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inquiry2,6,6-TRIMETHYL-1-CYCLOHEXENE-1-ACETALDEHYDE Basic information Product Name: 2,6,6-TRIMETHYL-1-CYCLOHEXENE-1-ACETALDEHYDE Synonyms: (2,6,6-Trimethyl-1-cyclohexen-1-
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryProduct Name: 2,6,6-TRIMETHYL-1-CYCLOHEXENE-1-ACETALDEHYDE CAS: 472-66-2 MF: C11H18O MW: 166.26 EINECS: 207-454-0 Mol File: 472-66-2.mol 2,6,6-TRIMETHYL-1-CYCLOHEXENE-1-ACETALDEHYDE Structure 2,6,6-TRIMETHYL-1-CYCLOHEXENE-1-ACETAL
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inquiry2,6,6-TRIMETHYL-1-CYCLOHEXENE-1-ACETALDEHYDE CAS:472-66-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in hig
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
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inquiry1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiry2-((E)-2-Methoxy-vinyl)-1,3,3-trimethyl-cyclohexene
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
With perchloric acid In tetrahydrofuran for 0.5h; Ambient temperature; | 94% |
2,2,6-trimethylcyclohexan-1-one
Bromoacetaldehyde diethyl acetal
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
Stage #1: Bromoacetaldehyde diethyl acetal With iodine; magnesium In tetrahydrofuran at 30 - 35℃; for 3.25h; Inert atmosphere; Stage #2: 2,2,6-trimethylcyclohexan-1-one In tetrahydrofuran at 10 - 15℃; for 3h; | 93.7% |
2-bromomethyl-1,3-dioxolane
2,2,6-trimethylcyclohexan-1-one
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
Stage #1: 2-bromomethyl-1,3-dioxolane With iodine; magnesium In 2-methyltetrahydrofuran at 30 - 40℃; for 3.25h; Inert atmosphere; Stage #2: 2,2,6-trimethylcyclohexan-1-one In 2-methyltetrahydrofuran at 10 - 15℃; for 3h; | 93.1% |
1-bromo-2,2-dimethoxyethane
2,2,6-trimethylcyclohexan-1-one
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
Stage #1: 1-bromo-2,2-dimethoxyethane With iodine; magnesium In tetrahydrofuran at 30 - 35℃; for 3.25h; Inert atmosphere; Stage #2: 2,2,6-trimethylcyclohexan-1-one In tetrahydrofuran at 10 - 15℃; for 3h; Temperature; Solvent; | 92.8% |
chloroacetaldehyde dimethyl acetal
2,2,6-trimethylcyclohexan-1-one
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
Stage #1: chloroacetaldehyde dimethyl acetal With iodine; magnesium In ethylene dibromide at 30 - 45℃; for 3.41667h; Inert atmosphere; Stage #2: 2,2,6-trimethylcyclohexan-1-one In ethylene dibromide at 10 - 15℃; for 3h; | 90.7% |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
With perchloric acid In diethyl ether for 5h; | 78.9% |
α--2,6,6,-trimethyl-1-cyclohexenemethanol
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
With formic acid for 0.166667h; Ambient temperature; | 75% |
1-ethoxyethynyl-2,2,6-trimethyl-cyclohexanol
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
With quinoline; Petroleum ether bei partieller Hydrierung an bleihaltigem Palladium, anschl. mit wss. H2SO4; |
2-acetoxyvinylidene-1,1,3-trimethyl-cyclohexane
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
With hydrogenchloride; water |
1-ethynyl-2,2,6-trimethyl-1-cyclohexanol
ethanethiol
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
In tetrachloromethane (i) AIBN, (irradiation), (ii) CF3CO2H; Multistep reaction; |
1-ethynyl-2,2,6-trimethyl-1-cyclohexanol
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
With vanadium tri-n-propoxide; benzoic acid; triphenylhydroxysilane In various solvent(s) at 140 - 150℃; | 81 % Turnov. |
1-ethynyl-2,2,6-trimethyl-1-cyclohexanol
A
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
B
α-(2,6,6-Trimethyl-1-cyclohexenyl)acetaldehyd
Conditions | Yield |
---|---|
tetrabutoxytitanium; p-Toluic acid; copper(l) chloride In 1,2-dichloro-benzene at 130℃; for 4h; Title compound not separated from byproducts; |
(E)-3-(2,6,6-trimethylcyclohex-1-enyl)acrylic acid
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
With hydrogenchloride; diphenyl phosphoryl azide; triethylamine 1) dioxan, RT, 1 h, 2.) reflux, 15 min; Yield given. Multistep reaction; |
2,2,6-trimethylcyclohexan-1-one
lithium acetylide-ethylenediamine complex
