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2-(4-chloro-2-methylphenoxy)ethanol
sodium 2-methyl-4-chlorophenoxyacetate
Conditions | Yield |
---|---|
With sodium hydroxide; oxygen; bismuth(III) nitrate; palladium on activated charcoal at 90℃; for 2h; | 98% |
2-methyl-4-chlorophenol
sodium monochloroacetic acid
sodium 2-methyl-4-chlorophenoxyacetate
Conditions | Yield |
---|---|
With sodium hydroxide In water for 8h; Reflux; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium carbonate / toluene / 0.5 h / 120 °C 2: iron(III) chloride; tert-butyl methyl sulphide; thionyl chloride / 0.5 h / 40 °C 3: sodium hydroxide / 4 h / 70 °C View Scheme |
sodium 2-methyl-4-chlorophenoxyacetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: iron(III) chloride; tert-butyl methyl sulphide; thionyl chloride / 0.5 h / 40 °C 2: sodium hydroxide / 4 h / 70 °C View Scheme |
Conditions | Yield |
---|---|
With sodium hydroxide at 70℃; for 4h; | 223.74 g |
C19H40NO(1+)*Cl(1-)
sodium 2-methyl-4-chlorophenoxyacetate
cyclohexyldecyloxymethyldimethylammonium 4-chloro-2-methylphenoxyacetate
Conditions | Yield |
---|---|
In water-d2 at 20℃; for 24h; | 98% |
Cl(1-)*C13H28NO(1+)
sodium 2-methyl-4-chlorophenoxyacetate
butoxymethylcyclohexyldimethylammonium 4-chloro-2-methylphenoxyacetate
Conditions | Yield |
---|---|
In water-d2 at 20℃; for 24h; | 94% |
C21H44NO(1+)*Cl(1-)
sodium 2-methyl-4-chlorophenoxyacetate
cyclohexyldodecyloxymethyldimethylammonium 4-chloro-2-methylphenoxyacetate
Conditions | Yield |
---|---|
In water-d2 at 20℃; for 24h; | 94% |
C15H32NO(1+)*Cl(1-)
sodium 2-methyl-4-chlorophenoxyacetate
cyclohexylhexyloxymethyldimethylammonium 4-chloro-2-methylphenoxyacetate
Conditions | Yield |
---|---|
In water-d2 at 20℃; for 24h; | 93% |
sodium 2-methyl-4-chlorophenoxyacetate
8-hydroxy-1-octyl-quinolinium (4-chloro-2-methylphenoxy)acetate
Conditions | Yield |
---|---|
In methanol for 12h; | 90% |
C17H36NO(1+)*Cl(1-)
sodium 2-methyl-4-chlorophenoxyacetate
cyclohexyldimethyloctyloxymethylammonium 4-chloro-2-methylphenoxyacetate
Conditions | Yield |
---|---|
In water-d2 at 20℃; for 24h; | 90% |
C23H48NO(1+)*Cl(1-)
sodium 2-methyl-4-chlorophenoxyacetate
cyclohexyldimethyltetradecyloxymethylammonium 4-chloro-2-methylphenoxyacetate
Conditions | Yield |
---|---|
In water-d2 at 20℃; for 24h; | 86% |
1,2,3-trimethyl-benzimidazolium; chloride
sodium 2-methyl-4-chlorophenoxyacetate
Conditions | Yield |
---|---|
In methanol at 65℃; | 71% |
methanol
salicylhydroxamic acid
di-2-pyridyl ketone oxime
sodium 2-methyl-4-chlorophenoxyacetate
Conditions | Yield |
---|---|
With sodium methoxide In methanol salicylhydroxamic acid, di(2pyridyl)ketonoxime, excess MeONa and NaCl2*6H2O were dissolved in MeOH and stirred for 1 h, sodium salt MCPA was added; elem. anal.; | 60% |
sodium 2-methyl-4-chlorophenoxyacetate
Conditions | Yield |
---|---|
In water elem. anal.; |
zinc(II) nitrate
sodium 2-methyl-4-chlorophenoxyacetate
Conditions | Yield |
---|---|
With H2O In water double decompn. react. between zinc nitrate and the sodium butyrate in aq. soln.; elem. anal.; | |
With H2O In water ion exchange react. in aq. soln.; pptn.; |
methanol
di-2-pyridyl ketone oxime
Salicylhydroxamic acid
sodium 2-methyl-4-chlorophenoxyacetate
Conditions | Yield |
---|---|
With NaOH In methanol addn. of Na-salt of substituted phenoxyacetic acid to mixt. of other educts and NaOH; crystn. on slow evapn. (48 h); elem. anal.; |
4-dodecyl-4-methyl-morpholine chloride
sodium 2-methyl-4-chlorophenoxyacetate
4-dodecyl-4-methyl-morpholine (4-chloro-2-methylphenoxy)acetate
Conditions | Yield |
---|---|
In water at 20℃; for 24h; |
3,5-diphenyl-1,2-dimethylpyrazolium chloride
sodium 2-methyl-4-chlorophenoxyacetate
Conditions | Yield |
---|---|
In water at 19.84℃; for 24h; |
Conditions | Yield |
---|---|
With hydrogenchloride In water pH=1; |
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