As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:484-94-6
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inquirysuperior quality Appearance:powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as Pharmaceutical Intermediates Transportation:as per your
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
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Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Benzene,1-fluoro-2-methoxy-3-nitro-Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express
Best quality with low price Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:484-94-6
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Cerametek Materials (CMT) is your industrial and R&D supplier: 1. Semiconductor materials: Compounds of II, III, IV, V, VI groups such as Metal Sulfides, Selenides, Tellurides, Arsenide, Antimonide, Phosphide... 2. Advanced ceramic and crys
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inquiryAt Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App
FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 2-Fluoro-6-nitroanisole, CAS:484-94-6 with the most competitive price and the best qu
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inquiryConditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal In ethyl acetate for 24h; | 94% |
With platinum Hydrogenation; | |
With hydrogen; palladium on activated charcoal In methanol at 20℃; for 27h; |
Conditions | Yield |
---|---|
Stage #1: 2-(Diethylamino)ethanol With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.666667h; Stage #2: 1-fluoro-2-methoxy-3-nitrobenzene In N,N-dimethyl-formamide at 20℃; | 19% |
1-fluoro-2-methoxy-3-nitrobenzene
1-bromo-2-methoxy-3-fluorobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: H2 / Pd/C / methanol / 27 h / 20 °C 2.1: aq. HBr; NaNO2 / 0 - 5 °C 2.2: CuBr; aq. HBr / 60 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C / 2844.39 Torr 2.1: sodium nitrite / water / 1 h / -5 - 0 °C 2.2: 2 h / 0 - 50 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: hydrogen; palladium 10% on activated carbon / methanol / 4 h / 20 °C / 2844.39 Torr 2.1: sodium nitrite; hydrogen bromide / water / 1 h / -5 - 0 °C 2.2: 2 h / 0 - 50 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: palladium 10% on activated carbon; hydrogen / methanol / 20 °C / 2844.39 Torr 2.1: hydrogen bromide; sodium nitrite / water / 1 h / -5 - 0 °C 2.2: 2 h / 0 - 50 °C View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
4-bromo-2-fluoro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: H2 / Pd/C / methanol / 27 h / 20 °C 2.1: aq. HBr; NaNO2 / 0 - 5 °C 2.2: CuBr; aq. HBr / 60 °C 3.1: LDA / tetrahydrofuran; hexane / 1.5 h / -78 °C 3.2: tetrahydrofuran; hexane / -78 - 20 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C / 2844.39 Torr 2.1: sodium nitrite / water / 1 h / -5 - 0 °C 2.2: 2 h / 0 - 50 °C 3.1: diisopropylamine; n-butyllithium / tetrahydrofuran / 1 h / -70 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: hydrogen; palladium 10% on activated carbon / methanol / 4 h / 20 °C / 2844.39 Torr 2.1: sodium nitrite; hydrogen bromide / water / 1 h / -5 - 0 °C 2.2: 2 h / 0 - 50 °C 3.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -70 °C View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: H2 / Pd/C / methanol / 27 h / 20 °C 2.1: aq. HBr; NaNO2 / 0 - 5 °C 2.2: CuBr; aq. HBr / 60 °C 3.1: LDA / tetrahydrofuran; hexane / 1.5 h / -78 °C 3.2: tetrahydrofuran; hexane / -78 - 20 °C 4.1: oxalyl chloride; DMF / CH2Cl2 / 20 °C View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