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
(i), (ii) Ph3SiOH, (iii) (Ph3SiO)3VO; Multistep reaction; |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
With methanol; water; sodium hydrogencarbonate |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
With ethanol; water; toluene-4-sulfonic acid |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 92 percent / NaOH, Br2 / H2O; dioxane / 4 h / Ambient temperature 2: 1.) Et3N, diphenyl phosphoryl azide, 2.) 0.5 N aq. HCl / 1) dioxan, RT, 1 h, 2.) reflux, 15 min View Scheme |
2,6,6-trimethylcyclohex-1-enecarbaldehyde
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: s-BuLi / 1.) THF, hexane, from -70 deg C to -25 deg C, 2.) -25 deg C, 0.5 h 2: 75 percent / 90percent aq. formic acid / 0.17 h / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 1: 61 percent / tetrahydrofuran / 1 h / Ambient temperature 2: 94 percent / 60percent perchloric acid / tetrahydrofuran / 0.5 h / Ambient temperature View Scheme |
acetic acid-(1-ethynyl-2,2,6-trimethyl-cyclohexyl ester)
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: zinc oxide; silicon oil / 200 °C / Erhitzen unter vermindertem Druck 2: HCl; water View Scheme |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
trimethyl orthoformate
Dimethoxy-2',2' ethyl-2 trimethyl-1,3,3 cyclohexene-1
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In methanol for 24h; Ambient temperature; | 100% |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium acetate In methanol; water Reflux; | 100% |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
2,2-dideutero-2-(2,6,6-trimethylcyclohex-1-en-1-yl)ethanal
Conditions | Yield |
---|---|
With water-d2; sodium hydride In pyridine at 25℃; for 4h; deuteration; | 99.9% |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
(2,6,6-trimethylcyclohex-1-enyl)acetonitrile
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; triethylamine In ethyl acetate; N,N-dimethyl-formamide at 100℃; | 97% |
Multi-step reaction with 2 steps 1: hydroxylamine hydrochloride; sodium acetate / methanol; water / Reflux 2: 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide / tetrahydrofuran; ethyl acetate / 20 °C / Inert atmosphere View Scheme |
pyrrolidine
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
1-<2-(2,6,6-trimethyl-1-cyclohexen-1-yl)ethenyl>pyrrolidine
Conditions | Yield |
---|---|
In toluene at 60℃; for 1h; | 96% |
In toluene at 60℃; for 1h; | 88% |
3-bromo-1-trifluoromethylbenzene
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
1-(3-(trifluoromethyl)phenyl)-2-(2,6,6-trimethylcyclohex-1-enyl)ethanol
Conditions | Yield |
---|---|
Stage #1: 3-bromo-1-trifluoromethylbenzene With iodine; magnesium In tetrahydrofuran for 0.0833333h; Reflux; Stage #2: (2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde In tetrahydrofuran at -78 - 20℃; for 2h; | 90% |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
2,4,4-trimethyl-3-(2'-hydroxymethyl)-2-cyclohexene
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol at 0 - 20℃; for 1h; | 85% |
With lithium aluminium tetrahydride In diethyl ether Heating; | |
With lithium aluminium tetrahydride | |
With lithium aluminium tetrahydride In diethyl ether | |
With sodium tetrahydroborate In methanol Inert atmosphere; |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
tert-butyldimethylsilyl chloride
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran | 85% |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
Conditions | Yield |
---|---|
With titanium tetrachloride In dichloromethane at -40 - 0℃; for 10h; diastereoselective reaction; | 85% |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
(+/-)-dihydroactinidiolide
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In chloroform for 17h; Heating; | 83% |
Multi-step reaction with 2 steps 1: 81 percent / m-CPBA (50-60percent), p-TsOH / CHCl3 / 1 h / Ambient temperature 2: 83 percent / silica gel / Heating; Irradiation; microwave irradiation (1.0 kW), 5-10 min View Scheme |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
S-benzyl malonic acid half thioester
