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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Phosphorous acid

Cas:10294-56-1

Min.Order:1 Kilogram

FOB Price: $3.0

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Phosphorous Acid supplier in China

Cas:10294-56-1

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Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

high quality Phosphorous acid

Cas:10294-56-1

Min.Order:1 Gram

FOB Price: $1.0

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:10294-56-1

Cas:10294-56-1

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Phosphorous Acid

Cas:10294-56-1

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Hangzhou Think Chemical Co. Ltd

HANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & distribution, thinkchem specializes in exp

Phosphorous acid

Cas:10294-56-1

Min.Order:1 Metric Ton

FOB Price: $850.0

Type:Other

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Siwei Development Group Ltd.

Product name: Phosphorous Acid CAS No.: 10294-56-1 Molecule Formula:H3PO3 Molecule Weight:81.99 Purity: 98.0% Package: 25kg/bag Description:White crystals Manufacture Standards:Enterprise Standard TESTING ITEMS

High Purity Phosphorous Acid

Cas:10294-56-1

Min.Order:1 Kilogram

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Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

Phosphorous acid

Cas:10294-56-1

Min.Order:0

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Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

Phosphorous acid 50% aqueous solution

Cas:10294-56-1

Min.Order:0

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Zhuozhou Wenxi import and Export Co., Ltd

Product Description Description & Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard

Hot selling products CAS 10294-56-1 with fast delivery

Cas:10294-56-1

Min.Order:1 Kilogram

FOB Price: $112.0

Type:Trading Company

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HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical Intermediates Tr

Phosphorous acid

Cas:10294-56-1

Min.Order:1 Kilogram

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Hangzhou Fandachem Co.,Ltd

Phosphorous acidAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:pharmaceutical intermediate Transportation:by air, by sea, by express

Phosphorous acid

Cas:10294-56-1

Min.Order:0

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Type:Other

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HENAN SUNLAKE ENTERPRISE CORPORATION

Our Services 1.Certificate Of Analysis (COA) 2.Material Safety Data Sheet (MSDS) 3.Route of synthesis (ROS) 4.Method of Aanlysis (MOA) 5.Nuclear Magnetic Resonance (NMR) 6.Packing pictures and loading video before loading 7.Free Sampl

Phosphorous acid 10294-56-1 H3PO3

Cas:10294-56-1

Min.Order:1 Kilogram

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Hubei Sky Lake Chemical Co., Ltd.

Synonyms: Orthophosphorous acid; phosphonic acid (IUPAC) De: Phosphonsäure ES: Ácido fosfónico Fr:Acide phosphonique Molecular Weight: 81.996 Molecular Formula: H3PO3 Structural Formula: Density: 1.6510 M.P.: 73.6°

Phosphorous acid

Cas:10294-56-1

Min.Order:0 Metric Ton

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Qingdao Sigma Chemical Co., Ltd.

Qingdao Sigma Chemical Ltd is is a global chemical industry manufacturers and suppliers of pharmaceuticals and intermediates, peptide,Nootropis etc API, food and feed additives, herbal extracts, agrochemicals and fine chemicals etc. Our Labo

High Quality Phosphorous acid

Cas:10294-56-1

Min.Order:1 Gram

FOB Price: $1.0

Type:Trading Company

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Xiamen BaiFuchem Co.,Ltd

BaiFuChem is a Professional chemical raw material supplier in China, our main products include Biochemical , Pharma Intermediate and Organic chemical etc. BaiFuChem have wealth of products,experience , expertise and state-of-the-art

Best price Phosphorous Acid

Cas:10294-56-1

Min.Order:1 Kilogram

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XinChem Corporation

We have our own research and development center, provide reliable quality products for you. Port:shanghai

Phosphorous acid

Cas:10294-56-1

Min.Order:1 Kilogram

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Type:Other

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Chungking Joyinchem Co., Ltd.

Joyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom

Phosphorous acid

Cas:10294-56-1

Min.Order:0

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Hangzhou Yierdechem Co. Ltd

With about ten years experiences in the field of pharmaceutical chemicals, Yierdechem has established solid business cooperation relationships with many large companys worldwide.As a leading supplier of API and pharmaceutical intermediates, holds its

Phosphorous acid

Cas:10294-56-1

Min.Order:0

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Type:Other

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Shanghai AngewChem Co., Ltd.

