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Qingdao Beluga Import and Export Co., LTD

ascofuranone CAS:38462-04-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediate

ascofuranone CAS:38462-04-3

Cas:38462-04-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

ASCOFURANONE

Cas:38462-04-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

ASCOFURANONE

Cas:38462-04-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Ascofuranone

Cas:38462-04-3

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

ascofuranone

Cas:38462-04-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

ASCOFURANONE

Cas:38462-04-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

ascofuranone

Cas:38462-04-3

Min.Order:0

Negotiable

Type:Manufacturers

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

ASCOFURANONE

Cas:38462-04-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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DB BIOTECH CO., LTD

best seller Application:API

ascofuranone

Cas:38462-04-3

Min.Order:0

Negotiable

Type:Trading Company

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Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

ascofuranone

Cas:38462-04-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

38462-04-3

Cas:38462-04-3

Min.Order:0

Negotiable

Type:Trading Company

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Hebei Muhuang Technology Co., Ltd

best seller Application:API

ascofuranone

Cas:38462-04-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

ascofuranone

Cas:38462-04-3

Min.Order:0

Negotiable

Type:Trading Company

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HuBei Ipure Biotech CO.,ltd

HuBei ipure is a diversified product production and operation enterprise, with API, pharma intermediates, and other fine chemicals as well as R&D and pigments development and sales as one of the large enterprises, with more than 130 acres of pl

Ascofuranone Cas No: 38462-04-3

Cas:38462-04-3

Min.Order:1 Gram

FOB Price: $1.0

Type:Trading Company

inquiry

Chengdu Push Bio-technology Co., Ltd

Chengdu Push Bio-technology Co., Ltd. provides more than 4,000 natural monomeric substances, including approximately 6,000 products at different grades, specifications and purities. We have specialized in the R&D of medicinally active ingredients sta

Ascofuranone

Cas:38462-04-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Zhejiang Huida Biotech Co., Ltd

High quality Short lead time Cost competitiveness Application:Antiviral

Ascofuranone

Cas:38462-04-3

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

inquiry

Hebei Ruishun Trade Co.,Ltd

Supply top quality products with a reasonable price Application:api

38462-04-3

Cas:38462-04-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

(1''S,4''S)-(-)-ascofuranol
51759-79-6

(1''S,4''S)-(-)-ascofuranol

Ascofuranone
38462-04-3

Ascofuranone

Conditions
ConditionsYield
With pyridinium chlorochromate In dichloromethane for 3h; Ambient temperature;22.2%
(2E,6E,1'S,4'S)-(+)-7-(4'-hydroxy-3',3'-dimethyl-2'-oxacyclopentyl)-3,7-dimethyl-2,6-heptadienyl acetate
99529-56-3

(2E,6E,1'S,4'S)-(+)-7-(4'-hydroxy-3',3'-dimethyl-2'-oxacyclopentyl)-3,7-dimethyl-2,6-heptadienyl acetate

Ascofuranone
38462-04-3

Ascofuranone

Conditions
ConditionsYield
Multi-step reaction with 9 steps
1: imidazole / dimethylformamide / 6 h / Ambient temperature
2: 92.9 percent / K2CO3 / methanol; H2O / 48 h / Ambient temperature
3: 1.26 g / n-BuLi, Ph3CH, p-TsCl, LiCl / diethyl ether; hexamethylphosphoric acid triamide; hexane / 0.42 h / 0 °C
4: n-BuLi, HMPA / tetrahydrofuran; hexane / 0.75 h / -70 °C
5: 50.2 percent / CaCO3, NCS / H2O; dimethylformamide / Ambient temperature
6: 57 percent / DBU / tetrahydrofuran / 6 h / Heating
7: 1) EtMgBr / 1) ether, room temp., 1 h. 10 min.; 2) ether evaporated; 100 degC, 10 min.
8: 71 percent / HF / acetonitrile; H2O / 1 h / Ambient temperature
9: 22.2 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature
View Scheme
(2E,6E,1'S*,4'S*)-7-(4'-hydroxy-3',3'-dimethyl-2'-oxacyclopentyl)-3,7-dimethyl-2,6-heptadienyl acetate
99477-55-1, 99529-54-1, 99529-56-3, 99529-57-4

