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Mesembrine CAS: 468-53-1 Specification Product Name: Mesembrine Synonyms: Mesembrine;(3aR,7aR)-3a-(3,4-dimethoxyphenyl)-1-methyl-2,3,4,5,7,7a-hexahydroindol-6-one CAS: 468-53-1 MF: C17H23NO3
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
We product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Specification : (3aR,7aR)-3a-(3,4-dimethoxyphenyl
Appearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:By Sea/Air/Courier Port:Qingdao
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inquiryKanna extract,Mesembrine Product Name: Kanna Extract, Lampranthus Spectabilis Extract Latin Name: Sceletium tortuosum Part Used: Whole Herb Appearance: Brown Yellow Powder Specification: 10:1, 20:1,98% Mesembrine Mesh size: 100% pass 80 Mesh
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inquirySuperior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediates Tr
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Cas:468-53-1
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GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:468-53-1
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inquiryR & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
Cas:468-53-1
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inquiry1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane at 0 - 20℃; for 1.33333h; | 81% |
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
With ammonium hydroxide; lithium In tetrahydrofuran; tert-butyl alcohol for 0.5h; Birch Reduction; Inert atmosphere; | 77% |
With ammonia; lithium In tetrahydrofuran; tert-butyl alcohol at -78℃; for 0.75h; | 77% |
(3aR,8bS)-3a-(3,4-dimethoxyphenyl)-1,6-dimethyl-1,2,3,3a,4,5,6,8b-octahydro-8H-isoxazolo[3,4-g]indol-8-one
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
With hexacarbonyl molybdenum In water; acetonitrile for 12h; Heating; | 75% |
(3aR,6S,7aR)-3a-(3,4-dimethoxyphenyl)-1-methyloctahydro-1H-indol-6-ol
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
With dipyridinium dichromate In dichloromethane at 20℃; for 2h; Inert atmosphere; | 48% |
(R)-2-(3,4-Dimethoxy-phenyl)-2-(2-methylamino-ethyl)-5-oxo-hexanal
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
With sodium hydroxide Ambient temperature; |
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
With acid Yield given; |
[(S)-1-(3,4-Dimethoxy-phenyl)-3-((S)-2-methoxymethyl-pyrrolidine-1-carbonyl)-4-oxo-cyclohex-2-enyl]-acetaldehyde
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: triethylamine / 1,2-dichloro-ethane / 0.08 h / 20 °C 2: 190 mg / NaBH3CN / 1,2-dichloro-ethane / 6 h / 20 °C 3: 60 percent / ethanol / 6 h / Heating 4: 75 percent / Mo(CO)6 / acetonitrile; H2O / 12 h / Heating View Scheme |
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 190 mg / NaBH3CN / 1,2-dichloro-ethane / 6 h / 20 °C 2: 60 percent / ethanol / 6 h / Heating 3: 75 percent / Mo(CO)6 / acetonitrile; H2O / 12 h / Heating View Scheme |
((R)-1-allyl-5-(3,4-dimethoxyphenyl)-2-methoxycyclohexa-2,5-dienyl)((S)-2-(methoxymethyl)pyrrolidin-1-yl)methanone
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1.1: 95 percent / HCl / methanol / 15 h / 20 °C 2.1: 80 percent / 1,2-dichloro-benzene / 10 h / Heating 3.1: O3; Sudan III / methanol / 0.03 h / -78 °C 3.2: dimethyl sulfide / methanol / 7 h / 20 °C 4.1: triethylamine / 1,2-dichloro-ethane / 0.08 h / 20 °C 5.1: 190 mg / NaBH3CN / 1,2-dichloro-ethane / 6 h / 20 °C 6.1: 60 percent / ethanol / 6 h / Heating 7.1: 75 percent / Mo(CO)6 / acetonitrile; H2O / 12 h / Heating View Scheme |