ethyl 3-(4-bromo-2-fluoro-3-methoxyphenyl)-3-oxopropionate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: H2 / Pd/C / methanol / 27 h / 20 °C 2.1: aq. HBr; NaNO2 / 0 - 5 °C 2.2: CuBr; aq. HBr / 60 °C 3.1: LDA / tetrahydrofuran; hexane / 1.5 h / -78 °C 3.2: tetrahydrofuran; hexane / -78 - 20 °C 4.1: oxalyl chloride; DMF / CH2Cl2 / 20 °C 5.1: n-BuLi / hexane; tetrahydrofuran / -78 °C 5.2: 4.70 g / hexane; tetrahydrofuran; CH2Cl2 / -78 - 10 °C View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
7-bromo-9-cyclopropyl-8-methoxy-9H-isothiazolo[5,4-b]quinoline-3,4-dione
Conditions | Yield |
---|---|
Multi-step reaction with 10 steps 1.1: H2 / Pd/C / methanol / 27 h / 20 °C 2.1: aq. HBr; NaNO2 / 0 - 5 °C 2.2: CuBr; aq. HBr / 60 °C 3.1: LDA / tetrahydrofuran; hexane / 1.5 h / -78 °C 3.2: tetrahydrofuran; hexane / -78 - 20 °C 4.1: oxalyl chloride; DMF / CH2Cl2 / 20 °C 5.1: n-BuLi / hexane; tetrahydrofuran / -78 °C 5.2: 4.70 g / hexane; tetrahydrofuran; CH2Cl2 / -78 - 10 °C 6.1: sodium hydride / dimethylformamide / 0 - 20 °C 6.2: 76 percent / dimethylformamide / 24 h / 20 °C 7.1: sodium hydride / dimethylformamide / 72 h / 75 °C 8.1: 290.9 mg / m-chloroperbenzoic acid / CH2Cl2 / 1 h / 20 °C 9.1: sodium hydrosulfide / dimethylformamide / 1 h / 50 °C 10.1: 121.9 g / aq. NaHCO3; hydroxylamine-O-sulfonic acid / tetrahydrofuran / 2.5 h / 20 °C View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
ethyl 7-bromo-1-cyclopropyl-8-methoxy-2-methylsulfanyl-4-oxo-1,4-dihydroquinoline-3-carboxylate
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1.1: H2 / Pd/C / methanol / 27 h / 20 °C 2.1: aq. HBr; NaNO2 / 0 - 5 °C 2.2: CuBr; aq. HBr / 60 °C 3.1: LDA / tetrahydrofuran; hexane / 1.5 h / -78 °C 3.2: tetrahydrofuran; hexane / -78 - 20 °C 4.1: oxalyl chloride; DMF / CH2Cl2 / 20 °C 5.1: n-BuLi / hexane; tetrahydrofuran / -78 °C 5.2: 4.70 g / hexane; tetrahydrofuran; CH2Cl2 / -78 - 10 °C 6.1: sodium hydride / dimethylformamide / 0 - 20 °C 6.2: 76 percent / dimethylformamide / 24 h / 20 °C 7.1: sodium hydride / dimethylformamide / 72 h / 75 °C View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
ethyl 7-bromo-1-cyclopropyl-2-mercapto-8-methoxy-4-oxo-1,4-dihydroquinoline-3-carboxylate
Conditions | Yield |
---|---|
Multi-step reaction with 9 steps 1.1: H2 / Pd/C / methanol / 27 h / 20 °C 2.1: aq. HBr; NaNO2 / 0 - 5 °C 2.2: CuBr; aq. HBr / 60 °C 3.1: LDA / tetrahydrofuran; hexane / 1.5 h / -78 °C 3.2: tetrahydrofuran; hexane / -78 - 20 °C 4.1: oxalyl chloride; DMF / CH2Cl2 / 20 °C 5.1: n-BuLi / hexane; tetrahydrofuran / -78 °C 5.2: 4.70 g / hexane; tetrahydrofuran; CH2Cl2 / -78 - 10 °C 6.1: sodium hydride / dimethylformamide / 0 - 20 °C 6.2: 76 percent / dimethylformamide / 24 h / 20 °C 7.1: sodium hydride / dimethylformamide / 72 h / 75 °C 8.1: 290.9 mg / m-chloroperbenzoic acid / CH2Cl2 / 1 h / 20 °C 9.1: sodium hydrosulfide / dimethylformamide / 1 h / 50 °C View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
ethyl 7-bromo-1-cyclopropyl-2-methanesulfinyl-8-methoxy-4-oxo-1,4-dihydroquinoline-3-carboxylate
Conditions | Yield |
---|---|
Multi-step reaction with 8 steps 1.1: H2 / Pd/C / methanol / 27 h / 20 °C 2.1: aq. HBr; NaNO2 / 0 - 5 °C 2.2: CuBr; aq. HBr / 60 °C 3.1: LDA / tetrahydrofuran; hexane / 1.5 h / -78 °C 3.2: tetrahydrofuran; hexane / -78 - 20 °C 4.1: oxalyl chloride; DMF / CH2Cl2 / 20 °C 5.1: n-BuLi / hexane; tetrahydrofuran / -78 °C 5.2: 4.70 g / hexane; tetrahydrofuran; CH2Cl2 / -78 - 10 °C 6.1: sodium hydride / dimethylformamide / 0 - 20 °C 6.2: 76 percent / dimethylformamide / 24 h / 20 °C 7.1: sodium hydride / dimethylformamide / 72 h / 75 °C 8.1: 290.9 mg / m-chloroperbenzoic acid / CH2Cl2 / 1 h / 20 °C View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: H2 / Pd/C / methanol / 27 h / 20 °C 2.1: aq. HBr; NaNO2 / 0 - 5 °C 2.2: CuBr; aq. HBr / 60 °C 3.1: LDA / tetrahydrofuran; hexane / 1.5 h / -78 °C 3.2: tetrahydrofuran; hexane / -78 - 20 °C 4.1: oxalyl chloride; DMF / CH2Cl2 / 20 °C 5.1: n-BuLi / hexane; tetrahydrofuran / -78 °C 5.2: 4.70 g / hexane; tetrahydrofuran; CH2Cl2 / -78 - 10 °C 6.1: sodium hydride / dimethylformamide / 0 - 20 °C 6.2: 76 percent / dimethylformamide / 24 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 94 percent / hydrogen / 5percent Pd/C / ethyl acetate / 24 h 3: 84 percent / 48percent HBr / 4.5 h / Heating View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
