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inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1232.html Product Name 3-Benzyloxyphenol
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inquiryName: Benzyl 3-hydroxyphenyl ether CAS: 3769-41-3 MF: C13H12O2 Appearance:White Powder Storage:Store in cool and dry place, away from sun light. Package:25kg Application:APIs Transportation:By sea or by air Port:Qingdao Port
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Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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Shanghai Finebiotech Co.,Ltd.was established in 2020, which providing professional chemical services. As a customer-oriented company, we have distinguished ourself from others in providing worldwide customers with cost-effective and efficient service
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white to light yellow crystal powder Storage:Room temperature with sealed well Package:according to the clients requirement Appl
3-Benzyloxyphenol cas 3769-41-3Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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Changzhou Helios Biochemical Co., Ltd is a leading manufacturer and supplier for medical intermediates and pesticide intermediates . We specialize in custom synthesis of benzene ring, pyridine and pyrimidine derivatives to help customers to accelerat
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inquiry1-benzoyloxy-3-benzyloxy-benzene
3-Benzyloxyphenol
Conditions | Yield |
---|---|
With sodium hydroxide In methanol | 99% |
3-Benzyloxyphenol
Conditions | Yield |
---|---|
With acetic acid; trifluoroacetic acid In water for 0.0666667h; Reflux; | 98% |
3-Benzyloxyphenyl acetate
3-Benzyloxyphenol
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran | 96% |
With sodium hydroxide In tetrahydrofuran | 96% |
3-Benzyloxyphenol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol at 20℃; for 1h; | 86% |
3-(benzyloxy)phenylboronic acid
3-Benzyloxyphenol
Conditions | Yield |
---|---|
With dihydrogen peroxide In water at 30℃; Green chemistry; | 85% |
Conditions | Yield |
---|---|
With potassium carbonate at 80℃; for 2h; | 83% |
With potassium carbonate In acetone Heating; | 77% |
With potassium carbonate In acetonitrile for 96h; Heating; | 70% |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In acetic acid at 25℃; under 760 Torr; | 81% |
1-(benzyloxy)-3-iodobenzene
3-Benzyloxyphenol
Conditions | Yield |
---|---|
With basolite C300; potassium hydroxide In water; dimethyl sulfoxide at 125℃; for 12h; | 80% |
3-((2-Bromobenzyl)oxy)phenol
3-Benzyloxyphenol
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium tert-butylate In N,N-dimethyl-formamide at 95℃; for 48h; | 77% |
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetone for 48.5h; Reflux; | 72% |
Stage #1: benzyl chloride; recorcinol In dimethyl sulfoxide at 20℃; Stage #2: With potassium hydroxide at 90℃; for 16h; | 55% |
With sodium hydride In N,N-dimethyl-formamide for 18h; Ambient temperature; | 54% |
3-Benzyloxyphenol
Conditions | Yield |
---|---|
With boron tribromide dimethyl sulfide complex In dichloromethane for 0.416667h; Inert atmosphere; | 70% |
Multi-step reaction with 3 steps 1: peracetic acid; acetic acid / dichloromethane / 0.07 h 2: N,O-bis-(trimethylsilyl)-acetamide / toluene / 0.58 h / Reflux 3: acetic acid; trifluoroacetic acid / water / 0.07 h / Reflux View Scheme |
Conditions | Yield |
---|---|
Stage #1: 3-(benzyloxy)aniline With sulfuric acid at 20℃; Cooling with ice; Stage #2: With sodium nitrite In water Reflux; | 64% |
A
3-Benzyloxyphenol
Conditions | Yield |
---|---|
In toluene Reflux; Inert atmosphere; | A n/a B 63% |
Conditions | Yield |
---|---|
Stage #1: recorcinol With pyridine; poly(ethylene glycol) 4000; oxalyl dichloride In dichloromethane at 20℃; for 18h; Stage #2: PhCH2-halide With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 18h; Stage #3: With sodium hydroxide at 20℃; for 2h; | 56% |