Conditions | Yield |
---|---|
With 5-methoxy-1H-benzimidazole; ytterbium(III) triflate In tetrahydrofuran at 25℃; for 16h; Doebner-Knoevenagel condensation; | 82% |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
(+/-)-aeginetolide
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid In chloroform for 1h; Ambient temperature; | 81% |
Conditions | Yield |
---|---|
With water; sodium hydroxide In N,N-dimethyl-formamide at 30℃; Solvent; Temperature; Reagent/catalyst; Concentration; Aldol Condensation; | 81% |
3-fluorobromobenzene
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
1-(3-fluorophenyl)-2-(2,6,6-trimethylcyclohex-1-enyl)ethanol
Conditions | Yield |
---|---|
Stage #1: 3-fluorobromobenzene With iodine; magnesium In tetrahydrofuran for 0.0833333h; Reflux; Stage #2: (2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde In tetrahydrofuran at -78 - 20℃; for 2h; | 75% |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
A
(+/-)-dihydroactinidiolide
(+/-) aeginetolide
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In tetrachloromethane at 0 - 30℃; for 3h; Yields of byproduct given; | A n/a B 73% |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
(E)-2-(2,6,6-trimethylcyclohexen-1-yl)-ethenyl (trifluoromethyl)sulfonate
Conditions | Yield |
---|---|
Stage #1: (2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -78℃; for 2h; Stage #2: phenylbis[(trifluoromethyl)sulfonyl]amine In tetrahydrofuran; hexane at -78℃; Cooling; stereoselective reaction; | 73% |
1-bromo-3-chlorobenzene
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
1-(3-chlorophenyl)-2-(2,6,6-trimethylcyclohex-1-enyl)ethanol
Conditions | Yield |
---|---|
Stage #1: 1-bromo-3-chlorobenzene With iodine; magnesium In tetrahydrofuran for 0.0833333h; Reflux; Stage #2: (2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde In tetrahydrofuran at -78 - 20℃; for 2h; | 72% |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
A
2,4,4-trimethyl-3-(2-oxoethyl)-2-cyclohexen-1-one
Conditions | Yield |
---|---|
With pyridine N-oxide; selenium(IV) oxide In 1,4-dioxane at 80℃; for 4h; | A 15% B 64% |
N,N-phenylbistrifluoromethane-sulfonimide
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
(E)-2-(2,6,6-trimethylcyclohexen-1-yl)-ethenyl (trifluoromethyl)sulfonate
Conditions | Yield |
---|---|
Stage #1: (2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde With potassium tert-butylate In tetrahydrofuran at 0℃; for 0.25h; Stage #2: N,N-phenylbistrifluoromethane-sulfonimide In tetrahydrofuran at 20℃; for 0.5h; | 58% |
Nonafluorobutanesulfonyl fluoride
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
(E)-2-(2,6,6-trimethylcyclohexen-1-yl)ethenyl nonafluorobutanesulfonate
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran for 1h; Heating; | 52% |
With potassium tert-butylate In tetrahydrofuran for 1h; Heating; | 52% |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
2-(4-fluoro-3-(trifluoromethyl)phenyl)-1-(2,6,6-trimethylcyclohex-1-enyl)ethanol
Conditions | Yield |
---|---|
Stage #1: 4-fluoro-3-trifluoromethylbenzyl bromide With magnesium In diethyl ether for 1.25h; Reflux; Stage #2: (2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde In diethyl ether at -78 - 20℃; for 1h; | 42% |
4-bromo-2-fluoro-1-(trifluoromethoxy)benzene
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
1-(3-fluoro-4-(trifluoromethoxy)phenyl)-2-(2,6,6-trimethylcyclohex-1-enyl)ethanol
Conditions | Yield |
---|---|
Stage #1: 4-bromo-2-fluoro-1-(trifluoromethoxy)benzene With magnesium In diethyl ether for 0.666667h; Reflux; Stage #2: (2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde In diethyl ether at -78 - 20℃; for 1h; | 42% |
(2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde
1-bromomethyl-3-methyl-benzene
2-m-tolyl-1-(2,6,6-trimethylcyclohex-1-enyl)ethanol
Conditions | Yield |
---|---|
Stage #1: 1-bromomethyl-3-methyl-benzene With magnesium In diethyl ether for 1.33333h; Reflux; Stage #2: (2,6,6-trimethyl-1-cyclohexen-1-yl)acetaldehyde In diethyl ether at -78 - 20℃; for 1h; | 41% |
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