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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquirySuperiority We can customize and synthesize products that other suppliers may not be able to provide. 1. best service, high quality and reasonable way for h
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inquiryFactory direct sales, accept customization. N-Methyl-1,2-phenylenediamine may be used in the following studies: One-pot synthesis of 1-methyl-2(hetero)arylbenzimidazoles. Preparation of 1-methyl-1H-benzimidazole-2(3H)-thione. Total synthesis of
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inquiryN-Methylbenzene-1,2-diamine Chemical Properties Melting point 22 °C (lit.) Boiling point 123-124 °C/10 mmHg (lit.) density 1.075 g/mL at 25 °C (lit.) refractive index n20/D 1.612(lit.) Fp >230 °F form Liquid
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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Shanghai Lonwin Chemical company is a subsidiary of Lonwin Industry Group Limited, was established in 2011 and is headquartered in Shanghai, adjacent to China National Convention and Exhibition Center and Hongqiao transportation hub.Lonwinchem is
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inquiryConditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In methanol at 20℃; for 0.5h; | 98% |
With palladium 10% on activated carbon; hydrogen In methanol; ethanol at 20℃; under 3102.97 Torr; for 16h; Inert atmosphere; | 98% |
With iron; acetic acid at 60℃; for 1h; | 91% |
Conditions | Yield |
---|---|
With C12H16IrN4O2(1+)*BF4(1-); potassium hydroxide at 120℃; for 5h; Irradiation; Inert atmosphere; Sealed tube; | 91% |
1,2-diamino-benzene
carbonic acid dimethyl ester
A
1,3-dihydro-2H-benzimidazol-2-one
B
1,3-dimethyl-1,3-dihydrobenzimidazol-2-one
C
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
With lead(II) nitrate at 169.85℃; for 0.5h; | A 88% B n/a C n/a |
1,2-diamino-benzene
carbonic acid dimethyl ester
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
at 110℃; for 12h; Inert atmosphere; Molecular sieve; | 77% |
at 110℃; for 12h; Inert atmosphere; Molecular sieve; | 77% |
With zeolite NaY for 2h; Heating; | 75% |
NaY-faujasite zeolite for 5h; Heating / reflux; | |
With aluminum 1,4-benzenedicarboxylate at 170℃; for 8h; |
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
With water | 74% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 3h; | 61% |
With methanol |
Conditions | Yield |
---|---|
With methanesulfonic acid; trimethylsilylazide In tetrachloromethane at 80℃; for 4h; | 60% |
1-methyl-4-phenyl-1H-benzo[b][1,4]diazepin-2(3H)-one
A
3-phenyl-4H-isoxazol-5-one
B
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium acetate In ethanol Ambient temperature; | A 40% B 25% |
With hydroxylamine hydrochloride; sodium acetate In ethanol; water Ambient temperature; | A 40% B 25% |
Conditions | Yield |
---|---|
With sodium amide; naphthalene-1,8-diamine In xylene at 120 - 130℃; for 3h; | 38% |
carbon dioxide
phenylsilane
1,2-diamino-benzene
A
benzoimidazole
C
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
With methyl 5-(dimethylamino)-2-methyl-5-oxopentanoate at 50℃; under 750.075 Torr; for 8h; Time; Temperature; Pressure; | A 20% B 35% C n/a |
1,2-diamino-benzene