(S)-4-allyl-4-(3,4-dimethoxyphenyl)-2-((S)-2-(methoxymethyl)pyrrolidin-1-carbonyl)cyclohex-2-en-1-one
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: O3; Sudan III / methanol / 0.03 h / -78 °C 1.2: dimethyl sulfide / methanol / 7 h / 20 °C 2.1: triethylamine / 1,2-dichloro-ethane / 0.08 h / 20 °C 3.1: 190 mg / NaBH3CN / 1,2-dichloro-ethane / 6 h / 20 °C 4.1: 60 percent / ethanol / 6 h / Heating 5.1: 75 percent / Mo(CO)6 / acetonitrile; H2O / 12 h / Heating View Scheme |
(R)-2-allyl-4-(3,4-dimethoxyphenyl)-2-((S)-2-(methoxymethyl)pyrrolidin-1-carbonyl)cyclohex-3-en-1-one
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: 80 percent / 1,2-dichloro-benzene / 10 h / Heating 2.1: O3; Sudan III / methanol / 0.03 h / -78 °C 2.2: dimethyl sulfide / methanol / 7 h / 20 °C 3.1: triethylamine / 1,2-dichloro-ethane / 0.08 h / 20 °C 4.1: 190 mg / NaBH3CN / 1,2-dichloro-ethane / 6 h / 20 °C 5.1: 60 percent / ethanol / 6 h / Heating 6.1: 75 percent / Mo(CO)6 / acetonitrile; H2O / 12 h / Heating View Scheme |
(3aR,7aR)-3a-(3,4-dimethoxyphenyl)-7-((S)-2-(methoxymethyl)pyrrolidin-1-carbonyl)-1-methylhexahydro-1H-indol-6(2H)-one
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 60 percent / ethanol / 6 h / Heating 2: 75 percent / Mo(CO)6 / acetonitrile; H2O / 12 h / Heating View Scheme |
2-(but-3'-ynyl)-2-methyl-1,3-dioxolane
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 10 steps 1: EtMgBr / diethyl ether; toluene 2: 1.) n-BuLi, 2.) CuBr 3: 1.) Zn-Cu, 2.) Zn, AcOH / 1.) THF, 0 deg C, 2.) RT, 1 h 4: aq. AcOH / 2 h / 60 °C 5: K2CO3 / methanol 6: methanol 7: 83 percent / tetrahydrofuran / Heating 8: PTS 9: LiAlH4 / tetrahydrofuran 10: acid View Scheme |
(3aR,7aR)-3a-(3,4-Dimethoxy-phenyl)-1-methyl-hexahydro-indole-2,6-dione
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: PTS 2: LiAlH4 / tetrahydrofuran 3: acid View Scheme |
3'a-(3,4-dimethoxy-phenyl)-1'-methyl-hexahydro-spiro[[1,3]dioxolane-2,6'-indol]-2'-one
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: LiAlH4 / tetrahydrofuran 2: acid View Scheme |
2-Methyl-2-[4-((S)-toluene-4-sulfinyl)-but-3-ynyl]-[1,3]dioxolane
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 9 steps 1: 1.) n-BuLi, 2.) CuBr 2: 1.) Zn-Cu, 2.) Zn, AcOH / 1.) THF, 0 deg C, 2.) RT, 1 h 3: aq. AcOH / 2 h / 60 °C 4: K2CO3 / methanol 5: methanol 6: 83 percent / tetrahydrofuran / Heating 7: PTS 8: LiAlH4 / tetrahydrofuran 9: acid View Scheme |
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: methanol 2: 83 percent / tetrahydrofuran / Heating 3: PTS 4: LiAlH4 / tetrahydrofuran 5: acid View Scheme |
[(S)-1-(3,4-Dimethoxy-phenyl)-4-oxo-cyclohex-2-enyl]-acetic acid methyl ester
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 83 percent / tetrahydrofuran / Heating 2: PTS 3: LiAlH4 / tetrahydrofuran 4: acid View Scheme |
2-[(E)-3-(3,4-Dimethoxy-phenyl)-4-((R)-toluene-4-sulfinyl)-but-3-enyl]-2-methyl-[1,3]dioxolane
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 8 steps 1: 1.) Zn-Cu, 2.) Zn, AcOH / 1.) THF, 0 deg C, 2.) RT, 1 h 2: aq. AcOH / 2 h / 60 °C 3: K2CO3 / methanol 4: methanol 5: 83 percent / tetrahydrofuran / Heating 6: PTS 7: LiAlH4 / tetrahydrofuran 8: acid View Scheme |
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: K2CO3 / methanol 2: methanol 3: 83 percent / tetrahydrofuran / Heating 4: PTS 5: LiAlH4 / tetrahydrofuran 6: acid View Scheme |