(2E,6E,1'S*,4'S*)-7-(4'-hydroxy-3',3'-dimethyl-2'-oxacyclopentyl)-3,7-dimethyl-2,6-heptadienyl acetate

Ascofuranone
38462-04-3

Ascofuranone

Conditions
ConditionsYield
Multi-step reaction with 11 steps
1: 5.14 g / 14 h / 80 °C
2: 76.3 percent / Et3N, HSiCl3 / benzene / 96 h / Ambient temperature
3: imidazole / dimethylformamide / 6 h / Ambient temperature
4: 92.9 percent / K2CO3 / methanol; H2O / 48 h / Ambient temperature
5: 1.26 g / n-BuLi, Ph3CH, p-TsCl, LiCl / diethyl ether; hexamethylphosphoric acid triamide; hexane / 0.42 h / 0 °C
6: n-BuLi, HMPA / tetrahydrofuran; hexane / 0.75 h / -70 °C
7: 50.2 percent / CaCO3, NCS / H2O; dimethylformamide / Ambient temperature
8: 57 percent / DBU / tetrahydrofuran / 6 h / Heating
9: 1) EtMgBr / 1) ether, room temp., 1 h. 10 min.; 2) ether evaporated; 100 degC, 10 min.
10: 71 percent / HF / acetonitrile; H2O / 1 h / Ambient temperature
11: 22.2 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature
View Scheme
(2E,6E,1'S,4'S)-(+)-7-(4'-t-butyldimethylsilyloxy-3',3'-dimethyl-2'-oxacyclopentyl)-3,7-dimethyl-2,6-heptadien-1-ol
99477-58-4

(2E,6E,1'S,4'S)-(+)-7-(4'-t-butyldimethylsilyloxy-3',3'-dimethyl-2'-oxacyclopentyl)-3,7-dimethyl-2,6-heptadien-1-ol

Ascofuranone
38462-04-3

Ascofuranone

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: 1.26 g / n-BuLi, Ph3CH, p-TsCl, LiCl / diethyl ether; hexamethylphosphoric acid triamide; hexane / 0.42 h / 0 °C
2: n-BuLi, HMPA / tetrahydrofuran; hexane / 0.75 h / -70 °C
3: 50.2 percent / CaCO3, NCS / H2O; dimethylformamide / Ambient temperature
4: 57 percent / DBU / tetrahydrofuran / 6 h / Heating
5: 1) EtMgBr / 1) ether, room temp., 1 h. 10 min.; 2) ether evaporated; 100 degC, 10 min.
6: 71 percent / HF / acetonitrile; H2O / 1 h / Ambient temperature
7: 22.2 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature
View Scheme
(2E,6E,1'S,4'S)-7-(4'-t-butyldimethylsilyloxy-3',3'-dimethyl-2'-oxacyclopentyl)-3,7-dimethyl-2,6-heptadienyl chloride
99477-59-5

(2E,6E,1'S,4'S)-7-(4'-t-butyldimethylsilyloxy-3',3'-dimethyl-2'-oxacyclopentyl)-3,7-dimethyl-2,6-heptadienyl chloride

Ascofuranone
38462-04-3

Ascofuranone

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: n-BuLi, HMPA / tetrahydrofuran; hexane / 0.75 h / -70 °C
2: 50.2 percent / CaCO3, NCS / H2O; dimethylformamide / Ambient temperature
3: 57 percent / DBU / tetrahydrofuran / 6 h / Heating
4: 1) EtMgBr / 1) ether, room temp., 1 h. 10 min.; 2) ether evaporated; 100 degC, 10 min.
5: 71 percent / HF / acetonitrile; H2O / 1 h / Ambient temperature
6: 22.2 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature
View Scheme
(2E,6E,1'S,4'S)-(+)-7-(4'-t-butyldimethylsilyloxy-3',3'-dimethyl-2'-oxacyclopentyl)-3,7-dimethyl-2,6-heptadienyl acetate
99477-57-3, 99529-58-5

(2E,6E,1'S,4'S)-(+)-7-(4'-t-butyldimethylsilyloxy-3',3'-dimethyl-2'-oxacyclopentyl)-3,7-dimethyl-2,6-heptadienyl acetate

