Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:135-88-6
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:135-88-6
Min.Order:1 Kilogram
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Type:Manufacturers
inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:OLED Intermediate Transportation:by air or by sea Port:Shanghai, Qingdao
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:135-88-6
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:135-88-6
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryChemical name: N-Phenyl-2-napthylamine CAS No.: 135-88-6 Molecular Formula: C16H13N Properties: Light gray powder, the melting point 108 °C, the boiling point 395-399.5 °C, the specific gravity 1.18. extremely s
Cas:135-88-6
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquirybest price,best quality and fast delivery assurance available in sample product and customization with years of export experience along with excellent quality, advanced services and competitive prices the quality of products conform u
Cas:135-88-6
Min.Order:10 Gram
Negotiable
Type:Trading Company
inquiryTriumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis: Trading(Raw Mater
Cas:135-88-6
Min.Order:0 Metric Ton
FOB Price: $18.0 / 20.0
Type:Lab/Research institutions
inquirysuperior quality Appearance:light grey powder or crystals Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used as Pharmaceutical Intermediates Tra
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:135-88-6
Min.Order:0 Metric Ton
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:135-88-6
Min.Order:0
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Type:Lab/Research institutions
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:135-88-6
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:135-88-6
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe are leading fine chemicals supplier in China with ISO certificate, Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED
Cas:135-88-6
Min.Order:1 Gram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as
Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard
Cas:135-88-6
Min.Order:1 Kilogram
FOB Price: $112.0
Type:Trading Company
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:135-88-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryAmoychem is committed to providing the top-quality chemical products and services Internationally. We offer our customers with friendly, professional service and reliable, high performance products that have been manufactured according to the accredi
N-(2-Naphthyl)aniline CAS NO.135-88-6 Application:N-(2-Naphthyl)aniline CAS NO.135-88-6
Xiamen Luyunjia Trading Co.,Ltd Package:1kg/bag; 4154kg/drum, or as customer's request. Application:Xiamen Luyunjia Trading Co.,Ltd Transportation:DHL, EMS, FedEx, TNT, AIR, SEA Port:Beijing,Shanghai,Guangzhou ,China main port
1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highl
N-(2-Naphthyl)aniline CAS NO.135-88-6Appearance:light grey powder or crystals Storage:Dry and ventilated Package:Standard or as customer's require Application:intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small am
Cas:135-88-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
Quality assurance, stable process and affordable priceAppearance:detailed see specifications Storage:enquiry Package:according to the clients requirement Application:Pharmaceutical intermediates Transportation:Normal Port:chengdu
Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:135-88-6
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiry2-naphthalenesulfonic acid sodium salt
sodium anilide
N-Phenyl-2-naphthylamine
Conditions | Yield |
---|---|
With aniline at 290℃; for 0.25h; | 99% |
With aniline at 290℃; for 0.25h; Product distribution; other temp.: 190 to 270 deg. C; other reaction time: 0.5 to 12 h; | 99% |
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0); sodium t-butanolate In toluene at 85℃; for 8h; | 99% |
naphthalen-2-yl 1,1,2,2,3,3,4,4,4-nonafluorobutane-1-sulfonate
aniline
N-Phenyl-2-naphthylamine
Conditions | Yield |