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: aq. AcOH / 2 h / 60 °C 2: K2CO3 / methanol 3: methanol 4: 83 percent / tetrahydrofuran / Heating 5: PTS 6: LiAlH4 / tetrahydrofuran 7: acid View Scheme |
(3aR,5aR,8S,9aR)-3a-(3,4-Dimethoxy-phenyl)-8-isopropyl-1,5a-dimethyl-decahydro-oxazolo[3,2-a]pyrrolo[3,2-e]pyridine
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: Bu4NH2PO4 / ethanol 2: 4N NaOH / Ambient temperature View Scheme |
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: CNBH3(-) 2: LiAl(OEt)H3 / 1,2-dimethoxy-ethane; toluene / -20 °C 3: Bu4NH2PO4 / ethanol 4: 4N NaOH / Ambient temperature View Scheme |
(3S,6R,8aR)-6-(3,4-Dimethoxy-phenyl)-3-isopropyl-8a-methyl-6-(2-methylamino-ethyl)-hexahydro-oxazolo[3,2-a]pyridin-5-one
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: LiAl(OEt)H3 / 1,2-dimethoxy-ethane; toluene / -20 °C 2: Bu4NH2PO4 / ethanol 3: 4N NaOH / Ambient temperature View Scheme |
(S)-6-(3,4-Dimethoxy-phenyl)-3-isopropyl-8a-methyl-hexahydro-oxazolo[3,2-a]pyridin-5-one
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 90 percent / s-BuLi / tetrahydrofuran / -20 °C 2: OsO4, NaIO4 / diethyl ether; H2O / 8 h / 25 °C 3: CNBH3(-) 4: LiAl(OEt)H3 / 1,2-dimethoxy-ethane; toluene / -20 °C 5: Bu4NH2PO4 / ethanol 6: 4N NaOH / Ambient temperature View Scheme |
(3S,6R,8aR)-6-Allyl-6-(3,4-dimethoxy-phenyl)-3-isopropyl-8a-methyl-hexahydro-oxazolo[3,2-a]pyridin-5-one
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: OsO4, NaIO4 / diethyl ether; H2O / 8 h / 25 °C 2: CNBH3(-) 3: LiAl(OEt)H3 / 1,2-dimethoxy-ethane; toluene / -20 °C 4: Bu4NH2PO4 / ethanol 5: 4N NaOH / Ambient temperature View Scheme |
(3aR,6S,7aR)-3a-(3,4-dimethoxyphenyl)-1-methyloctahydro-1H-indol-6-amine
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Stage #1: (3aR,6S,7aR)-3a-(3,4-dimethoxyphenyl)-1-methyloctahydro-1H-indol-6-amine With 3,5-di-tert-butyl-o-benzoquinone In tetrahydrofuran; methanol for 1h; Stage #2: With oxalic acid In tetrahydrofuran; methanol; water Stage #3: With potassium hydroxide In tetrahydrofuran; methanol; water |
1-(3,4-Dimethoxy-phenyl)-1-methyl-iminomethyl-cyclopropan
methyl vinyl ketone
A
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Stage #1: 1-(3,4-Dimethoxy-phenyl)-1-methyl-iminomethyl-cyclopropan With chloro-trimethyl-silane; sodium iodide In DMF (N,N-dimethyl-formamide) at 90℃; for 3h; Stage #2: With hydrogenchloride In diethyl ether; dichloromethane Stage #3: methyl vinyl ketone With sodium hydroxide more than 3 stages; |
2-bromo-4,5-dimethoxy-N-((1R,5S)-2-methylene-5-(prop-1-en-2-yl)cyclohexyl)benzene sulfonamide
(3aR,7aR)-3a-(3,4-Dimethoxyphenyl)-1-methylhexahydro-1H-indol-6(2H)-one
Conditions | Yield |
---|---|
Multi-step reaction with 9 steps 1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C 1.2: 15 h / 0 - 20 °C 2.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 15 h / 40 °C 3.1: palladium diacetate; triphenylphosphine; potassium carbonate / N,N-dimethyl-formamide / 15 h / 110 °C / Inert atmosphere 4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 15 h / 20 °C 4.2: 15 h / 0 - 20 °C 5.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 19 h / 20 °C / 760.05 Torr 6.1: 3-chloro-benzenecarboperoxoic acid / chloroform-d1; water-d2 / 48 h / 20 °C 7.1: lithium; ammonia / tetrahydrofuran / -78 - 20 °C / Inert atmosphere 7.2: 4 h / 20 °C 8.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / Inert atmosphere; Reflux 9.1: dipyridinium dichromate / dichloromethane / 2 h / 20 °C / Inert atmosphere View Scheme |
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