Shanghai AngewChemCo., Ltd. is an innovative enterprise on fine chemicals and pharmaceuticals. Based on Shanghai R&D center and Hunan chemical manufacturing plant, we offer chemical research, process development, and large-scale production. Complete

Phosphorous acid

Cas:10294-56-1

Min.Order:0

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Shanghai Run-Biotech Co., Ltd.

Shanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por

Phosphorous acid

Cas:10294-56-1

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Taian Xiangheng Chemical Imp&Exp Co.,Ltd

1) Product: phosphorous acid 2) Synonyms: orthophosphorous acid; phosphonic acid 3) CAS No.: 10294-56-1 4) Molecular formula: H3PO3 5) Molecul…

Phosphorous acid

Cas:10294-56-1

Min.Order:20 Metric Ton

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Skyrun Industrial Co.,Ltd

SkyRun Industrial CO.,LTD is a leading chemical producer in China. We supply Intermediate, Agro-Chemical and Petrol Chemicals for different usage.SkyRun Industrial CO.,LTD is a leading chemical producer in China. We supply Intermediate, Agro-Chemic

Phosphorous acid

Cas:10294-56-1

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Wuhan Sunrise Pharmaceutical Technology Co., Ltd

Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers. Package:According client's requirements Application:Pharmaceutical Intermediate Transportation:According client's requirements Port:SHA

Phosphorous acid

Cas:10294-56-1

Min.Order:0

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Type:Lab/Research institutions

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Nanjing Raymon Biotech Co., Ltd.

high quality Phosphorous acidAppearance:Colorless to light yellow liquid Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier li

high quality Phosphorous acid

Cas:10294-56-1

Min.Order:0

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Type:Trading Company

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Wuxi Morality Chemical Co., Ltd

Do best quality products, erect the morality model Application:Please email us, thanks

Phosphorous acid

Cas:10294-56-1

Min.Order:0

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Type:Other

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Shanghai Yanchu chemicals Co., Ltd

low price and good quality Application:It is an important raw material and intermediate used in Organic Synthesis, Pharmaceuticals, Agrochemicals and D

Phosphorous acid

Cas:10294-56-1

Min.Order:0

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Hebei Ruishun Trade Co.,Ltd

Supply top quality products with a reasonable price Application:api

10294-56-1

Cas:10294-56-1

Min.Order:0

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Type:Trading Company

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Shanxi Jiuhongjiu Chemical Co.,Ltd

We are a manufactory in chemical industry raw material for 23 years and have a high reputation in China.and we are glad to give you superior quality a…

Phosphorous acid

Cas:10294-56-1

Min.Order:0

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Type:Trading Company

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Henan Qingshuiyuan Technology Co., Ltd

Chemical name: Phosphorous Acid Molecular Formula: H3PO3 Molecular Weight: 82.0 CAS Number:13958-36-2 Typical Properties: …

Phosphorous acid

Cas:10294-56-1

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Synthetic route

phosphorus

phosphorus

phosphorous acid
10294-56-1

phosphorous acid

Conditions
ConditionsYield
With chlorine byproducts: HCl;
silver (I) ion
14701-21-4

silver (I) ion

hypophosphorous acid
6303-21-5

hypophosphorous acid

A

silver
7440-22-4

silver

B

phosphorous acid
10294-56-1

phosphorous acid

Conditions
ConditionsYield
In perchloric acid Kinetics; oxidation hypophosphorous acid with silver(I) in aq. perchloric acid soln. at 30°C;
phosphorus tribromide
7789-60-8

phosphorus tribromide

A

phosphonic Acid
13598-36-2

phosphonic Acid

B

phosphorous acid
10294-56-1

phosphorous acid

Conditions
ConditionsYield
With water In neat (no solvent) formation of H3PO3 and P(OH)3 is proved by UV absorption and mild oxidation of products of hydrolysis;;
hydrogenchloride
7647-01-0

