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inquiryGood quantity Sodium 2-naphthalenesulfonate Basic information Product Name: Sodium 2-naphthalenesulfonate Synonyms: 2-Naphthalenesulfonicacid,sod;sodiumnaphthalene-2-sulfonate;sodiumna
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inquiryProduct Name 2-Naphthalenesulfonic acid sodium salt CAS Registry Number 532-02-5 Molecular Structure Molecular Formula
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inquirymethyl naphthalene-2-sulfonate
A
methanol
B
2-naphthalenesulfonic acid sodium salt
Conditions | Yield |
---|---|
With sodium hydroxide at 25℃; Rate constant; in the presence of various cetyltrialkylammonium compounds; |
3-nitro-4-chlorobenzenesulfonic acid
iron
2-naphthalenesulfonic acid sodium salt
Conditions | Yield |
---|---|
With sodium carbonate In water; acetic acid |
2-naphthalenesulfonic acid sodium salt
sodium anilide
N-Phenyl-2-naphthylamine
Conditions | Yield |
---|---|
With aniline at 290℃; for 0.25h; | 99% |
With aniline at 290℃; for 0.25h; Product distribution; other temp.: 190 to 270 deg. C; other reaction time: 0.5 to 12 h; | 99% |
2-naphthalenesulfonic acid sodium salt
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide Pd complex mixed with 4 equiv. of NaONs in DMF at room temp.; | 99% |
Conditions | Yield |
---|---|
With trichlorophosphate In chloroform at 90℃; for 9h; Temperature; Solvent; Concentration; | 95.8% |
With trichlorophosphate; N,N-dimethyl acetamide In sulfolane; acetonitrile at 68 - 72℃; for 0.25h; | 91% |
With 1,3,5-trichloro-2,4,6-triazine; 18-crown-6 ether In acetone for 20h; Heating; | 89% |
With chlorine-triphenylphosphine In acetonitrile for 15h; Ambient temperature; |
Conditions | Yield |
---|---|
With triphenylphosphine; 18-crown-6 ether; iodine In benzene for 36h; Heating; | 93% |
With 18-crown-6 ether; iodine; triphenylphosphine In benzene for 36h; Heating; | 93% |
With potassium hydrosulfide in eisernen Gefaessen unter Druck; | |
With diphosphorus pentasulfide; lithium aluminium tetrahydride 1.) sulfolane, 90 deg C for 25 h 2.) ether, room temperature for 30 min; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
Stage #1: 2-naphthalenesulfonic acid sodium salt With 1,3,5-trichloro-2,4,6-triazine; tetrabutylammomium bromide In acetonitrile at 60℃; for 12h; Stage #2: With potassium hydrogen difluoride In acetone; acetonitrile at 20℃; for 12h; | 93% |
(trimethylsilyl)methylmagnesium chloride
2-naphthalenesulfonic acid sodium salt
trimethyl(naphthalen-2-ylmethyl)silane
Conditions | Yield |
---|---|
With bis(tricyclohexylphosphine)nickel(II) dichloride In tetrahydrofuran at 20℃; for 20h; Sealed tube; Inert atmosphere; | 92% |
2-naphthalenesulfonic acid sodium salt
aniline
A
N-Phenyl-2-naphthylamine
B
β-naphthol
Conditions | Yield |
---|---|
With potassium hydroxide at 230℃; for 6h; Product distribution; other bases: NaOH + K2CO3, NaOH + Na2CO3, NaOH + KCl, NaOH + KF, NaOH; other temp.: 230 to 310 deg. C, other reaction time: 2 to 12 h; | A 90% B 3% |
With sodium hydroxide; potassium carbonate at 310℃; for 4h; | A 34% B 65% |
Conditions | Yield |
---|---|
In methanol; water at 50 - 55℃; for 1h; | 90% |
2-naphthalenesulfonic acid sodium salt
silver(I) naphthalene-2-sulfonate
Conditions | Yield |
---|---|
With H(1+) In methanol; acetonitrile byproducts: CO2; Sonication; aq. soln. of Na compd. passed down a cation exchange column (acid form);solvent evapd.; redissolved in MeOH-MeCN; Ag2CO3 (1 equiv.) added; soni cated at room temp. for 30 min; filtered; concd. under reduced pressure; pptd. by addition of Et2O; elem. anal.; | 89% |
methylmagnesium chloride
2-naphthalenesulfonic acid sodium salt