fluoro-3 methoxy-2 benzaldehhyde
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 94 percent / hydrogen / 5percent Pd/C / ethyl acetate / 24 h View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: platinum / Hydrogenation 2: concentrated aqueous HCl / Diazotization.anschliessende Behandlung mit NaBF4 und Erhitzen des erhaltenen Diazonium-tetrafluoroborats unter vermindertem Druck View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: platinum / Hydrogenation 2: concentrated aqueous HCl / Diazotization.anschliessende Behandlung mit NaBF4 und Erhitzen des erhaltenen Diazonium-tetrafluoroborats unter vermindertem Druck 3: concentrated H2SO4; HNO3 View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: platinum / Hydrogenation 2: concentrated aqueous HCl / Diazotization.anschliessende Behandlung mit NaBF4 und Erhitzen des erhaltenen Diazonium-tetrafluoroborats unter vermindertem Druck 3: concentrated H2SO4; HNO3 4: platinum; methanol / Hydrogenation View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: platinum / Hydrogenation 2: concentrated aqueous HCl / Diazotization.anschliessende Behandlung mit NaBF4 und Erhitzen des erhaltenen Diazonium-tetrafluoroborats unter vermindertem Druck 3: concentrated H2SO4; HNO3 4: platinum; methanol / Hydrogenation 5: aqueous H2SO4; aqueous CuSO4-solution; xylene / Diazotization View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
4-nitro-benzoic acid-(3-fluoro-2-methoxy-anilide)
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: platinum / Hydrogenation View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
4-nitro-benzoic acid-(3,5-difluoro-4-methoxy-anilide)
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: platinum / Hydrogenation 2: concentrated aqueous HCl / Diazotization.anschliessende Behandlung mit NaBF4 und Erhitzen des erhaltenen Diazonium-tetrafluoroborats unter vermindertem Druck 3: concentrated H2SO4; HNO3 4: platinum; methanol / Hydrogenation View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
5-(2,6-diiodo-4-nitro-phenoxy)-1,3-difluoro-2-methoxy-benzene
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: platinum / Hydrogenation 2: concentrated aqueous HCl / Diazotization.anschliessende Behandlung mit NaBF4 und Erhitzen des erhaltenen Diazonium-tetrafluoroborats unter vermindertem Druck 3: concentrated H2SO4; HNO3 4: platinum; methanol / Hydrogenation 5: aqueous H2SO4; aqueous CuSO4-solution; xylene / Diazotization 6: K2CO3; pentanone-(2) View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
4,4'-dimethoxy-3,3',5,5'-tetrafluoroazoxybenzene
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: platinum / Hydrogenation 2: concentrated aqueous HCl / Diazotization.anschliessende Behandlung mit NaBF4 und Erhitzen des erhaltenen Diazonium-tetrafluoroborats unter vermindertem Druck 3: concentrated H2SO4; HNO3 4: platinum; methanol / Hydrogenation View Scheme |
1-fluoro-2-methoxy-3-nitrobenzene
4-(3,5-difluoro-4-methoxy-phenoxy)-3,5-diiodo-aniline; hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: platinum / Hydrogenation 2: concentrated aqueous HCl / Diazotization.anschliessende Behandlung mit NaBF4 und Erhitzen des erhaltenen Diazonium-tetrafluoroborats unter vermindertem Druck 3: concentrated H2SO4; HNO3 4: platinum; methanol / Hydrogenation 5: aqueous H2SO4; aqueous CuSO4-solution; xylene / Diazotization 6: K2CO3; pentanone-(2) 7: tin (II)-chloride; acetic acid View Scheme |
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