benzyl bromide
recorcinol
A
1,3-bis(benzyloxy)benzene
B
3-Benzyloxyphenol
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 60℃; for 4h; | A n/a B 32% |
Conditions | Yield |
---|---|
With N,N-dimethyl-formamide; silver(l) oxide Behandeln des erhaltenen Reaktionsprodukts mit aethanol. KOH; |
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; for 24h; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 76 percent / PPh3; diisopropyl azodicarboxylate / tetrahydrofuran 2: 99 percent / aq. NaOH / methanol View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 76 percent / PPh3; diisopropyl azodicarboxylate / tetrahydrofuran 2: 99 percent / aq. NaOH / methanol View Scheme |
1-(benzyloxy)-3-(prop-2-yn-1-yloxy)benzene
A
3-Benzyloxyphenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: copper(I) thiophene-2-carboxylate / toluene / 2 h / 20 °C / Inert atmosphere 2: toluene / Reflux; Inert atmosphere View Scheme |
3-Benzyloxyphenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: ammonia / methanol / 0.33 h / 20 °C 2.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 2.2: 0.33 h / 20 °C / Inert atmosphere 3.1: boron tribromide dimethyl sulfide complex / dichloromethane / 0.42 h / Inert atmosphere View Scheme | |
Multi-step reaction with 5 steps 1.1: ammonia / methanol / 0.33 h / 20 °C 2.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 2.2: 0.33 h / 20 °C / Inert atmosphere 3.1: peracetic acid; acetic acid / dichloromethane / 0.07 h 4.1: N,O-bis-(trimethylsilyl)-acetamide / toluene / 0.58 h / Reflux 5.1: acetic acid; trifluoroacetic acid / water / 0.07 h / Reflux View Scheme |
3-Benzyloxyphenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N,O-bis-(trimethylsilyl)-acetamide / toluene / 0.58 h / Reflux 2: acetic acid; trifluoroacetic acid / water / 0.07 h / Reflux View Scheme |
3-Benzyloxyphenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: acetic acid / 2.5 h / Reflux 2.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 2.2: 0.33 h / 20 °C / Inert atmosphere 3.1: boron tribromide dimethyl sulfide complex / dichloromethane / 0.42 h / Inert atmosphere View Scheme | |
Multi-step reaction with 5 steps 1.1: acetic acid / 2.5 h / Reflux 2.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 2.2: 0.33 h / 20 °C / Inert atmosphere 3.1: peracetic acid; acetic acid / dichloromethane / 0.07 h 4.1: N,O-bis-(trimethylsilyl)-acetamide / toluene / 0.58 h / Reflux 5.1: acetic acid; trifluoroacetic acid / water / 0.07 h / Reflux View Scheme |
3-Benzyloxyphenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h 2.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 2.2: 0.33 h / 20 °C / Inert atmosphere 3.1: boron tribromide dimethyl sulfide complex / dichloromethane / 0.42 h / Inert atmosphere View Scheme | |
Multi-step reaction with 5 steps 1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.08 h 2.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 2.2: 0.33 h / 20 °C / Inert atmosphere 3.1: peracetic acid; acetic acid / dichloromethane / 0.07 h 4.1: N,O-bis-(trimethylsilyl)-acetamide / toluene / 0.58 h / Reflux 5.1: acetic acid; trifluoroacetic acid / water / 0.07 h / Reflux View Scheme |
3-Benzyloxyphenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: hydrogenchloride / water / 1 h / 75 °C 2.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 2.2: 0.33 h / 20 °C / Inert atmosphere 3.1: boron tribromide dimethyl sulfide complex / dichloromethane / 0.42 h / Inert atmosphere View Scheme | |
Multi-step reaction with 5 steps 1.1: hydrogenchloride / water / 1 h / 75 °C 2.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 2.2: 0.33 h / 20 °C / Inert atmosphere 3.1: peracetic acid; acetic acid / dichloromethane / 0.07 h 4.1: N,O-bis-(trimethylsilyl)-acetamide / toluene / 0.58 h / Reflux 5.1: acetic acid; trifluoroacetic acid / water / 0.07 h / Reflux View Scheme |
