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Hangzhou Think Chemical Co. Ltd

Name Mitotan Synonyms 2,4'-Dichlorodiphenyldichloroethane; 1,1-Dichloro-2,2-bis(2,4'-dichlorophenyl)ethane; 1-Chloro-2-(2,2-dichloro-1-(4-chlorophenyl)ethyl)benzene; 2,2-(2-Chlor

Good Supply Mitotane USP41 with competitive price

Cas:53-19-0

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Mitotan Manufacturer/High quality/Best price/In stock

Cas:53-19-0

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Appearance White crystalline powder White crystalline powder (A) IR ch

High purity Various Specifications 1-(2-chlorophenyl)-1-(4-chlorophenyl)-2,2-dichloroethane CAS:53-19-0

Cas:53-19-0

Min.Order:1 Gram

FOB Price: $100.0 / 500.0

Type:Trading Company

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Mitotane supplier in China

Cas:53-19-0

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

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Hubei Vanz Pharm Co.,Ltd

We are manufacture for the materials, and other sarms,steriods ,we also produce, price is very competitive, quality very good. Appearance:white powder Application:Pharmaceutical

CAS 53-19-0 MITOTANE

Cas:53-19-0

Min.Order:1 Gram

FOB Price: $10.0

Type:Manufacturers

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Wuhan Fortuna Chemical Co.,Ltd

Product Name: 1-(2-chlorophenyl)-1-(4-chlorophenyl)-2,2-dichloroethane CAS RN.: 53-19-0 EINECS:

Mitotan 53-19-0

Cas:53-19-0

Min.Order:25 Kilogram

Negotiable

Type:Trading Company

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Mitotane

Cas:53-19-0

Min.Order:1

Negotiable

Type:Other

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price API 99% Mitotan 53-19-0 GMP Manufacturer

Cas:53-19-0

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Shanghai Seasonsgreen Chemical Co.,Ltd

Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu

lower price High quality Mitotan

Cas:53-19-0

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Manufacturers

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

1-(2-Chlorophenyl)-1-(4-chlorophenyl)-2,2-dichloroethane

Cas:53-19-0

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con

53-19-0 Mitotan

Cas:53-19-0

Min.Order:1 Kilogram

FOB Price: $15.0 / 50.0

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

Mitotan,53-19-0

Cas:53-19-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 53-19-0 with competitive price

Cas:53-19-0

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after the dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available &diam

Mitotan CAS53-19-0

Cas:53-19-0

Min.Order:1 Kilogram

FOB Price: $7.0 / 10.0

Type:Trading Company

inquiry

HANWAYS CHEMPHARM CO.,LIMITED

We are concentrating on APIs and pharmaceutical intermediates. With in depth knowledge and understanding in this industry, we are indulged in supplying a wide assortments of Mitotane from Wuhan, Hubei, China. It is mad

Mitotane

Cas:53-19-0

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Benzene,1-chloro-2-[2,2-dichloro-1-(4-chlorophenyl)ethyl]- 53-19-0

Cas:53-19-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Xi'an Faithful Biotech Co., Ltd.

We are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery

Hangzhou Sartort Biopharma Co., Ltd

Appearance:White to off-white powder Storage:Room temperature Package:25kg/drum Application:Antitumor drugs Transportation:Express/Sea/Air Port:Any port in china

Good Supply Mitotane Mitotan 2,4-Dichlorodiphenyldichloroethane Mitotane

Cas:53-19-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

Mitotane/CAS:53-19-0

Cas:53-19-0

Min.Order:100 Milligram

FOB Price: $45.0

Type:Trading Company

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Benzene,1-chloro-2-[2,2-dichloro-1-(4-chlorophenyl)ethyl]-

Cas:53-19-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

Mitotan

Cas:53-19-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Taizhou Crene Biotechnology co.ltd

Our company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-

Mitotane 53-19-0

Cas:53-19-0

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Mitotan

Cas:53-19-0

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Mitotan

Cas:53-19-0

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

Mitotane

Cas:53-19-0

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fonlynn Health Technology Co., Ltd.

Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Transportation:Express/Sea/Air Port:Ningbo/Shanghai/Qingd

Mitotan

Cas:53-19-0

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shaanxi Cuicheng Biomedical Technology Co., Ltd.

Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu

Mitotan

Cas:53-19-0

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

superior quality Appearance:Crystalline Solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:aminobiphoshphanate for treatment of osteoporosis an

1-(2-chlorophenyl)-1-(4-chlorophenyl)-2,2-dichloroethane

Cas:53-19-0

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

TaiChem Taizhou Limited

Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site

Mitotan

Cas:53-19-0

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Siwei Development Group Ltd.