hydrogenchloride

phosphorus

phosphorus

water
7732-18-5

water

butanone
78-93-3

butanone

A

1-hydroxy-1-methylpropylphosphine oxide

1-hydroxy-1-methylpropylphosphine oxide

B

bis(1-hydroxy-1-methylpropyl)phosphine oxide

bis(1-hydroxy-1-methylpropyl)phosphine oxide

C

hypophosphorous acid
6303-21-5

hypophosphorous acid

D

phosphorous acid
10294-56-1

phosphorous acid

Conditions
ConditionsYield
With aluminium for 8h; Inert atmosphere; Schlenk technique; Sealed tube; Electrolysis;
hydrogenchloride
7647-01-0

hydrogenchloride

phosphorus

phosphorus

water
7732-18-5

water

2-Pentanone
107-87-9

2-Pentanone

A

1-hydroxy-1-methylbutylphosphine oxide

1-hydroxy-1-methylbutylphosphine oxide

B

bis(1-hydroxy-1-methylbutyl)phosphine oxide

bis(1-hydroxy-1-methylbutyl)phosphine oxide

C

hypophosphorous acid
6303-21-5

hypophosphorous acid

D

phosphorous acid
10294-56-1

phosphorous acid

Conditions
ConditionsYield
With aluminium for 8h; Inert atmosphere; Schlenk technique; Sealed tube; Electrolysis;
hydrogenchloride
7647-01-0

hydrogenchloride

phosphorus

phosphorus

water
7732-18-5

water

A

phosphoric acid
86119-84-8, 7664-38-2

phosphoric acid

B

hypophosphorous acid
6303-21-5

hypophosphorous acid

C

phosphorous acid
10294-56-1

phosphorous acid

Conditions
ConditionsYield
With 3,3-dimethyl-butan-2-one; aluminium for 8h; Inert atmosphere; Schlenk technique; Sealed tube; Electrolysis;
triphenyl phosphite
101-02-0

triphenyl phosphite

A

phenyl hydrogen phosphonate
2310-89-6

phenyl hydrogen phosphonate

B

phosphorous acid
10294-56-1

phosphorous acid

Conditions
ConditionsYield
With [Pt(H2O)2(1,1'-bis(diphenylphosphanyl)octamethylferrocene)](trifluoromethylsulfonate)2; water In tetrahydrofuran at 20℃; for 8h; Catalytic behavior; Mechanism; Reagent/catalyst; Solvent; Inert atmosphere; Schlenk technique; Sealed tube;
diphenyl hydrogen phosphite
4712-55-4

diphenyl hydrogen phosphite

A

phenyl hydrogen phosphonate
2310-89-6

phenyl hydrogen phosphonate

B

phosphorous acid
10294-56-1

phosphorous acid

Conditions
ConditionsYield
With water In tetrahydrofuran at 20℃; for 0.5h; Inert atmosphere; Schlenk technique; Sealed tube;
tris-(2-chloro, 1-methylethyl)-phosphate
13674-84-5

tris-(2-chloro, 1-methylethyl)-phosphate

A

LACTIC ACID
849585-22-4

LACTIC ACID

B

propylene glycol
57-55-6

propylene glycol

C

1-hydroxypropan-2-yl dihydrogenphosphate
14807-82-0

1-hydroxypropan-2-yl dihydrogenphosphate

D

diisopropylphosphate
1611-31-0

diisopropylphosphate

E

triisopropyl phosphate
513-02-0

triisopropyl phosphate

F

cis-1-chloropropene
16136-84-8

cis-1-chloropropene

G

carbon dioxide
124-38-9

carbon dioxide

H

phosphoric acid
86119-84-8, 7664-38-2

phosphoric acid

I

bis(1-hydroxypropan-2-yl) hydrogenphosphate

bis(1-hydroxypropan-2-yl) hydrogenphosphate

J

chloride
16887-00-6

chloride

K

oxalic acid
144-62-7

oxalic acid

L

hydrogen cation

hydrogen cation

M

Phosphate
14265-44-2

Phosphate

N

isopropyl alcohol
67-63-0

isopropyl alcohol

O

phosphorous acid
10294-56-1

phosphorous acid

Conditions
ConditionsYield
With dihydrogen peroxide In water UV-irradiation;
lauric acid
143-07-7

lauric acid

phosphorus trichloride
7719-12-2, 52843-90-0

phosphorus trichloride

phosphorous acid
10294-56-1

phosphorous acid

Conditions
ConditionsYield
at 63℃; for 3h;
benzylamine
100-46-9

benzylamine

phosphorous acid
10294-56-1

phosphorous acid

dibenzylamine
103-49-1

dibenzylamine

Conditions
ConditionsYield
With benzaldehyde; triethylamine98%
β-naphthol
135-19-3