---|---|
With tris(dibenzylideneacetone)dipalladium (0); 2,4,6-(i-Pr)3-[2-P(t-Bu)2-phenyl]benzene; 1,8-diazabicyclo[5.4.0]undec-7-ene In toluene at 150℃; for 0.5h; microwave irradiation; | 99% |
Conditions | Yield |
---|---|
With copper(II) acetate monohydrate; triethylamine In acetonitrile at 20℃; for 24h; Chan-Lam Coupling; | 99% |
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); potassium tert-butylate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In 1,4-dioxane at 100℃; for 1.5h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With bis[chloro(1,2,3-trihapto-allylbenzene)palladium(II)]; N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; potassium carbonate at 130℃; for 4h; Schlenk technique; Inert atmosphere; Sealed tube; | 98% |
With N-[2-(di(1-adamantyl)phosphino)phenyl]morpholine; [Pd(π-cinnamyl)Cl]2 at 130℃; for 4h; Schlenk technique; Inert atmosphere; Sealed tube; | 98% |
With NiCl(1-naphthyl)(PPh3)2; sodium hydride; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride In 1,4-dioxane at 110℃; Inert atmosphere; | 75% |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); lithium hexamethyldisilazane; 1,2-bis-(dicyclohexylphosphino)ethane In toluene at 100℃; for 12h; Buchwald-Hartwig Coupling; | 97% |
Conditions | Yield |
---|---|
With di-tert-butyl{2′-isopropoxy-[1,1′-binaphthalen]-2-yl}phosphane; potassium phosphate; palladium diacetate; phenylboronic acid In butan-1-ol at 110℃; for 15h; Inert atmosphere; | 96% |
With (1,3-bis(2,6-diisopropylphenyl)imidazolidene)Ni(styrene)2; lithium tert-butoxide In 1,4-dioxane for 10h; Inert atmosphere; Heating; Schlenk technique; | 93% |
With sodium t-butanolate; 1,3-bis[2,6-diisopropylphenyl]imidazolium chloride; chlorobis(triphenylphosphine)(1-naphthyl)nickel(II) In 1,4-dioxane at 110℃; for 0.5h; | 92% |
Conditions | Yield |
---|---|
With aniline In water | 94% |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)rhodium(I) tetrafluoroborate; sodium t-butanolate; 1,3-diisopropyl-1H-imidazol-3-ium chloride In 1,2-dimethoxyethane at 80℃; for 12h; Inert atmosphere; | 94% |
With [Cu(N,N'-bis(diisopropylphosphino)-N,N'-dimethyl-2,6-diaminopyridine)Br]; potassium tert-butylate In tetrahydrofuran at 110℃; for 16h; Inert atmosphere; Sealed tube; | 86% |
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 40℃; | 82% |
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 40℃; | 82% |
Conditions | Yield |
---|---|
With palladium diacetate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1-methyl-pyrrolidin-2-one at 150℃; for 24h; Inert atmosphere; Sealed vessel; | 94% |
Conditions | Yield |
---|---|
With ethene; 5%-palladium/activated carbon In 5,5-dimethyl-1,3-cyclohexadiene at 150℃; under 760.051 Torr; for 24h; Molecular sieve; Autoclave; | 94% |
With sulfur; oxygen In pyridine; cyclohexane at 110℃; for 24h; Sealed tube; | 63% |
With gold-palladium bimetallic nanoparticles supported on TiO2 In 1,3,5-trimethyl-benzene at 160℃; under 760.051 Torr; for 24h; Inert atmosphere; Schlenk technique; | 66 %Chromat. |
N-(2-naphthyl)-N-phenyl-acetamide
N-Phenyl-2-naphthylamine
Conditions | Yield |
---|---|
With triethyl borane; sodium hydroxide In tert-butyl methyl ether at 80℃; for 6h; Inert atmosphere; Sealed tube; | 92% |
Stage #1: N-(2-naphthyl)-N-phenyl-acetamide With Triethoxysilane; sodium triethylborohydride In tert-butyl methyl ether at 80℃; for 6h; Stage #2: With hydrogenchloride In tert-butyl methyl ether; water at 20℃; for 1h; chemoselective reaction; | 89% |
Multi-step reaction with 2 steps 1: potassium hydroxide; triethyl borane / tetrahydrofuran / 24 h / 25 °C / Inert atmosphere; Schlenk technique; Sealed tube 2: sodium hydroxide; water / tetrahydrofuran / 1 h / 25 °C / Inert atmosphere; Schlenk technique; Sealed tube View Scheme |
2-naphthalenesulfonic acid sodium salt
aniline
A
N-Phenyl-2-naphthylamine
B
β-naphthol
Conditions | Yield |
---|---|
With potassium hydroxide at 230℃; for 6h; Product distribution; other bases: NaOH + K2CO3, NaOH + Na2CO3, NaOH + KCl, NaOH + KF, NaOH; other temp.: 230 to 310 deg. C, other reaction time: 2 to 12 h; | A 90% B 3% |