Product name: Mitotane CAS No.:53-19-0 Molecule Formula:C14H10Cl4 Molecule Weight:320.04 Purity: 98.0% Package: 25kg/drum Description:White to off-white solid Manufacture Standards:Enterprise Standard TESTING ITEMS

High Quality Mitotane in stock

Cas:53-19-0

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

2,2‐dichloro‐1‐(2‐chlorophenyl)ethan‐1‐one
24123-67-9

2,2‐dichloro‐1‐(2‐chlorophenyl)ethan‐1‐one

chlorobenzene
108-90-7

chlorobenzene

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

Conditions
ConditionsYield
Stage #1: 2,2‐dichloro‐1‐(2‐chlorophenyl)ethan‐1‐one With sodium tetrahydroborate In methanol at 20℃; for 0.333333h; Schlenk technique; Inert atmosphere;
Stage #2: chlorobenzene With sulfuric acid at 20℃; for 0.166667h;
89%
2,2-dichloro-1-(2-chlorophenyl)ethanol
27683-60-9

2,2-dichloro-1-(2-chlorophenyl)ethanol

chlorobenzene
108-90-7

chlorobenzene

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

Conditions
ConditionsYield
With sulfuric acid at 35℃; for 6h;71%
With sulfuric acid at 30 - 60℃;
With sulfuric acid; sulfur trioxide
o,p'-DDT
789-02-6

o,p'-DDT

A

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

B

1-(4-chlorophenyl)-1-phenylethane
60617-89-2

1-(4-chlorophenyl)-1-phenylethane

C

1-(o-chlorophenyl)-1-(p-chlorophenyl)ethane
77008-62-9

1-(o-chlorophenyl)-1-(p-chlorophenyl)ethane

D

1-(2-chloro-phenyl)-1-phenyl-ethane
76690-79-4

1-(2-chloro-phenyl)-1-phenyl-ethane

Conditions
ConditionsYield
With hydrogen; triethylamine; palladium on activated charcoal In methanol at 20℃; for 0.166667h;A 25%
B n/a
C 42%
D n/a
p,p'-DDT
50-29-3

p,p'-DDT

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

o,p'-DDT
789-02-6

o,p'-DDT

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

Conditions
ConditionsYield
With aluminium amalgam In ethanol
o,p'-DDT
789-02-6

o,p'-DDT

A

1-chloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane
13312-58-8

1-chloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane

B

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

Conditions
ConditionsYield
With sodium tetrahydroborate In dimethyl sulfoxide
sulfuric acid
7664-93-9

sulfuric acid

2,2-dichloro-1-(2-chlorophenyl)ethanol
27683-60-9

2,2-dichloro-1-(2-chlorophenyl)ethanol

chlorobenzene
108-90-7

chlorobenzene

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

Conditions
ConditionsYield
at 30 - 60℃;
2-chlorophenylmagnesium bromide
36692-27-0

2-chlorophenylmagnesium bromide

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: diethyl ether
2: concentrated H2SO4 / 30 - 60 °C
View Scheme
chlorobenzene
108-90-7

chlorobenzene

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: H2SO4
View Scheme
Multi-step reaction with 2 steps
1: H2SO4
View Scheme
2,2,2-trichloro-1-(2-chloro-phenyl)-ethanol
10291-39-1

2,2,2-trichloro-1-(2-chloro-phenyl)-ethanol

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Al-Hg, iPrOH
2: SO3/H2SO4
View Scheme
2-chloro-benzaldehyde
89-98-5

2-chloro-benzaldehyde

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: nBuLi
2: SO3/H2SO4
View Scheme
2-chlorophenylacetylene
873-31-4

2-chlorophenylacetylene

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium hydrogensulfate monohydrate; water; lithium chloride / acetonitrile / 24 h / 20 °C / Schlenk technique
2.1: sodium tetrahydroborate / methanol / 0.33 h / 20 °C / Schlenk technique; Inert atmosphere
2.2: 0.17 h / 20 °C
View Scheme
1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

1-Chloro-2-o-chlorophenyl-2-p'-chlorophenylethylene
14835-94-0

1-Chloro-2-o-chlorophenyl-2-p'-chlorophenylethylene

Conditions
ConditionsYield
With potassium hydroxide In ethanol at 80 - 90℃; for 2h;78%
With potassium hydroxide In 1,4-dioxane
1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

o-Chlorophenyl-1-p'-chlorophenylmethane
52094-02-7

o-Chlorophenyl-1-p'-chlorophenylmethane

Conditions
ConditionsYield
With potassium hydroxide In ethylene glycol for 6h; Heating;68%
1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