Ascofuranone
38462-04-3

Ascofuranone

Conditions
ConditionsYield
Multi-step reaction with 8 steps
1: 92.9 percent / K2CO3 / methanol; H2O / 48 h / Ambient temperature
2: 1.26 g / n-BuLi, Ph3CH, p-TsCl, LiCl / diethyl ether; hexamethylphosphoric acid triamide; hexane / 0.42 h / 0 °C
3: n-BuLi, HMPA / tetrahydrofuran; hexane / 0.75 h / -70 °C
4: 50.2 percent / CaCO3, NCS / H2O; dimethylformamide / Ambient temperature
5: 57 percent / DBU / tetrahydrofuran / 6 h / Heating
6: 1) EtMgBr / 1) ether, room temp., 1 h. 10 min.; 2) ether evaporated; 100 degC, 10 min.
7: 71 percent / HF / acetonitrile; H2O / 1 h / Ambient temperature
8: 22.2 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature
View Scheme
(2'E,6'E,1''S,4''S)-(+)-3-<7'-(4''-t-butyldimethylsilyloxy-3'',3''-dimethyl-2''-oxacyclopentyl)-3',7'-dimethyl-2',6'-heptadienyl>-2,4-dimethoxy-6-methyl-1,4-cyclohexadiene
99477-60-8

(2'E,6'E,1''S,4''S)-(+)-3-<7'-(4''-t-butyldimethylsilyloxy-3'',3''-dimethyl-2''-oxacyclopentyl)-3',7'-dimethyl-2',6'-heptadienyl>-2,4-dimethoxy-6-methyl-1,4-cyclohexadiene

Ascofuranone
38462-04-3

Ascofuranone

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 50.2 percent / CaCO3, NCS / H2O; dimethylformamide / Ambient temperature
2: 57 percent / DBU / tetrahydrofuran / 6 h / Heating
3: 1) EtMgBr / 1) ether, room temp., 1 h. 10 min.; 2) ether evaporated; 100 degC, 10 min.
4: 71 percent / HF / acetonitrile; H2O / 1 h / Ambient temperature
5: 22.2 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature
View Scheme
(2'E,6'E,1''S,4''S)-4-chloro-2-<7'-(4''-t-butyldimethylsilyloxy-3'',3''-dimethyl-2''-oxacyclopentyl)-3',7'-dimethyl-2',6'-heptadienyl>orcinol
99477-62-0

(2'E,6'E,1''S,4''S)-4-chloro-2-<7'-(4''-t-butyldimethylsilyloxy-3'',3''-dimethyl-2''-oxacyclopentyl)-3',7'-dimethyl-2',6'-heptadienyl>orcinol

Ascofuranone
38462-04-3

Ascofuranone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1) EtMgBr / 1) ether, room temp., 1 h. 10 min.; 2) ether evaporated; 100 degC, 10 min.
2: 71 percent / HF / acetonitrile; H2O / 1 h / Ambient temperature
3: 22.2 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature
View Scheme
(2'E,6'E,1''S,4''S)-3-<7'-(4''-t-butyldimethylsilyloxy-3'',3''-dimethyl-2''-oxacyclopentyl)-3',7'-dimethyl-2',6'-heptadienyl>-1,5-dichloro-6-methyl-2,4-cyclohexanedione
99477-61-9

(2'E,6'E,1''S,4''S)-3-<7'-(4''-t-butyldimethylsilyloxy-3'',3''-dimethyl-2''-oxacyclopentyl)-3',7'-dimethyl-2',6'-heptadienyl>-1,5-dichloro-6-methyl-2,4-cyclohexanedione

Ascofuranone
38462-04-3

Ascofuranone

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 57 percent / DBU / tetrahydrofuran / 6 h / Heating
2: 1) EtMgBr / 1) ether, room temp., 1 h. 10 min.; 2) ether evaporated; 100 degC, 10 min.
3: 71 percent / HF / acetonitrile; H2O / 1 h / Ambient temperature
4: 22.2 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature
View Scheme
(2'E,6'E,1''S,4''S)-5-chloro-2,4-dihydroxy-6-methyl-3-<7'-(4''-t-butyldimethylsilyloxy-3'',3''-dimethyl-2''-oxacyclopentyl)-3',7'-dimethyl-2',6'-heptadienyl>benzaldehyde
99477-63-1

