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1H-Pyrido[4,3-b]indole,2,3,4,5-tetrahydro-2-methyl-5-(phenylmethyl)- cas 524-81-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiry5-BENZYL-2-METHYL-2,3,4,5-TETRAHYDRO-1H-PYRIDO[4,3-B]INDOLE Basic information Product Name: 5-BENZYL-2-METHYL-2,3,4,5-TETRAHYDRO-1H-PYRIDO[4,3-B]INDOLE Synonyms: 5-BENZYL-2-METHYL-2,3,4,5-TETRAHYDRO-1H-PY
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Min.Order:500 Gram
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inquirymebhydrolin
Conditions | Yield |
---|---|
With sodium hydroxide | 97% |
mebhydrolin
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol at 20℃; for 24h; | 73% |
Conditions | Yield |
---|---|
With hydrogenchloride | |
With sulfuric acid |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 88 percent / propan-2-ol / 3.5 h / Heating 2: 73 percent / NaBH4 / aq. ethanol / 24 h / 20 °C View Scheme |
2-methyl-2H-pyrido[4,3-b]indole
mebhydrolin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 88 percent / propan-2-ol / 3.5 h / Heating 2: 73 percent / NaBH4 / aq. ethanol / 24 h / 20 °C View Scheme |
1-methyl-4-oxo-piperidine-3-carboxylic acid methyl ester
mebhydrolin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogenchloride / water / 5.17 h / Reflux 2: 10 h / Reflux View Scheme |
1-methylpiperidin-4-one hydrochloride
N-benzyl-N-phenylhydrazine
mebhydrolin
Conditions | Yield |
---|---|
for 10h; Time; Reflux; |
Conditions | Yield |
---|---|
In ethanol for 18h; cooling; | 94% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; | 92% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 48h; | 91% |
mebhydrolin
Conditions | Yield |
---|---|
With dihydrogen peroxide In methanol Heating; | 86% |
mebhydrolin
Conditions | Yield |
---|---|
In water at 40℃; for 2h; | 78% |
mebhydrolin
acetic acid
2-acetamido-1-N-(bromoacetyl)-2-deoxy-β-D-glucopyranosylamine
Conditions | Yield |
---|---|
Stage #1: mebhydrolin; 2-acetamido-1-N-(bromoacetyl)-2-deoxy-β-D-glucopyranosylamine In methanol at 20℃; for 16h; Stage #2: acetic acid In methanol; water | 66% |
mebhydrolin
A
1-Benzyl-5-methyl-4,5-dihydro-1H,3H-benzo[b][1,5]diazocine-2,6-dione
C
1-Benzyl-1'-methyl-spiro[indolin-2,3'-pyrrolidin]-3-on
Conditions | Yield |
---|---|
With sodium periodate In methanol for 24h; Product distribution; Mechanism; Ambient temperature; var. of reagent, temp., ratio, solvent, time; | A 18% B 10% C 12% D 10% E 23% |
With sodium periodate In methanol; water for 24h; Product distribution; Mechanism; Ambient temperature; var. of reagent, temp., solvent, ratio, time; | A 18% B 10% C 12% D 10% E 23% |
mebhydrolin
A
1-Benzyl-5-methyl-4,5-dihydro-1H,3H-benzo[b][1,5]diazocine-2,6-dione
B
1-Benzyl-1'-methyl-spiro[indolin-2,3'-pyrrolidin]-3-on
Conditions | Yield |
---|---|
With sodium periodate In methanol for 24h; Ambient temperature; Further byproducts given; | A 18% B 12% C 10% D 23% |
With sodium periodate In methanol; water for 24h; Ambient temperature; Further byproducts given; | A 18% B 12% C 10% D 23% |
mebhydrolin
benzyl chloride
2,5-dibenzyl-2-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indolium; chloride
Conditions | Yield |
---|---|
With acetone |
mebhydrolin
dimethyl sulfate
5-benzyl-2,2-dimethyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indolium; methyl sulfate
Conditions | Yield |
---|---|
With acetone |
mebhydrolin
potassium cyanide
5-Benzyl-2-methyl-2,3,4,5-tetrahydro-1H-pyrido[4,3-b]indole-1-carbonitrile
Conditions | Yield |
---|---|
With maleic acid; palladium 2) H2O; Yield given. Multistep reaction; | |
With maleic acid; palladium 1) heating, 2) H2O; Yield given. Multistep reaction; |
mebhydrolin
Conditions | Yield |
---|---|
With lead(IV) acetate; perchloric acid 1) CHCl3, 1 h; Yield given. Multistep reaction; | |
With lead(IV) acetate; perchloric acid 1) CHCl3, 1 h, 2) CHCl3; Yield given. Multistep reaction; | |
Multi-step reaction with 3 steps 1: 1) maleic acid / 1) Pd / 1) heating, 2) H2O 2: 92 percent / HClO4 / ethanol 3: 17 percent / aq. NaOH / 18 h View Scheme | |
Multi-step reaction with 3 steps 1: 1) maleic acid / 1) Pd / 2) H2O 2: 92 percent / HClO4 / ethanol 3: 17 percent / aq. NaIO4, NaOH / 18 h View Scheme |
mebhydrolin
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1) maleic acid / 1) Pd / 1) heating, 2) H2O 2: 92 percent / HClO4 / ethanol View Scheme | |
Multi-step reaction with 2 steps 1: 1) maleic acid / 1) Pd / 2) H2O 2: 92 percent / HClO4 / ethanol View Scheme |
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