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Cas:5205-39-0
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Min.Order:1 Kilogram
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Min.Order:1 Gram
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inquiry5-chloro-5-oxoPentanoic acid ethyl ester Application:5-chloro-5-oxoPentanoic acid ethyl ester
Ethyl 5-chloro-5-oxovalerate cas 5205-39-0Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquirythionyl chloride
5-ethoxy-5-oxopentanoic acid
ethyl glutaroyl chloride
Conditions | Yield |
---|---|
68% |
Conditions | Yield |
---|---|
(i), (ii) SOCl2; Multistep reaction; | |
Stage #1: glutaric anhydride,; ethanol Heating; Stage #2: With thionyl chloride |
Conditions | Yield |
---|---|
With thionyl chloride | |
With thionyl chloride for 72h; | |
With phosphorus pentachloride In diethyl ether for 1h; Ambient temperature; |
ethyl glutaroyl chloride
Conditions | Yield |
---|---|
With thionyl chloride; diethyl ether |
ethyl glutaroyl chloride
Conditions | Yield |
---|---|
With thionyl chloride; diethyl ether |
ethyl glutaroyl chloride
{5-chloro-2-[(2,2-dimethylpropyl)amino]phenyl}(2-chlorophenyl)methanol
ethyl 5-[{4-chloro-2-[(2-chlorophenyl)(hydroxy)methyl]-phenyl}(2,2-dimethylpropyl)amino]-5-oxopentanoate
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane at 20℃; for 2h; Cooling with ice; | 100% |
ethyl glutaroyl chloride
(S)-(5-methoxy-1,2,3,4-tetrahydro-naphthalen-2-yl)-propylamine hydrochloride
(S)-ethyl 5-((5-methoxy-1,2,3,4-tetrahydronaphthalen-2-yl)(propyl)amino)-5-oxopentanoate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 3h; | 99% |
Conditions | Yield |
---|---|
With pyridine In benzene at 90℃; for 0.5h; | 98% |
ethyl glutaroyl chloride
1-hexynylzinc chloride
5-oxo-undec-6-ynoic acid ethyl ester
Conditions | Yield |
---|---|
In tetrahydrofuran at -78 - 0℃; for 1h; | 98% |
ethyl glutaroyl chloride
2-methoxy-4,4,5,5-tetramethyl-1,3,2-dioxaphospholane
5-Oxo-5-(4,4,5,5-tetramethyl-2-oxo-2λ5-[1,3,2]dioxaphospholan-2-yl)-pentanoic acid ethyl ester
Conditions | Yield |
---|---|
at 20 - 35℃; | 97% |
ethyl glutaroyl chloride
amino-2 bis(ethoxycarbonylamino)-4,4' biphenyle
glutaramate d'ethyle
Conditions | Yield |
---|---|
In chlorobenzene Heating; | 96% |
ethyl glutaroyl chloride
4,4,5,5-tetramethyl<1,3,2>dioxaphospholane-2-oxide
2-methoxy-4,4,5,5-tetramethyl-1,3,2-dioxaphospholane
5-Hydroxy-5,5-bis-(4,4,5,5-tetramethyl-2-oxo-2λ5-[1,3,2]dioxaphospholan-2-yl)-pentanoic acid ethyl ester
Conditions | Yield |
---|---|
at 80℃; for 6h; | 96% |
ethyl glutaroyl chloride
(2-aminophenyl)(phenyl)methanone
4-(2-Benzoyl-phenylcarbamoyl)-butyric acid ethyl ester
Conditions | Yield |
---|---|
With pyridine In dichloromethane Ambient temperature; | 95% |
ethyl glutaroyl chloride
1'-[3-(4-ethoxycarbonyl-butyryl)-3-aza-spiro[5.5]undecane-9-carbonyl]-[4,4']bipiperidinyl-1-carboxylic acid benzyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane | 92% |
ethyl glutaroyl chloride
4-(1-oxo-2,8-diazaspiro[4.5]dec-2-yl)benzonitrile
5-[2-(4-cyanophenyl)-1-oxo-2,8-diazaspiro[4.5]dec-8-yl]-5-oxopentanoic acid ethyl ester
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 4h; | 92% |
ethyl glutaroyl chloride
2-phenylaniline
N-(biphenylyl-2) glutaramate d'ethyle
Conditions | Yield |
---|---|
In diethyl ether at 25℃; | 90% |
Conditions | Yield |
---|---|
Stage #1: butyl magnesium bromide With tributylphosphine In tetrahydrofuran at 20℃; Stage #2: ethyl glutaroyl chloride In tetrahydrofuran at -40℃; for 0.333333h; | 90% |