(2'E,6'E,1''S,4''S)-5-chloro-2,4-dihydroxy-6-methyl-3-<7'-(4''-t-butyldimethylsilyloxy-3'',3''-dimethyl-2''-oxacyclopentyl)-3',7'-dimethyl-2',6'-heptadienyl>benzaldehyde

Ascofuranone
38462-04-3

Ascofuranone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 71 percent / HF / acetonitrile; H2O / 1 h / Ambient temperature
2: 22.2 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature
View Scheme
Acetic acid (2E,6E)-7-[(2S,4S)-5,5-dimethyl-4-((R)-1-naphthalen-1-yl-ethylcarbamoyloxy)-tetrahydro-furan-2-yl]-3-methyl-octa-2,6-dienyl ester
99477-56-2

Acetic acid (2E,6E)-7-[(2S,4S)-5,5-dimethyl-4-((R)-1-naphthalen-1-yl-ethylcarbamoyloxy)-tetrahydro-furan-2-yl]-3-methyl-octa-2,6-dienyl ester

Ascofuranone
38462-04-3

Ascofuranone

Conditions
ConditionsYield
Multi-step reaction with 10 steps
1: 76.3 percent / Et3N, HSiCl3 / benzene / 96 h / Ambient temperature
2: imidazole / dimethylformamide / 6 h / Ambient temperature
3: 92.9 percent / K2CO3 / methanol; H2O / 48 h / Ambient temperature
4: 1.26 g / n-BuLi, Ph3CH, p-TsCl, LiCl / diethyl ether; hexamethylphosphoric acid triamide; hexane / 0.42 h / 0 °C
5: n-BuLi, HMPA / tetrahydrofuran; hexane / 0.75 h / -70 °C
6: 50.2 percent / CaCO3, NCS / H2O; dimethylformamide / Ambient temperature
7: 57 percent / DBU / tetrahydrofuran / 6 h / Heating
8: 1) EtMgBr / 1) ether, room temp., 1 h. 10 min.; 2) ether evaporated; 100 degC, 10 min.
9: 71 percent / HF / acetonitrile; H2O / 1 h / Ambient temperature
10: 22.2 percent / pyridinium chlorochromate / CH2Cl2 / 3 h / Ambient temperature
View Scheme
acetic anhydride
108-24-7

acetic anhydride

Ascofuranone
38462-04-3

Ascofuranone

2,4-O-di-acetylascofuranone

2,4-O-di-acetylascofuranone

Conditions
ConditionsYield
With pyridine at 20℃; Product distribution / selectivity;100%
Ascofuranone
38462-04-3

Ascofuranone

dimethyl sulfate
77-78-1

dimethyl sulfate

4-O-Methyl-ascofuranone

4-O-Methyl-ascofuranone

Conditions
ConditionsYield
With potassium carbonate In acetone for 1h; Heating / reflux;93%
ethyl bromoacetate
105-36-2

ethyl bromoacetate

Ascofuranone
38462-04-3

Ascofuranone

ethyl {2-chloro-6-[(2E,6E)-7-((S)-2,2-dimethyl-3-oxotetrahydrofuran-5-yl)-3-methyl-2,6-octadienyl]-4-formyl-5-hydroxy-3-methylphenoxy}acetate

ethyl {2-chloro-6-[(2E,6E)-7-((S)-2,2-dimethyl-3-oxotetrahydrofuran-5-yl)-3-methyl-2,6-octadienyl]-4-formyl-5-hydroxy-3-methylphenoxy}acetate

Conditions
ConditionsYield
Stage #1: Ascofuranone With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.166667h;
Stage #2: ethyl bromoacetate In N,N-dimethyl-formamide at 40℃; for 5.5h;
88%
Ascofuranone
38462-04-3