β-naphthol

phosphorous acid
10294-56-1

phosphorous acid

N-Phenyl-2-naphthylamine
135-88-6

N-Phenyl-2-naphthylamine

Conditions
ConditionsYield
With aniline In water94%
hydrogenchloride
7647-01-0

hydrogenchloride

molybdenum(VI) oxide

molybdenum(VI) oxide

potassium hydroxide

potassium hydroxide

phosphorous acid
10294-56-1

phosphorous acid

1.7K(1+)*0.3H(1+)*HPMo6O21(2-)

1.7K(1+)*0.3H(1+)*HPMo6O21(2-)

Conditions
ConditionsYield
In water at 100℃; for 6h; pH=Ca. 1.5; Temperature; Autoclave;92%
o-toluidine
95-53-4

o-toluidine

phosphorous acid
10294-56-1

phosphorous acid

recorcinol
108-46-3

recorcinol

3-(o-tolylamino)phenol
6264-98-8

3-(o-tolylamino)phenol

Conditions
ConditionsYield
In water90%
tris(4-(1H-imidazol-1-yl)-phenyl)amine
1258947-79-3

tris(4-(1H-imidazol-1-yl)-phenyl)amine

water
7732-18-5

water

zinc(II) oxide

zinc(II) oxide

phosphorous acid
10294-56-1

phosphorous acid

[Zn3(HPO3)3(tris(4-(1H-imidazol-1-yl)phenyl)amine)]·6H2O

[Zn3(HPO3)3(tris(4-(1H-imidazol-1-yl)phenyl)amine)]·6H2O

Conditions
ConditionsYield
With hydrogen fluoride In N,N-dimethyl-formamide at 145℃; for 168h; Autoclave;90%
N-methyltetrahydro-3-thiophenamine 1,1-dioxide hydrochloride

N-methyltetrahydro-3-thiophenamine 1,1-dioxide hydrochloride

phosphorous acid
10294-56-1

phosphorous acid

tetrahydro-N-methyl-N-(phosphonomethyl)-3-thiophenamine 1,1-dioxide

tetrahydro-N-methyl-N-(phosphonomethyl)-3-thiophenamine 1,1-dioxide

Conditions
ConditionsYield
With paraformaldehyde In P2 O5; ethanol; water86.3%
piperazine
110-85-0

piperazine

methanol
67-56-1

methanol

zinc(II) acetate dihydrate
5970-45-6

zinc(II) acetate dihydrate

phosphorous acid
10294-56-1

phosphorous acid

[N,N,N′,N′-tetramethylpiperazinium]0.5[Zn2(HPO3)2(H2PO3)]

[N,N,N′,N′-tetramethylpiperazinium]0.5[Zn2(HPO3)2(H2PO3)]

Conditions
ConditionsYield
In water at 160℃; for 168h; Autoclave; High pressure;82.6%
Ru(NH3)5Cl(2+)*2Cl(1-)=Ru(NH3)5Cl3

Ru(NH3)5Cl(2+)*2Cl(1-)=Ru(NH3)5Cl3

carbon monoxide
201230-82-2

carbon monoxide

water
7732-18-5

water

phosphorous acid
10294-56-1

phosphorous acid

zinc amalgam

zinc amalgam

CH15N4O4PRu(2+)*Cl4Zn(2-)*H2O

CH15N4O4PRu(2+)*Cl4Zn(2-)*H2O

Conditions
ConditionsYield
Stage #1: Ru(NH3)5Cl(2+)*2Cl(1-)=Ru(NH3)5Cl3; water; zinc amalgam With trifluoroacetic acid for 0.666667h; Inert atmosphere;
Stage #2: phosphorous acid for 1h; Inert atmosphere;
Stage #3: carbon monoxide for 5h;
82%
benzylamine
100-46-9