carbonic acid dimethyl ester
A
1,3-dihydro-2H-benzimidazol-2-one
B
1-methyl-2-benzimidazolone
C
1,3-dimethyl-1,3-dihydrobenzimidazol-2-one
D
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
With lead acetate at 159.85℃; for 1h; | A n/a B n/a C n/a D 6% |
With lead(II) nitrate at 159.85℃; for 1h; Product distribution; Further Variations:; Reagents; Reaction partners; Temperatures; |
1-methyl-1H-benzo[d][1,2,3]triazole
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
With ammonium bromide; ammonia; sodium |
1-(N-methyl-N-4-toluenesulfonylamino)-2-(N-4-toluenesulfonylamino)benzene
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
With sulfuric acid |
1-[bis-(toluene-4-sulfonyl)-amino]-2-[methyl-(toluene-4-sulfonyl)-amino]-benzene
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
With sulfuric acid |
methanol
1,2-diamino-benzene
methyl iodide
N-methyl-1,2-phenylenediamine
1,2-dimethyl-1H-benzimidazole
bromobenzene
A
acetophenone
B
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
With hydrogenchloride; lithium In diethyl ether; toluene for 4h; Product distribution; 4h 20 grad C, 1h reflux; |
4,5-Dihydro-2-<(2-aminophenyl)methylamino>-4-oxo-3-furancarboxylic acid ethyl ester
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
With sodium carbonate Heating; |
Conditions | Yield |
---|---|
at 150℃; |
1-methyl-1H-benzo[d][1,2,3]triazole
ammonia
N-methyl-1,2-phenylenediamine
hydrogenchloride
N-nitroso N-methyl-N-(2-nitroaniline)
N-methyl-1,2-phenylenediamine
hydrogenchloride
N-nitroso N-methyl-N-(2-nitroaniline)
N-methyl-1,2-phenylenediamine
N-nitroso N-methyl-N-(2-nitroaniline)
N-methyl-1,2-phenylenediamine
hydrogenchloride
N-nitroso N-ethyl-N-(2-nitroaniline)
N-methyl-1,2-phenylenediamine
hydrogenchloride
N-nitroso N-ethyl-N-(2-nitroaniline)
N-methyl-1,2-phenylenediamine
N-nitroso N-ethyl-N-(2-nitroaniline)
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 98 percent / methanol; H2O / Heating 2: 98 percent / H2 / Pd/C / methanol / 0.5 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 82 percent / Et3N / CH2Cl2 / Ambient temperature 2: 86 percent / K2CO3 / dimethylformamide / 0.25 h / 60 - 70 °C 3: 59 percent / cyclohexene / 10percent Pd/C / ethanol / Heating 4: 7percent aq. Na2CO3 / Heating View Scheme |
4,5-Dihydro-2-<(2-nitrophenyl)amino>-4-oxo-3-furancarboxylic acid ethyl ester
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 86 percent / K2CO3 / dimethylformamide / 0.25 h / 60 - 70 °C 2: 59 percent / cyclohexene / 10percent Pd/C / ethanol / Heating 3: 7percent aq. Na2CO3 / Heating View Scheme |
4,5-Dihydro-2-<(2-nitrophenyl)methylamino>-4-oxo-3-furancarboxylic acid ethyl ester
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 59 percent / cyclohexene / 10percent Pd/C / ethanol / Heating 2: 7percent aq. Na2CO3 / Heating View Scheme |
4-bromo-benzaldehyde
N-methyl-1,2-phenylenediamine
2-(4-bromophenyl)-1-methyl-1H-benzo[d]imidazole
Conditions | Yield |
---|---|
With oxygen; cetylpyridinium bromide In water at 20℃; for 0.75h; | 100% |
With dodecatungstosilic acid In ethyl acetate at 20℃; for 0.5h; | 99% |
3,5-di-tert-butyl-2-hydroxybenzaldehyde
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
In benzene for 2h; Reflux; | 100% |
In methanol for 16h; | 71% |
N-methyl-1,2-phenylenediamine