Ascofuranone

methyl iodide
74-88-4

methyl iodide

4-O-Methyl-ascofuranone

4-O-Methyl-ascofuranone

Conditions
ConditionsYield
With potassium carbonate In acetone for 1h; Heating;87%
acetic anhydride
108-24-7

acetic anhydride

Ascofuranone
38462-04-3

Ascofuranone

4-O-Acetyl-ascofuranone
60217-09-6

4-O-Acetyl-ascofuranone

Conditions
ConditionsYield
With pyridine at 20℃;68%
pyridine-3-carbonyl chloride hydrochloride
20260-53-1

pyridine-3-carbonyl chloride hydrochloride

Ascofuranone
38462-04-3

Ascofuranone

4-O-Nicotinoyl-ascofuranone

4-O-Nicotinoyl-ascofuranone

Conditions
ConditionsYield
With pyridine at 20℃;67%
isonicotinoyl chloride hydrochloride
39178-35-3

isonicotinoyl chloride hydrochloride

Ascofuranone
38462-04-3

Ascofuranone

4-O-Isonicotinoyl-ascofuranone

4-O-Isonicotinoyl-ascofuranone

Conditions
ConditionsYield
In pyridine at 20℃; for 1h;54%
Stage #1: isonicotinoyl chloride hydrochloride; Ascofuranone With pyridine at 20℃; for 1h;
Stage #2: With water at 20℃; for 0.5h;
54%
glutaric anhydride,
108-55-4

glutaric anhydride,

Ascofuranone
38462-04-3

Ascofuranone

4-O-(4-Carboxybutanoyl)ascofuranone

4-O-(4-Carboxybutanoyl)ascofuranone

Conditions
ConditionsYield
With pyridine; dmap at 50℃;32%
Ascofuranone
38462-04-3

Ascofuranone

3-chloro-4,6-dihydroxy-2-methyl-5-[3-methyl-7-(tetrahydro-5,5-dimethyl-4-oxo-2-furanyl)octyl]-benzaldehyde
1027952-60-8

3-chloro-4,6-dihydroxy-2-methyl-5-[3-methyl-7-(tetrahydro-5,5-dimethyl-4-oxo-2-furanyl)octyl]-benzaldehyde

Conditions
ConditionsYield
With hydrogen; 5%-palladium/activated carbon In ethanol at 0℃; for 3h;25%
Ascofuranone
38462-04-3

Ascofuranone

Dehydroascofuranone

Dehydroascofuranone

Conditions
ConditionsYield
With sodium hydroxide; silver nitrate In 1,4-dioxane at 20℃; for 3h;24%
With sodium hydroxide; silver nitrate In 1,4-dioxane; water at 20℃; for 3h;24%
Ascofuranone
38462-04-3

Ascofuranone

5-[(E,E)-7-(3-chloro-2,6-dihydroxy-5-hydroxyiminomethyl-4-methylphenyl)-1,5-dimethyl-1,5-heptadienyl]-4,5-dihydro-2,2-dimethyl-3(2H)-furanone

5-[(E,E)-7-(3-chloro-2,6-dihydroxy-5-hydroxyiminomethyl-4-methylphenyl)-1,5-dimethyl-1,5-heptadienyl]-4,5-dihydro-2,2-dimethyl-3(2H)-furanone

Conditions
ConditionsYield
With pyridine; hydroxylamine hydrochloride at 20 - 25℃; for 3.5h;20%
Ascofuranone
38462-04-3

Ascofuranone

2-O-Methyl-ascofuranone

2-O-Methyl-ascofuranone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 68 percent / pyridine / 20 °C
2: 24 percent / K2CO3 / acetone / 2 h / Heating
3: 90 percent / aq. NaOH / methanol / 4 h / 20 °C
View Scheme
Ascofuranone
38462-04-3

Ascofuranone

4-O-Acetyl-2-O-methyl-ascofuranone
290361-56-7

4-O-Acetyl-2-O-methyl-ascofuranone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 68 percent / pyridine / 20 °C
2: 24 percent / K2CO3 / acetone / 2 h / Heating
View Scheme
Ascofuranone
38462-04-3

Ascofuranone

4-O-Carboxymethyl-ascofuranone

4-O-Carboxymethyl-ascofuranone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: NaH / dimethylformamide / 0.17 h / 20 °C
1.2: 88 percent / dimethylformamide / 5.5 h / 40 °C
2.1: 91 percent / aq. K2CO3 / methanol / 2 h / 20 °C
View Scheme

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