benzylamine

phosphorous acid
10294-56-1

phosphorous acid

N-benzylcyclohexylamine
4383-25-9

N-benzylcyclohexylamine

Conditions
ConditionsYield
80%
iron(II) chloride hexahydrate

iron(II) chloride hexahydrate

sodium hydroxide
1310-73-2

sodium hydroxide

phosphorous acid
10294-56-1

phosphorous acid

2Na(1+)*Fe(2+)*2HPO3(2-)=Na2Fe(HPO3)2

2Na(1+)*Fe(2+)*2HPO3(2-)=Na2Fe(HPO3)2

Conditions
ConditionsYield
With NH3*H2O In water High Pressure; Fe salt, NaOH, H3PO4 and H2O mixed in molar ratio 2:2.5:2.5:667, treatedwith NH3*H2O soln. to pH=7.0, sealed in stainless sleel autoclave, heat ed at 433 K for 5 d; filtered, washed (ethanol), dried at room temp., XRD, elem. anal.;80%
phosphorous acid
10294-56-1

phosphorous acid

iminodiacetic acid
142-73-4

iminodiacetic acid

phosphonomethylimino-di-acetic acid
5994-61-6

phosphonomethylimino-di-acetic acid

Conditions
ConditionsYield
With formaldehyd; sulfuric acid78.2%
With formaldehyd; sulfuric acid75.3%
With formaldehyd; sulfuric acid74.2%
With formaldehyd; sulfuric acid In water59.8%
zinc(II) nitrate hexahydrate

zinc(II) nitrate hexahydrate

1,12-Diaminododecane
2783-17-7

1,12-Diaminododecane

terephthalic acid
100-21-0

terephthalic acid

hydrogen fluoride
7664-39-3

hydrogen fluoride

phosphorous acid
10294-56-1

phosphorous acid

(H2DIA)Zn2(1,4-benzenedicarboxylate)(HPO3)2

(H2DIA)Zn2(1,4-benzenedicarboxylate)(HPO3)2

Conditions
ConditionsYield
In water; N,N-dimethyl-formamide at 150℃; for 48h;78%
methanol
67-56-1

methanol

zinc(II) acetate dihydrate
5970-45-6

zinc(II) acetate dihydrate

(RS)-2-methylpiperazine
109-07-9

(RS)-2-methylpiperazine

phosphorous acid
10294-56-1

phosphorous acid

[N,N,N’,N’-tetramethyl-2-methylpiperazinium][Zn3(HPO3)4]

[N,N,N’,N’-tetramethyl-2-methylpiperazinium][Zn3(HPO3)4]

Conditions
ConditionsYield
In water at 155℃; for 168h; Autoclave;77.4%
Thiophene-2,5-dicarboxylic acid
4282-31-9

Thiophene-2,5-dicarboxylic acid

zinc(II) nitrate hexahydrate

zinc(II) nitrate hexahydrate

1,12-Diaminododecane
2783-17-7

1,12-Diaminododecane

phosphorous acid
10294-56-1

phosphorous acid

C12H28N2*2HO3P(2-)*C6H2O4S(2-)*2H(1+)*2Zn(2+)

C12H28N2*2HO3P(2-)*C6H2O4S(2-)*2H(1+)*2Zn(2+)

Conditions
ConditionsYield
In water; N,N-dimethyl-formamide at 150℃; for 48h; Autoclave;76%
1,4-diazabicyclo[2.2.2]octane hexahydrate

1,4-diazabicyclo[2.2.2]octane hexahydrate

zinc(II) acetate dihydrate
5970-45-6

zinc(II) acetate dihydrate

phosphorous acid
10294-56-1

phosphorous acid

Zn(dabco)0.5(HPO3)

Zn(dabco)0.5(HPO3)

Conditions
ConditionsYield
In ethanol; water at 160℃; for 216h;72.1%
1-(N-morpholino)cyclopent-1-ene
936-52-7

1-(N-morpholino)cyclopent-1-ene

phosphorous acid
10294-56-1

phosphorous acid

N-cyclopentylmorpholine
39198-78-2

N-cyclopentylmorpholine

Conditions
ConditionsYield
72%
4,4'-bipyridine dihydrate

4,4'-bipyridine dihydrate

vanadia

vanadia

phosphorous acid
10294-56-1

phosphorous acid

(VO)4((4,4'-bipyridine)2(HPO3)4

(VO)4((4,4'-bipyridine)2(HPO3)4

Conditions
ConditionsYield
With (CH3)4NOH*5H2O In water High Pressure; mixt. of V2O5, H3PO3, bipyridine, (CH3)4NOH*5H2O and distd. H2O (ratio 1:10:2:8:555) heated at 160°C for 120 h; washed (distd. H2O), filtered, dried in air; elem. anal.;72%
cobalt(II) chloride hexahydrate