3-Benzyloxyphenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: acetic acid / water / 0.02 h / Reflux 2.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 2.2: 0.33 h / 20 °C / Inert atmosphere 3.1: boron tribromide dimethyl sulfide complex / dichloromethane / 0.42 h / Inert atmosphere View Scheme | |
Multi-step reaction with 5 steps 1.1: acetic acid / water / 0.02 h / Reflux 2.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 2.2: 0.33 h / 20 °C / Inert atmosphere 3.1: peracetic acid; acetic acid / dichloromethane / 0.07 h 4.1: N,O-bis-(trimethylsilyl)-acetamide / toluene / 0.58 h / Reflux 5.1: acetic acid; trifluoroacetic acid / water / 0.07 h / Reflux View Scheme |
3-Benzyloxyphenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 1.2: 0.33 h / 20 °C / Inert atmosphere 2.1: boron tribromide dimethyl sulfide complex / dichloromethane / 0.42 h / Inert atmosphere View Scheme | |
Multi-step reaction with 4 steps 1.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 1.2: 0.33 h / 20 °C / Inert atmosphere 2.1: peracetic acid; acetic acid / dichloromethane / 0.07 h 3.1: N,O-bis-(trimethylsilyl)-acetamide / toluene / 0.58 h / Reflux 4.1: acetic acid; trifluoroacetic acid / water / 0.07 h / Reflux View Scheme |
3-Benzyloxyphenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: hydrogen bromide / water / 1.17 h / Reflux 2.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 2.2: 0.33 h / 20 °C / Inert atmosphere 3.1: boron tribromide dimethyl sulfide complex / dichloromethane / 0.42 h / Inert atmosphere View Scheme | |
Multi-step reaction with 5 steps 1.1: hydrogen bromide / water / 1.17 h / Reflux 2.1: sodium hydride / N,N-dimethyl-formamide / 0.08 h / 55 °C / Inert atmosphere 2.2: 0.33 h / 20 °C / Inert atmosphere 3.1: peracetic acid; acetic acid / dichloromethane / 0.07 h 4.1: N,O-bis-(trimethylsilyl)-acetamide / toluene / 0.58 h / Reflux 5.1: acetic acid; trifluoroacetic acid / water / 0.07 h / Reflux View Scheme |
3-Benzyloxyphenol
1-Bromo-2-bromomethyl-benzene
1-bromo-2-(3-benzyloxyphenyloxymethyl)benzene
Conditions | Yield |
---|---|
Stage #1: 3-Benzyloxyphenol With sodium hydride In tetrahydrofuran for 0.5h; Metallation; Heating; Stage #2: 1-Bromo-2-bromomethyl-benzene In tetrahydrofuran for 4h; Etherification; Heating; Further stages.; | 100% |
3-Benzyloxyphenol
2-bromo-4-fluorobenzaldehyde
4-(3-benzyloxy-phenoxy)-2-bromo-benzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 16h; Product distribution / selectivity; | 100% |
With caesium carbonate In N,N-dimethyl-formamide at 80℃; |
Conditions | Yield |
---|---|
Stage #1: 3-Benzyloxyphenol With sodium hydride In tetrahydrofuran Stage #2: ethyl phosphodichloridite In tetrahydrofuran Reflux; | 98% |
With sodium hydride In tetrahydrofuran Reflux; | 98% |
1-(diphenylmethyl)-1H-indole-2,3-dione
3-Benzyloxyphenol
3-[4-(benzyloxy)-2-hydroxyphenyl]-1-(diphenylmethyl)-3-hydroxy-1,3-dihydro-2H-indol-2-one
Conditions | Yield |
---|---|
Stage #1: 3-Benzyloxyphenol With isopropylmagnesium chloride In tetrahydrofuran at 0℃; Stage #2: 1-(diphenylmethyl)-1H-indole-2,3-dione In dichloromethane at 0 - 20℃; Stage #3: With water; ammonium chloride In dichloromethane | 97% |
Stage #1: 3-Benzyloxyphenol With isopropylmagnesium chloride In tetrahydrofuran at 0℃; Stage #2: 1-(diphenylmethyl)-1H-indole-2,3-dione In tetrahydrofuran; dichloromethane at 0 - 20℃; for 16h; Stage #3: With ammonium chloride In tetrahydrofuran; dichloromethane | 97% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 12h; Inert atmosphere; | 95.2% |
3-Benzyloxyphenol
2-chlorophenylsulfonyl chloride
2-Chlorobenzenesulfonic acid 3-benzyloxyphenyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane | 95% |
3-iodopropionaldehyde dimethylacetal
3-Benzyloxyphenol
3-(3-benzyloxyphenoxy)propionaldehyde dimethyl acetal
Conditions | Yield |
---|---|
Stage #1: 3-Benzyloxyphenol With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; Stage #2: 3-iodopropionaldehyde dimethylacetal at 20℃; | 93% |
With potassium hydroxide 1) THF, r.t., 2) THF, reflux; Yield given. Multistep reaction; | |
With potassium hydroxide In tetrahydrofuran | |