ethyl glutaroyl chloride
[13C]methyl iodide
Ethyl (6-13C)-5-oxohexanoate
Conditions | Yield |
---|---|
With copper(l) iodide; lithium In diethyl ether | 90% |
Conditions | Yield |
---|---|
With potassium carbonate In water; ethyl acetate at 0℃; for 2h; | 89% |
Conditions | Yield |
---|---|
In tetrahydrofuran at -10 - 20℃; for 1.5h; | 88% |
ethyl glutaroyl chloride
2-Benzenesulfonylmethyl-cyclohex-2-enol
C20H26O6S
Conditions | Yield |
---|---|
With pyridine In dichloromethane | 88% |
ethyl glutaroyl chloride
4,4'-dinitro-2-biphenylamine
(dinitro-4,4' biphenylyl-2)glutaramate d'ethyle
Conditions | Yield |
---|---|
In chlorobenzene Heating; | 87% |
ethyl glutaroyl chloride
(trimethylsilyl)methylmagnesium chloride
ethyl 5-oxo-6-trimethylsilylhexanoate
Conditions | Yield |
---|---|
With copper(l) iodide In tetrahydrofuran at -40℃; for 1.5h; | 86% |
ethyl glutaroyl chloride
3β-hydroxy-28-lupanal
Conditions | Yield |
---|---|
With pyridine; dmap at 20℃; for 48h; | 86% |
ethyl glutaroyl chloride
3,5-dimethyl-2-ethoxycarbonyl-1H-pyrrole
ethyl 5-<5-(ethoxycarbonyl)-2,4-dimethylpyrrol-3-yl>-5-oxopentanoate
Conditions | Yield |
---|---|
With tin(IV) chloride In dichloromethane at 0℃; | 84% |
With tin(ll) chloride In dichloromethane at 0℃; for 1.5h; | 84.1% |
ethyl glutaroyl chloride
glycine ethyl ester hydrochloride
ethyl N-(ethoxyglutaryl)glycinate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane 1.) 2h; 2.) reflux, 2 h; | 83% |
ethyl glutaroyl chloride
(phenylethynyl)zinc chloride
ethyl 5-oxo-7-phenylhept-6-ynoate
Conditions | Yield |
---|---|
In tetrahydrofuran at -78 - 0℃; for 1h; | 82% |
ethyl glutaroyl chloride
(E)-1-(4-hydroxyphenyl)-2-nitroethene
ethyl 4-<(E)-2-nitroethenyl>phenyl glutarate
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In dichloromethane for 6.5h; Ambient temperature; | 80% |
Conditions | Yield |
---|---|
Stage #1: methylmagnesium bromide With tributylphosphine In tetrahydrofuran at 20℃; Stage #2: ethyl glutaroyl chloride In tetrahydrofuran at -40℃; for 0.333333h; | 80% |
With copper(l) iodide In tetrahydrofuran at -78 - 20℃; Inert atmosphere; |
ethyl glutaroyl chloride
Conditions | Yield |
---|---|
Stage #1: ethyl glutaroyl chloride With aluminum (III) chloride In dichloromethane at 0℃; for 0.5h; Stage #2: 2-(1H-indol-5-yl)-N-{phenyl[2-(piperidin-1-yl)phenyl]methyl}acetamide In dichloromethane at 0 - 20℃; for 53h; | 80% |
Conditions | Yield |
---|---|
With copper(l) iodide In tetrahydrofuran at -78 - 20℃; Schlenk technique; | 78% |
ethyl glutaroyl chloride
Conditions | Yield |
---|---|
Stage #1: 2-chloro-7-ethoxy-3-(3-(4-iodophenyl)-4,5-dihydro-1H-pyrazol-5-yl)quinoline With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 0.25h; Stage #2: ethyl glutaroyl chloride In dichloromethane at 20℃; for 12h; | 78% |
Stage #1: 2-chloro-7-ethoxy-3-(3-(4-iodophenyl)-4,5-dihydro-1H-pyrazol-5-yl)quinoline With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 0.25h; Stage #2: ethyl glutaroyl chloride In dichloromethane at 20℃; for 12h; | 78% |
ethyl glutaroyl chloride
2-(phenylsulfonylmethyl)phenol
C20H22O6S
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; | 73% |
ethyl glutaroyl chloride
2,4,4'-trihydroxy deoxybenzoin
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; potassium carbonate In acetone for 25h; Cyclization; Heating; | 71% |
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