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Cas:4459-18-1
Min.Order:1 Gram
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Cas:4459-18-1
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Cas:4459-18-1
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
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Cas:4459-18-1
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Type:Manufacturers
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:4459-18-1
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Type:Lab/Research institutions
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Cas:4459-18-1
Min.Order:0
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Type:Trading Company
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
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Cas:4459-18-1
Min.Order:10 Milligram
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Cas:4459-18-1
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryFINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the Iodoperfluoro-tert-butane, CAS:4459-18-1 with the most competitive price and the best
Iodoperfluoro-tert-butane Application:2025666
Cas:4459-18-1
Min.Order:1 Gram
FOB Price: $500.0
Type:Trading Company
inquiry1,1,1,3,3,3-hexafluoro-2-iodo-2-(trifluoromethyl)propane CASNo.:4459-18-1 Storage:as prescribe by the manufaurer Package:pack as requested
Cas:4459-18-1
Min.Order:100 Kilogram
Negotiable
Type:Trading Company
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Cas:4459-18-1
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inquiry2-bromo-1,1,1,3,3,3-hexafluoro-2-trifluoromethyl-propane
A
1,1,1,3,3,3-hexafluoro-2-trifluoromethyl-propane
B
perfluoro-tert-butyl iodide
Conditions | Yield |
---|---|
With sodium iodide In acetonitrile for 5h; Heating; | A 75.7% B 5.3% |
2-chlorocarbonyloxy-1,1,1,3,3,3-hexafluoro-2-trifluoromethyl-propane
perfluoro-tert-butyl iodide
Conditions | Yield |
---|---|
With potassium iodide at 150 - 180℃; for 3h; | 30.8% |
iodotrifluoromethane
3,3-bis(trifluoromethyl)diazirine
perfluoro-tert-butyl iodide
Conditions | Yield |
---|---|
at 150 - 155℃; for 10h; | 9.8% |
Conditions | Yield |
---|---|
With potassium fluoride; iodine; nitrobenzene |
1,1,1,3,3,3-hexafluoro-2-nitroso-2-trifluoromethyl-propane
perfluoro-tert-butyl iodide
Conditions | Yield |
---|---|
With iodine |
perfluoropropylene
iodotrifluoromethane
A
1,1,1,2,2,3,3-heptafluoro-3-iodo-propane
B
perfluoroisobutylene
C
perfluoroisopropyl iodide
D
2-trifluoromethyl-perfluoropropyl iodide
E
perfluoro-tert-butyl iodide
Conditions | Yield |
---|---|
at 360℃; Product distribution; nickel reactor; other temperatures, influence of reactor material; |
perfluoropropylene
iodotrifluoromethane
A
perfluoroisopropyl iodide
B
2-trifluoromethyl-perfluoropropyl iodide
C
perfluoro-tert-butyl iodide
Conditions | Yield |
---|---|
at 360℃; Yield given. Further byproducts given. Yields of byproduct given; |
2-bromo-1,1,1,3,3,3-hexafluoro-2-trifluoromethyl-propane
A
iodotrifluoromethane
B
perfluoro-tert-butyl iodide
Conditions | Yield |
---|---|
With iodine Product distribution; Irradiation; multiple-photon IR laser excitation; different laser frequency and energy fluence; | |
With iodine Irradiation; Yield given. Yields of byproduct given; |
benzenediazonium hexafluorophosphate
A
2-phenylazo-2-trifluoromethylperfluoropropane
B
perfluoro-tert-butyl iodide
Conditions | Yield |
---|---|
In tetrahydrofuran at 25℃; |
methyl trifluoromethanesulfonate
A
perfluoro-tert-butyl iodide
B
1,1,1,3,3,3-hexafluoro-2-methyl-2-trifluoromethyl-propane
Conditions | Yield |
---|---|
In dichloromethane at 25℃; |
1,1,1,2,3,5,5,5-Octafluoro-2,3,4,4-tetrakis-trifluoromethyl-pentane
A
Perfluoro-2-iodo-3-methylbutane
B
perfluoroisopropyl iodide
C
perfluoro-tert-butyl iodide
Conditions | Yield |
---|---|
With iodine at 161℃; for 48h; | |
With iodine at 201℃; for 48h; | |
With iodine at 201℃; for 48h; Rate constant; Thermodynamic data; other temp., activation energy; |
Conditions | Yield |
---|---|
With hexaethylphosphoric triamide In dichloromethane byproducts: P(NEt2)3ClI; a soln. of ClGeEt3 and t-C4F9I in CH2Cl2 is cooled to -40 to -50°C with stirring in Ar, then a soln. of P(NEt2)3 in CH2Cl2 is added, stirred for 1-1.5 h, warmed to room temp. within 2-3 h; extd. (pentane), the extract is washed, dried, distd.; | 87% |
Cp*Rh(ethylene)2
perfluoro-tert-butyl iodide
trimethylphosphane