With potassium hydroxide In tetrahydrofuran for 17h; Heating; |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 93% |
3-Benzyloxyphenol
chloromethyl methyl ether
3-Benzyloxy-1-methoxymethoxybenzene
Conditions | Yield |
---|---|
Stage #1: 3-Benzyloxyphenol With sodium hydride In tetrahydrofuran at 20℃; for 0.166667h; Metallation; Stage #2: chloromethyl methyl ether In tetrahydrofuran; N,N-dimethyl-formamide at 20℃; for 1h; Etherification; | 91% |
With N-ethyl-N,N-diisopropylamine In dichloromethane |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide | 91% |
3-Benzyloxyphenol
methyl chloroacetate
(3-Benzyloxy-phenoxy)-acetic acid methyl ester
Conditions | Yield |
---|---|
With potassium carbonate; sodium iodide In acetone for 10h; Heating; | 90% |
3-Benzyloxyphenol
N,N-Dimethylthiocarbamoyl chloride
O-(3-benzyloxy)phenyldimethylthiocarbamate
Conditions | Yield |
---|---|
With sodium hydride In dimethyl sulfoxide at 20℃; for 2h; | 90% |
3-Benzyloxyphenol
propargyl bromide
1-(benzyloxy)-3-(prop-2-yn-1-yloxy)benzene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide; toluene at 20℃; for 7h; Inert atmosphere; | 90% |
With potassium carbonate In N,N-dimethyl-formamide; toluene at 20℃; for 7h; Inert atmosphere; | 90% |
With potassium carbonate In acetone for 24h; Inert atmosphere; Reflux; | 77% |
Conditions | Yield |
---|---|
Stage #1: C14H7ClF4O2 With thionyl chloride In dichloromethane at 20℃; for 5h; Stage #2: 3-Benzyloxyphenol With pyridine In dichloromethane at 20℃; for 48h; | 89.7% |
4-(benzyloxy)-2,3-difluorobenzoic acid
3-Benzyloxyphenol
Conditions | Yield |
---|---|
Stage #1: 4-(benzyloxy)-2,3-difluorobenzoic acid With thionyl chloride In dichloromethane for 5h; Reflux; Stage #2: 3-Benzyloxyphenol With pyridine In dichloromethane at 20℃; for 48h; | 89.7% |
3-Benzyloxyphenol
4-(4-dodecyloxybenzoyloxy)benzoic acid
1-benzyloxyphenylene-3-(4-n-dodecyloxybenzoyloxy-4-benzoate)
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane | 89% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; | |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 24h; | |
With dmap; dicyclohexyl-carbodiimide In dichloromethane |
Conditions | Yield |
---|---|
With triethylamine; magnesium chloride In tetrahydrofuran Inert atmosphere; Reflux; regioselective reaction; | 88% |
3-Benzyloxyphenol
4-(bromomethyl)benzaldehyde
Conditions | Yield |
---|---|
Stage #1: 3-Benzyloxyphenol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 0.283333h; Inert atmosphere; Sonication; Stage #2: 4-(bromomethyl)benzaldehyde In N,N-dimethyl-formamide at 20℃; for 16h; Inert atmosphere; | 88% |
3-Benzyloxyphenol
5-{3-[3-(benzyloxy)phenoxy]azetidine-1-yl}-5-methyl-2,2-diphenylhexanenitrile
Conditions | Yield |
---|---|
Stage #1: 1-(5-cyano-2-methyl-5,5-diphenylpentan-2-yl)azetidin-3-yl methanesulfonate monohydrochloride With caesium carbonate In acetonitrile at 20℃; Stage #2: 3-Benzyloxyphenol In acetonitrile at 75 - 80℃; for 12h; | 87% |
3-Benzyloxyphenol
2-(2-(2-(4-tritylphenoxy)ethoxy)ethoxy)ethyl 4-methylbenzenesulfonate
1-(2-{2-[2-(tritylphenoxy)ethoxy]ethoxy}ethoxy)-3-(benzyloxy)benzene
Conditions | Yield |
---|---|
With potassium carbonate; lithium bromide In acetonitrile for 96h; Heating; | 84% |
3-Benzyloxyphenol
4-((4-(heptyloxy)benzoyl)oxy)benzoic acid
4-((3-(benzyloxy)phenoxy)carbonyl)phenyl 4-(heptyloxy)benzoate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane for 12h; | 84% |
2-[(6-bromohexyl)oxy]tetrahydro-2H-pyran
3-Benzyloxyphenol
Conditions | Yield |
---|---|
With caesium carbonate In acetone at 70℃; | 83% |
With caesium carbonate In acetone at 70℃; | 83% |
3-Benzyloxyphenol
diphenyl 2,3,4,6-tetra-O-benzyl-α-D-mannopyranoside phosphate
Conditions | Yield |
---|---|
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at 20℃; for 1h; | 82% |
With trimethylsilyl trifluoromethanesulfonate In dichloromethane at 0 - 20℃; for 1h; | 82% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 50℃; for 24h; | 82% |
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