3-(adamantan-1-yl)-2-hydroxy-5-methylbenzaldehyde
Conditions | Yield |
---|---|
In benzene for 2h; Reflux; | 100% |
Conditions | Yield |
---|---|
In ethanol for 2h; | 100% |
Conditions | Yield |
---|---|
In ethanol for 2h; | 100% |
Conditions | Yield |
---|---|
In ethanol for 2h; | 100% |
Conditions | Yield |
---|---|
In ethanol for 2h; | 100% |
Conditions | Yield |
---|---|
In ethanol for 2h; | 100% |
N-methyl-1,2-phenylenediamine
2-nitro-benzaldehyde
1-methyl-2-(2-nitrophenyl)-2,3-dihydrobenzimidazole
Conditions | Yield |
---|---|
In methanol for 1h; Heating; | 99.5% |
With ethanol |
N-methyl-1,2-phenylenediamine
trifluoroacetic acid
1-methyl-2-(trifluoromethyl)-1H-benzo[d]imidazole
Conditions | Yield |
---|---|
at 70℃; for 16h; | 99% |
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
Stage #1: N-methyl-1,2-phenylenediamine With trimethylaluminum chloride In toluene at 0 - 20℃; Stage #2: hydroxymethyl JandaJelTM resin-bound 4-CF3-Ph ester In toluene for 24h; Heating; Further stages.; | 99% |
N-methyl-1,2-phenylenediamine
2-nitro-benzaldehyde
1-methyl-2-(2-nitrophenyl)-1H-benzo[d]imidazole
Conditions | Yield |
---|---|
With dodecatungstosilic acid In ethyl acetate at 20℃; for 0.0833333h; | 99% |
With Oxone In water; N,N-dimethyl-formamide at 20℃; | 80% |
4-chlorobenzaldehyde
N-methyl-1,2-phenylenediamine
2-(4-chlorophenyl)-1-methyl-1H-benzo[d]imidazole
Conditions | Yield |
---|---|
With dodecatungstosilic acid In ethyl acetate at 20℃; for 0.333333h; | 99% |
N-methyl-1,2-phenylenediamine
benzylamine
1-methyl-2-phenylbenzimidazole
Conditions | Yield |
---|---|
With 4-tert-butyl-5-methoxy-1,2-benzoquinone; oxygen; toluene-4-sulfonic acid In acetonitrile at 60℃; for 24h; Schlenk technique; | 99% |
With sulfur In neat (no solvent) at 140℃; for 16h; Inert atmosphere; | 85% |
With C8H7NO3; copper(ll) bromide In water; isopropyl alcohol at 45℃; for 24h; Green chemistry; | 85% |
benzoic acid anhydride
N-methyl-1,2-phenylenediamine
1-methyl-2-phenylbenzimidazole
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one; water at 445℃; under 187519 Torr; for 0.00277778h; Supercritical conditions; | 99% |
With water In 1-methyl-pyrrolidin-2-one at 400℃; under 187519 Torr; for 0.000491667h; Flow reactor; Green chemistry; | > 99 %Chromat. |
3-acetyl-4-hydroxy-6-methyl-2H-pyran-2-one
N-methyl-1,2-phenylenediamine
4-Hydroxy-6-methyl-3-{1-[(E)-2-methylamino-phenylimino]-ethyl}-pyran-2-one
Conditions | Yield |
---|---|
In methanol | 98% |
N-methyl-1,2-phenylenediamine
3-amino propanoic acid
2-(1-methyl-1H-benzo[d]imidazol-2-yl)ethanamine dihydrochloride
Conditions | Yield |
---|---|
Stage #1: N-methyl-1,2-phenylenediamine; 3-amino propanoic acid With hydrogenchloride In water for 96h; Reflux; Stage #2: In ethanol; water at 8℃; for 24h; | 97% |
With hydrogenchloride for 100h; Heating; | 70% |
benzaldehyde
N-methyl-1,2-phenylenediamine
1-methyl-2-phenylbenzimidazole
Conditions | Yield |
---|---|
With sodium metabisulfite In N,N-dimethyl-formamide Reflux; | 97% |
With Ag2CO3/celite In ethanol at 70℃; for 3h; | 94% |
In water; N,N-dimethyl-formamide at 80℃; | 90% |
N-(Benzyloxycarbonyl)glycine
N-methyl-1,2-phenylenediamine
N-[2-(N-methylamino)phenyl]-2-[(phenylmethoxy)carbonylamino]ethanamide
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In tetrahydrofuran at 20℃; for 6h; | 97% |