[(η5-pentamethylcyclopentadienyl)RhI(CH2CH2C(CF3)3)(trimethylphosphine)]
Conditions | Yield |
---|---|
In toluene byproducts: CH2CH2; High Pressure; (N2, Schlenk technique); heating mixt. of rhodium compd. and phosphine deriv. in toluene at 120°C for 24 h, cooling to room temp., addn. of perfluoroisopropyl iodide, stirring for 40 min; evapn. in vac., extn. (n-pentane), evapn., elem. anal.; | 80% |
With CH3O(2)H In (2)H8-toluene byproducts: (CF3)2CF(2)H; High Pressure; (N2, Schlenk technique); heating toluene-d8 soln. of rhodium compd. and phosphine deriv. at 120°c for 24 h, treatment with tert-perfluorobutyl iodide and methanol-d1; |
Conditions | Yield |
---|---|
Stage #1: perfluoro-tert-butyl iodide; C12H20I2Ir In pentane at 20℃; for 18h; Inert atmosphere; Schlenk technique; Stage #2: triphenylphosphine In tetrahydrofuran at 20℃; for 3h; Inert atmosphere; Schlenk technique; | 77.6% |
Conditions | Yield |
---|---|
In pentane at 20℃; for 22h; Inert atmosphere; Schlenk technique; | 64.2% |
Conditions | Yield |
---|---|
Stage #1: C12H20I2Rh; triphenylphosphine In toluene at 120℃; for 4h; Inert atmosphere; Schlenk technique; Stage #2: perfluoro-tert-butyl iodide In toluene at 20℃; for 1.5h; Inert atmosphere; Schlenk technique; | 60.3% |
Conditions | Yield |
---|---|
In tetrahydrofuran; benzene under N2; adding soln. of IC(CF3)3 in benzene to THF soln. of WCp2(C2H4), stirring for 15 min; removal of solvent in vacuo, dissolving residue in CH2Cl2, filtration, redn. of solvent vol., addn. of hexane; elem. anal.; | 60% |
perfluoro-tert-butyl iodide
Mo(C5H5)2[CH2CH2C(CF3)3]I
Conditions | Yield |
---|---|
In tetrahydrofuran; benzene under N2; adding soln. of IC(CF3)3 in benzene to THF soln. of MoCp2(C2H4), stirring for 0.5 h; removal of solvent, recrystn. from CH2Cl2/hexane; elem. anal.; | 54% |
Cp*Rh(ethylene)2
perfluoro-tert-butyl iodide
trimethylphosphane
B
[(η5-pentamethylcyclopentadienyl)RhI(CH2CH2C(CF3)3)(trimethylphosphine)]
Conditions | Yield |
---|---|
In toluene byproducts: CH2CH2; (N2, Schlenk technique); addn. of tert-perfluorobutyl iodide to rhodium compd. in pentane, stirring for 20 h at room temp., evapn., dissolving in toluene, addn. of phosphine deriv., stirring for 3 h; evapn., extn. (n-pentane), evapn., chromy. (silica gel, diethyl ether/n-hexane (1:1)), evapn., elem. anal.; | A n/a B 52% |
perfluoro-tert-butyl iodide
N-{2-(1,3-dioxoisoindolin-2-yl)acryloyl}-(1R,2S,4S)-bornane-10,2-sultam
N-{(R)-2-(1,3-dioxoisoindolin-2-yl)-3-perfluoro-tert-butylpropanoyl}-(1R,2S,4S)-bornane-10,2-sultam
Conditions | Yield |
---|---|
With tris-(trimethylsilyl)silane; sodium thiosulfate In dichloromethane; water at 20℃; UV-irradiation; Sealed tube; stereoselective reaction; | 51% |
perfluoro-tert-butyl iodide
(trimethylsilyl)diphenylphosphine
Ph2P(t-C4F9)
Conditions | Yield |
---|---|
In hexane at -30 - 20℃; Inert atmosphere; | 30% |
In chloroform-d1 at 20℃; for 0.5h; Inert atmosphere; | 30 %Spectr. |
diazomethane
perfluoro-tert-butyl iodide
1,1,1-trifluoro-4-iodo-2,2-bis-trifluoromethyl-butane
Conditions | Yield |
---|---|
In diethyl ether |
ethene
perfluoro-tert-butyl iodide
1,1,1-trifluoro-4-iodo-2,2-bis-trifluoromethyl-butane
Conditions | Yield |
---|---|
With dicyclohexyl peroxydicarbonate |
Conditions | Yield |
---|---|
With diiron nonacarbonyl In hexane |
1,4-dioxane-2,3-dione
perfluoro-tert-butyl iodide
3-perfluoro-tert-butyl-3-hydroxy-1,4-dioxan-2-one
Conditions | Yield |
---|---|
With magnesium; ethylene dibromide 1.) ether, -25 deg C, 1.5 h, 2.) from -12 deg C to RT; Yield given. Multistep reaction; |
perfluoro-tert-butyl iodide
fullerene-C60
Conditions | Yield |
---|---|
In various solvent(s) at -48.1℃; |
perfluoro-tert-butyl iodide
tris(dimethylamino)sulfonium1,1,1,3,3,3-hexafluoro-2-(trifluoromethyl)-2-propanide
Conditions | Yield |
---|---|
In tetrahydrofuran for 0.5h; | 720 mg |
Conditions | Yield |
---|---|
at 426.9 - 626.9℃; |
perfluoro-tert-butyl iodide
oxalic acid diethyl ester
ethyl 4,4,4-trifluoro-3,3-bis(trifluoromethyl)-2-oxobutyrate
Conditions | Yield |
---|---|
With magnesium; ethylene dibromide 1.) ether, -25 deg C, 1.5 h, 2.) from -12 deg C to RT; Yield given. Multistep reaction; |
perfluoro-tert-butyl iodide
acetone
4,4,4-trifluoro-2-methyl-3,3-bis(trifluoromethyl)-2-butanol
Conditions | Yield |
---|---|
With magnesium; ethylene dibromide 1.) ether, -25 deg C, 1.5 h, 2.) from -12 deg C to RT; Yield given. Multistep reaction; |
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