With sodium hydroxide; potassium carbonate at 310℃; for 4h; | A 34% B 65% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 110℃; for 5.5h; Inert atmosphere; | 90% |
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 80℃; Buchwald-Hartwig Coupling; | 83% |
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 80℃; | 80% |
Conditions | Yield |
---|---|
With PdCl2(N,N’-bis-(2,6-di(iso-propyl)phenyl)imidazolidin-2-ylidene)(AsPh3); potassium tert-butylate In 1,4-dioxane at 110℃; for 4h; Buchwald-Hartwig Coupling; | 88% |
Conditions | Yield |
---|---|
With copper diacetate; triethylamine In dichloromethane at 0 - 5℃; for 4h; Sonication; Green chemistry; | 87% |
With N-(pyrid-2-yl)benzamide; nickel(II) acetate tetrahydrate; N,N,N',N'-tetramethylguanidine In toluene at 60℃; for 24h; Chan-Lam Coupling; | 80% |
With [Cu(4-(dimethylamino)pyridine)4I]I In methanol at 20℃; for 0.25h; Chan-Lam Coupling; | 70% |
Conditions | Yield |
---|---|
Stage #1: β-naphthol With potassium hydroxide In water; toluene at 20℃; Flow reactor; Stage #2: aniline With methanesulfonato(2-dicyclohexylphosphino-3,6-dimethoxy-2',4',6'-tri-i-propyl-1,1'-biphenyl)(2'-methylamino-1,1'-biphenyl-2-yl)palladium(II) In water; toluene at 120℃; Flow reactor; | 85% |
With p-toluene sulfonic acid - choline chloride covalently immobilized on polymeric microspheres coated iron oxide magnetic nanoparticles In neat (no solvent) at 120℃; for 12h; chemoselective reaction; | 81% |
With boron trifluoride diethyl etherate at 80℃; for 15h; Inert atmosphere; | 77% |
chlorobenzene
naphthalen-2-ylamine
A
N-Phenyl-2-naphthylamine
B
1-phenyl-2-aminonaphthalene
Conditions | Yield |
---|---|
With 2,2,6,6-tetramethylpiperidinyl-lithium In diethyl ether; cyclohexane at 25℃; for 24h; Temperature; Solvent; Reagent/catalyst; Inert atmosphere; | A n/a B 84% |
Conditions | Yield |
---|---|
With copper(I) thiophene-2-carboxylate; sodium t-butanolate In dimethyl sulfoxide at 100℃; for 6h; Inert atmosphere; | 83% |
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium t-butanolate In toluene at 120℃; Inert atmosphere; | 43% |
aniline
4,4,5,5-tetramethyl-2-(naphthalen-2-yl)-1,3,2-dioxaborolane
N-Phenyl-2-naphthylamine
Conditions | Yield |
---|---|
With copper diacetate; triethylamine In methanol; acetonitrile at 80℃; for 24h; Chan-Lam Coupling; Molecular sieve; Sealed tube; | 77% |
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid In neat (no solvent) at 120℃; for 48h; Inert atmosphere; Sealed tube; | 75% |
Conditions | Yield |
---|---|
Stage #1: nitrobenzene With [2,2]bipyridinyl; [MoO2Cl2(dmf)2] In toluene for 0.0333333h; Stage #2: naphthalene-2-boronic acid With triphenylphosphine In toluene at 100℃; for 20h; | 74% |
Conditions | Yield |
---|---|
With indium; copper diacetate In methanol at 70℃; for 3h; | 70% |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene In tetrahydrofuran; 1,4-dioxane at 150℃; for 24h; Kumada Cross-Coupling; Inert atmosphere; | 70% |
Conditions | Yield |
---|---|
With hydrogenchloride; iodine; dimethyl sulfoxide In N,N,N,N,N,N-hexamethylphosphoric triamide; water at 110℃; for 20h; Schlenk technique; Sealed tube; Green chemistry; | 69% |
3-[(4-methylphenyl)sulfonyl]-1-phenyltriaz-1-ene
naphthalene-2-boronic acid
N-Phenyl-2-naphthylamine
Conditions | Yield |
---|---|
With 1,8-diazabicyclo[5.4.0]undec-7-ene In toluene at 110℃; for 24h; Molecular sieve; Inert atmosphere; Schlenk technique; | 65% |
phenylhydrazine
naphthalen-2-ylamine
A
N-Phenyl-2-naphthylamine
B
N,1-diphenylnaphthalen-2-amine
Conditions | Yield |
---|---|
With tetrabenzoporphyrinatocobalt(II); copper diacetate In acetonitrile at 0℃; for 13h; chemoselective reaction; | A 57% B 25% |
N-phenyl 2-naphthyl nitroxide
A
2-(phenylamino)naphthoquinone
B
2-(phenylamino)-4-(phenylimino)-1(4H)-naphthalenone
C
N-Phenyl-2-naphthylamine
D
N,N'-diphenyl-(1,1'-binaphthyl)-2,2'-diamine
Conditions | Yield |
---|---|
In benzene for 336h; Ambient temperature; in the dark; Further byproducts given; | A 47% B 2.5% C 40% D 0.5% |
Conditions | Yield |
---|---|
With sulfuric acid; silica gel; sodium nitrite In dichloromethane at 20℃; for 0.25h; | 99% |