3,5-Pyridinedicarboxylic acid
N-methyl-1,2-phenylenediamine
pyridine-3,5-bis(1-methyl-benzimidazole-2-yl)
Conditions | Yield |
---|---|
With polyphosphoric acid at 100 - 200℃; for 26h; | 97% |
tert-butylisonitrile
N-methyl-1,2-phenylenediamine
N-tert-butyl-1-methyl-1H-benzo[d]imidazol-2-amine
Conditions | Yield |
---|---|
With oxygen; palladium diacetate In 2-methyltetrahydrofuran at 75℃; for 2h; Molecular sieve; | 97% |
With dipotassium peroxodisulfate; sodium acetate; cobalt(II) diacetate tetrahydrate In 1,4-dioxane at 100℃; for 18h; | 87% |
With tert.-butylhydroperoxide; sodium carbonate; cobalt acetylacetonate In 1,4-dioxane at 75℃; for 1h; Sonication; | 69% |
With cobalt(II) acetate; potassium carbonate In acetonitrile at 80℃; for 24h; Sealed tube; | 44% |
Conditions | Yield |
---|---|
With dimethylamine borane; potassium carbonate In ethanol; water under 15001.5 Torr; for 18h; Catalytic behavior; Autoclave; | 97% |
With tris(pentafluorophenyl)borate; phenylsilane In tetrahydrofuran at 120℃; under 7500.75 Torr; for 24h; Autoclave; | 95% |
With dimethylamine borane In water at 100℃; under 18751.9 Torr; for 24h; Heating; Green chemistry; | 94% |
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 20℃; for 4.5h; | 96% |
glycolic Acid
N-methyl-1,2-phenylenediamine
(1-methyl-1H-benzimidazol-2-yl)methanol
Conditions | Yield |
---|---|
With hydrogenchloride In water at 130℃; Sealed tube; | 96% |
With phosphoric acid at 130℃; for 3h; | 76% |
With hydrogenchloride Heating; | |
Stage #1: glycolic Acid; N-methyl-1,2-phenylenediamine With hydrogenchloride In water at 95℃; for 12h; Phillips cyclocondensation; Inert atmosphere; Stage #2: With sodium hydrogencarbonate In water Saturated solution; | |
With hydrogenchloride In water at 65 - 100℃; for 5h; |
N,N-dimethyl-formamide
N-methyl-1,2-phenylenediamine
1-Methylbenzimidazole
Conditions | Yield |
---|---|
With hydrogenchloride In water at 150℃; for 0.0333333h; Microwave irradiation; | 96% |
With zinc(II) acetate dihydrate In neat (no solvent) at 120℃; under 7600.51 Torr; for 18h; Autoclave; Inert atmosphere; Green chemistry; | 95% |
With phenylsilane at 120℃; for 12h; | 31% |
With Triethoxysilane; carbon dioxide; tris(pentafluorophenyl)borate at 120℃; for 24h; | 94 %Spectr. |
N-methyl-1,2-phenylenediamine
Conditions | Yield |
---|---|
With phosphorus trichloride 1) ether, 0.5 h, room temperature, 2) reflux, 36 h; | 95.7% |
4-nitrobenzaldehdye
N-methyl-1,2-phenylenediamine
1-methyl-2-(4-nitrophenyl)-1H-benzimidazole
Conditions | Yield |
---|---|
With dodecatungstosilic acid In ethyl acetate at 20℃; for 0.0833333h; | 95% |
With oxygen; cetylpyridinium bromide In water at 20℃; for 1.75h; | 95% |
With p-toluenesulfonic acid adsorbed on silica gel at 60 - 70℃; for 0.0833333h; | 77% |
With ethanol |
Conditions | Yield |
---|---|
With pyridine In dichloromethane for 12h; Acylation; | 95% |
4-methyl-benzaldehyde
N-methyl-1,2-phenylenediamine
1-methyl-2-p-tolyl-1H-benzoimidazole
Conditions | Yield |
---|---|
With dodecatungstosilic acid In ethyl acetate at 20℃; for 0.5h; | 95% |
With palladium 10% on activated carbon In dodecane; N,N-dimethyl acetamide at 120℃; for 14h; Inert atmosphere; | 80% |
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