation; | 95% |
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 85℃; for 1h; Knoevenagel Condensation; Inert atmosphere; | 95% |
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With sodium azide; ammonium chloride In N,N-dimethyl-formamide for 24h; Reflux; | 95% |
3,4-dimethoxyphenylacetonitrile
Conditions | Yield |
---|---|
With water-d2; triethylamine at 20℃; for 24h; Inert atmosphere; | 95% |
Conditions | Yield |
---|---|
With potassium hydroxide In tert-butyl alcohol for 1h; Reagent/catalyst; Solvent; Reflux; | 94% |
With hydrogenchloride | |
Multi-step reaction with 3 steps 1: aq.-ethanolic KOH-solution 2: hydrogen chloride 3: aqueous ammonia View Scheme | |
With Rhodococcus rhodochrous ATCC BAA 870 cobalt nitrile hydratase In aq. buffer at 30℃; pH=7.6; Enzymatic reaction; |
3,4-dimethoxyphenylacetonitrile
4-chlorobenzaldehyde
(Z)-3-(4-chlorophenyl)-2-(3,4-dimethoxyphenyl)acrylonitrile
Conditions | Yield |
---|---|
With sodium methylate In ethanol at 20℃; for 2h; | 94% |
With ethanol; sodium ethanolate |
3,4-dimethoxyphenylacetonitrile
benzaldehyde
(Z)-2-(3,4-dimethoxyphenyl)-3-phenylacrylonitrile
Conditions | Yield |
---|---|
With sodium methylate In ethanol at 20℃; for 2h; | 94% |
With sodium ethanolate In ethanol at 85℃; for 1h; Knoevenagel condensation; Inert atmosphere; | 77% |
With ethanol; sodium ethanolate | |
With sodium ethanolate In ethanol Heating; |
3,4-dimethoxyphenylacetonitrile
2-azidobenzaldehyde
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol; acetonitrile for 12h; Ambient temperature; | 94% |
3,4-dimethoxyphenylacetonitrile
methyl iodide
2‐(3,4‐dimethoxyphenyl)‐2‐methylpropionitrile
Conditions | Yield |
---|---|
Stage #1: 3,4-dimethoxyphenylacetonitrile With sodium hydride In tetrahydrofuran at 0℃; for 0.5h; Stage #2: methyl iodide In tetrahydrofuran for 12h; Product distribution / selectivity; | 94% |
Stage #1: 3,4-dimethoxyphenylacetonitrile With sodium hydride In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran at 0 - 20℃; for 3h; Inert atmosphere; | 93% |
Stage #1: 3,4-dimethoxyphenylacetonitrile With sodium hydride In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran at 0 - 20℃; for 2.5h; Inert atmosphere; | 93% |
3,4-dimethoxyphenylacetonitrile
2,3,4-trimethoxybenzaldehyde
(Z)-3-(2,3,4-trimethoxyphenyl)-2-(3,4-dimethoxyphenyl)acrylonitrile
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 85℃; for 1h; Knoevenagel Condensation; Inert atmosphere; | 94% |
With sodium ethanolate In ethanol at 85℃; for 1h; Knoevenagel Condensation; Inert atmosphere; | 94% |
N-Acetylimidazole
3,4-dimethoxyphenylacetonitrile
α-(3,4-dimethoxyphenyl)acetoacetonitrile
Conditions | Yield |
---|---|
With lithium hydride In dimethyl sulfoxide at 20℃; for 0.5h; | 94% |
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