2-Methylnaphthalene
Conditions | Yield |
---|---|
With bis(tricyclohexylphosphine)nickel(II) dichloride In tetrahydrofuran at 20℃; for 20h; Reagent/catalyst; Sealed tube; Inert atmosphere; | 84% |
2-naphthalenesulfonic acid sodium salt
Conditions | Yield |
---|---|
In water | 83% |
Conditions | Yield |
---|---|
With bis(tricyclohexylphosphine)nickel(II) dichloride In tetrahydrofuran at 20℃; for 20h; Reagent/catalyst; Sealed tube; Inert atmosphere; | 79% |
2-naphthalenesulfonic acid sodium salt
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; caesium carbonate In tert-butyl alcohol at 70℃; for 24h; regioselective reaction; | 78% |
2-naphthalenesulfonic acid sodium salt
4-methoxyphenyl magnesium bromide
2-(4-methoxyphenyl)naphthalene
Conditions | Yield |
---|---|
With bis(tricyclohexylphosphine)nickel(II) dichloride In tetrahydrofuran at 20℃; for 20h; Sealed tube; Inert atmosphere; | 77% |
Conditions | Yield |
---|---|
With dichlorobis(tricyclohexylphosphine)cobalt(II); isopropylmagnesium chloride In tetrahydrofuran at 60℃; for 20h; Reagent/catalyst; Sealed tube; Inert atmosphere; | 75% |
With phosphoric acid Product distribution; Heating; microwave activation; time dependence, other reagents; |
2-naphthalenesulfonic acid sodium salt
benzylmagnesium chloride
2-benzylnaphthalene
Conditions | Yield |
---|---|
With bis(tricyclohexylphosphine)nickel(II) dichloride In tetrahydrofuran at 20℃; for 20h; Sealed tube; Inert atmosphere; | 72% |
carbon dioxide
2-naphthalenesulfonic acid sodium salt
naphthalene-2-carboxylate
Conditions | Yield |
---|---|
Stage #1: carbon dioxide; 2-naphthalenesulfonic acid sodium salt With copper(l) iodide; potassium tert-butylate; o-phenanthroline In dimethyl sulfoxide at 140℃; under 760.051 Torr; for 12h; Schlenk technique; Stage #2: With hydrogenchloride In water; dimethyl sulfoxide Schlenk technique; | 70% |
2-phenyl-oxazole-4-carboxylic acid ethyl ester
2-naphthalenesulfonic acid sodium salt
ethyl 5-(naphthalen-2'-yl)-2-phenyloxazole-4-carboxylate
Conditions | Yield |
---|---|
With oxygen; palladium diacetate; potassium carbonate; bis[2-(diphenylphosphino)phenyl] ether In 1,4-dioxane at 100℃; for 20h; | 67% |
2-naphthalenesulfonic acid sodium salt
Conditions | Yield |
---|---|
With water In ethanol; water PrCl3*6H2O and C10H7SO3Na dissolved in warmed ethanol-water (2:1 v/v), stirred; filtered while hot, cooled, ppt. collected, washed with mixed solvent, ethanol, and diethyl ether; | 58% |
Conditions | Yield |
---|---|
With dichloro bis(acetonitrile) palladium(II); copper acetylacetonate; sodium carbonate In 1,4-dioxane at 130℃; for 24h; Sealed tube; Air; | 58% |
Conditions | Yield |
---|---|
In water at 55℃; for 3h; | 56% |
Conditions | Yield |
---|---|
In water aq. soln. of sulfonate and Ag salt was stirred for 5 min; soln. of bipyridine in MeOH was added; filtered; aq. soln. of NH3 added dropwise; kept for 5 d in dark; elem. anal.; | 55% |
2-naphthalenesulfonic acid sodium salt
Conditions | Yield |
---|---|
In acetonitrile at 60℃; for 24h; | 54% |
Conditions | Yield |
---|---|
In water at 55℃; for 3h; | 54% |
Conditions | Yield |
---|---|
In water at 55℃; for 3h; | 45% |
Conditions | Yield |
---|---|
In water at 55℃; for 3h; | 43% |
Conditions | Yield |
---|---|
With PPA at 140 - 145℃; for 1h; | A 3% B 42% |
Conditions | Yield |
---|---|
With potassium carbonate at 400℃; for 10h; rotating autoclave; | 36% |
Conditions | Yield |
---|---|
In water at 55℃; for 3h; | 32% |
2-naphthalenecarbonitrile
2-naphthalenesulfonic acid sodium salt
bis(2-naphthyl)sulfide
Conditions | Yield |
---|---|
With sodium cyanide durch Schmelzen; |
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