With trichloromelamine; silica gel; sodium nitrite In dichloromethane; water at 20℃; for 0.416667h; | 92% |
With Nafion-H(R); silica gel; sodium nitrite In dichloromethane at 20℃; for 0.5h; | 75% |
N-Phenyl-2-naphthylamine
methyl iodide
N-methyl-N-phenylnaphthalen-2-amine
Conditions | Yield |
---|---|
Stage #1: N-Phenyl-2-naphthylamine With n-butyllithium In tetrahydrofuran; hexane at 0℃; for 0.5h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran; hexane at -78 - 20℃; | 99% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; sodium t-butanolate; palladium diacetate In toluene at 100℃; | 98% |
1-ferrocenylmethanol
N-Phenyl-2-naphthylamine
C5H5FeC5H4CH2N(C6H5)(C10H7)
Conditions | Yield |
---|---|
With HClO4 or HBF4 In dichloromethane byproducts: H2O; aq. HClO4 (70 %) or HBF4 (45 %) added (vigorous stirring) to the Fe-complex and the amine; soln. stirred (30 min, room temp.), addn. of ether; ethereal soln. washed twice (water), dried (sodium sulfate), solvent removed (vac.), recrystn. (ethyl acetate); elem. anal.; | 98% |
1,8-dibromopyrene
N-Phenyl-2-naphthylamine
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In o-xylene at 125 - 130℃; for 3.5h; Buchwald-Hartwig Coupling; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; palladium diacetate; caesium carbonate In toluene at 110℃; for 20h; Inert atmosphere; | 96% |
N-Phenyl-2-naphthylamine
N-phenyl-1,2,3,4-tetrahydronaphthalen-2-amine
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate; hydrogen In toluene at 60℃; under 15001.5 Torr; for 6h; Pressure; Solvent; Temperature; Inert atmosphere; Autoclave; | 94% |
With nickel at 100 - 150℃; under 147102 Torr; Hydrogenation; | |
With copper oxide-chromium oxide at 250 - 300℃; under 147102 Torr; Hydrogenation; |
1-Bromonaphthalene
N-Phenyl-2-naphthylamine
N-(naphthalen-2-yl)-N-phenylnaphthalen-1-amine
Conditions | Yield |
---|---|
Stage #1: 1-Bromonaphthalene; N-Phenyl-2-naphthylamine With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In toluene Buchwald-Hartwig Coupling; Inert atmosphere; Sealed tube; Stage #2: With n-hexyllithium In hexane; toluene at 105℃; for 2h; Buchwald-Hartwig Coupling; Inert atmosphere; Sealed tube; | 94% |
With 2-dicyclohexylphosphino-2',6'-dimethoxybiphenyl; n-hexyllithium; palladium diacetate In hexane; toluene at 105℃; for 2h; Buchwald-Hartwig Coupling; Inert atmosphere; | 94% |
N-Phenyl-2-naphthylamine
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate In toluene at 100℃; for 5h; Buchwald-Hartwig Coupling; Inert atmosphere; | 94% |
N-Phenyl-2-naphthylamine
C13H13BrN2O3
Conditions | Yield |
---|---|
With (R)-3,3'-bis(9-anthracenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In dichloromethane at -60℃; for 35h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 94% |
1-ferrocenylethanol
N-Phenyl-2-naphthylamine
C5H5FeC5H4CH(CH3)N(C6H5)(C10H7)
Conditions | Yield |
---|---|
With HClO4 or HBF4 In dichloromethane byproducts: H2O; aq. HClO4 (70 %) or HBF4 (45 %) added (vigorous stirring) to the Fe-complex and the amine; soln. stirred (30 min, room temp.), addn. of ether; ether soln. washed twice (water), dried (sodium sulfate), solvent removed (vac.); elem. anal.; | 93% |
N-Phenyl-2-naphthylamine
C5H5FeC5H4CH(C6H5)N(C6H5)(C10H7)
Conditions | Yield |
---|---|
With HBF4 or HClO4 In dichloromethane byproducts: H2O; aq. HBF4 (45 %) or HClO4 (70 %) added (vigorous stirring) to the Fe-complex and the amine; soln. stirred (30 min, room temp.), addn. of ether; ethereal soln. washed twice (water), dried (sodium sulfate), solvent removed (vac.), recrystn. (heptane); elem. anal.; | 91% |
N-Phenyl-2-naphthylamine
tert-butyl 2-oxoindolin-3-ylidenecarbamate
Conditions | Yield |
---|---|
With (R)-3,3'-bis(9-anthracenyl)-1,1'-binaphthyl-2,2'-diyl hydrogenphosphate In dichloromethane at -60℃; for 24h; Schlenk technique; Inert atmosphere; enantioselective reaction; | 91% |
Conditions | Yield |
---|---|
With sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine In toluene at 90℃; for 3h; | 90% |
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