C14H9Cl3
120189-90-4

C14H9Cl3

Conditions
ConditionsYield
With hexacarbonyl molybdenum In various solvent(s) at 145℃; for 3h;90 % Chromat.
1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

1-(2-chlorophenyl)-1-(4-chlorophenyl)-2,2-dichloro-2-iodoethane

1-(2-chlorophenyl)-1-(4-chlorophenyl)-2,2-dichloro-2-iodoethane

Conditions
ConditionsYield
With N-iodo-succinimide; lithium diisopropyl amide 1.) THF, ether, -78 deg C, 50 min, 2.) THF, ether, 15 min; Multistep reaction;
sulfuric acid
7664-93-9

sulfuric acid

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

nitric acid
7697-37-2

nitric acid

2.2-dichloro-1-<2-chloro-3.5-dinitro-phenyl>-1-<4-chloro-3.5-dinitro-phenyl>-ethane (?)

2.2-dichloro-1-<2-chloro-3.5-dinitro-phenyl>-1-<4-chloro-3.5-dinitro-phenyl>-ethane (?)

Conditions
ConditionsYield
auf dem Dampfbad;
1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

nitric acid
7697-37-2

nitric acid

2.2-dichloro-1-<4-chloro-3-nitro-phenyl>-1-<6-chloro-3-nitro-phenyl>-ethane (?)

2.2-dichloro-1-<4-chloro-3-nitro-phenyl>-1-<6-chloro-3-nitro-phenyl>-ethane (?)

Conditions
ConditionsYield
at 50℃;
1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

ethanolic KOH

ethanolic KOH

1-Chloro-2-o-chlorophenyl-2-p'-chlorophenylethylene
14835-94-0

1-Chloro-2-o-chlorophenyl-2-p'-chlorophenylethylene

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

2,4'-dichlorobenzophenone
85-29-0

2,4'-dichlorobenzophenone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 78 percent / KOH / ethanol / 2 h / 80 - 90 °C
2: 54 percent / CrO3 / acetic acid / 1.5 h / 100 °C
View Scheme
1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

1-(o-chlorophenyl)-1-(p-chlorophenyl)ethane
77008-62-9

1-(o-chlorophenyl)-1-(p-chlorophenyl)ethane

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 78 percent / KOH / ethanol / 2 h / 80 - 90 °C
2: 54 percent / CrO3 / acetic acid / 1.5 h / 100 °C
3: 65 percent / diethyl ether / 1 h / Heating
4: 80 percent / H2 / 5percent Pd/C / ethanol / 0.5 h
View Scheme
1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

1-o-Chlorophenyl-1-p'-chlorophenylethylene
39274-24-3

1-o-Chlorophenyl-1-p'-chlorophenylethylene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 78 percent / KOH / ethanol / 2 h / 80 - 90 °C
2: 54 percent / CrO3 / acetic acid / 1.5 h / 100 °C
3: 65 percent / diethyl ether / 1 h / Heating
View Scheme
1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

1,2-Dichloro-2-o-chlorophenyl-2-p'-chlorophenylethane
90284-72-3

1,2-Dichloro-2-o-chlorophenyl-2-p'-chlorophenylethane

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 78 percent / KOH / ethanol / 2 h / 80 - 90 °C
2: 54 percent / CrO3 / acetic acid / 1.5 h / 100 °C
3: 65 percent / diethyl ether / 1 h / Heating
4: 76 percent / Cl2 / CCl4 / 24 h
View Scheme
1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

A

(R)-(+)-1,1-dichloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane

(R)-(+)-1,1-dichloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane

B

(S)-(-)-1,1-dichloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane

(S)-(-)-1,1-dichloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane

Conditions
ConditionsYield
With Daicel Chiralcel OJ-H column Resolution of racemate;
1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane
53-19-0

1,1-dichloro-2-(o-chlorophenyl)-2-(p-chlorophenyl)ethane

1-chloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane
13312-58-8

1-chloro-2-(2-chlorophenyl)-2-(4-chlorophenyl)ethane

Conditions
ConditionsYield
With triethylsilane; {Rh(H)[SiMe2(o-C6H4SMe)](PPh3)2}[BArF4] In neat (no solvent) at 80℃; for 72h; Inert atmosphere; Schlenk technique;

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