cobalt(II) chloride hexahydrate

sodium hydroxide
1310-73-2

sodium hydroxide

phosphorous acid
10294-56-1

phosphorous acid

2Na(1+)*Co(2+)*2HPO3(2-)=Na2Co(HPO3)2

2Na(1+)*Co(2+)*2HPO3(2-)=Na2Co(HPO3)2

Conditions
ConditionsYield
With NH3*H2O In water High Pressure; Co salt, NaOH, H3PO4 and H2O mixed in molar ratio 2:2.5:2.5:667, treatedwith NH3*H2O soln. to pH=7.0, sealed in stainless sleel autoclave, heat ed at 433 K for 5 d; filtered, washed (ethanol), dried at room temp., XRD, elem. anal.;70%
dimethyl 6,6′-([ethane-1,2-diylbis{azanediyl}]bis[methylene])dipicolinate
761411-41-0

dimethyl 6,6′-([ethane-1,2-diylbis{azanediyl}]bis[methylene])dipicolinate

phosphorous acid
10294-56-1

phosphorous acid

N,N'-(methylphosphonate)-N,N'-[[6-(methoxycarbonyl)pyridin-2-yl]methyl]-1,2-diaminoethane

N,N'-(methylphosphonate)-N,N'-[[6-(methoxycarbonyl)pyridin-2-yl]methyl]-1,2-diaminoethane

Conditions
ConditionsYield
With 1,3,5-Trioxan; hydrogenchloride Reflux;70%
tris(4-(1H-imidazol-1-yl)-phenyl)amine
1258947-79-3

tris(4-(1H-imidazol-1-yl)-phenyl)amine

water
7732-18-5

water

zinc(II) oxide

zinc(II) oxide

phosphorous acid
10294-56-1

phosphorous acid

[Zn2(HPO3)2(tris(4-(1H-imidazol-1-yl)phenyl)amine)]·2H2O

[Zn2(HPO3)2(tris(4-(1H-imidazol-1-yl)phenyl)amine)]·2H2O

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 145℃; for 168h; Autoclave;70%
1,4-diaza-bicyclo[2.2.2]octane
280-57-9

1,4-diaza-bicyclo[2.2.2]octane

methanol
67-56-1

methanol

zinc(II) oxide

zinc(II) oxide

phosphorous acid
10294-56-1

phosphorous acid

[N,N'-dimethyl-1,4-diazabicyclo[2,2,2]octane][Zn3(HPO3)4]

[N,N'-dimethyl-1,4-diazabicyclo[2,2,2]octane][Zn3(HPO3)4]

Conditions
ConditionsYield
In water at 160℃; for 168h; Autoclave;68.7%
sodium molybdate dihydrate
7631-95-0

sodium molybdate dihydrate

1,3,5,-tris(4-carboxyphenyl)benzene
50446-44-1

1,3,5,-tris(4-carboxyphenyl)benzene

tetra(n-butyl)ammonium hydroxide
2052-49-5

tetra(n-butyl)ammonium hydroxide

zinc(II) chloride
7646-85-7

zinc(II) chloride

phosphorous acid
10294-56-1

phosphorous acid

molybdenum
7439-98-7

molybdenum

[tetrabutylammonium]3[ε-PMoV8MoVI4O36(OH)4Zn4][benzene tribenzoate]4/3

[tetrabutylammonium]3[ε-PMoV8MoVI4O36(OH)4Zn4][benzene tribenzoate]4/3

Conditions
ConditionsYield
With hydrogenchloride In water at 180℃; for 72h; pH=4.8; Autoclave;68%
sodium molybdate dihydrate
7631-95-0

sodium molybdate dihydrate

zinc(II) acetate dihydrate
5970-45-6

zinc(II) acetate dihydrate

trans-1,2-bis(pyridin-4-yl)ethene
13362-78-2

trans-1,2-bis(pyridin-4-yl)ethene

tetrapropylammonium hydroxide
4499-86-9

tetrapropylammonium hydroxide

phosphorous acid
10294-56-1

phosphorous acid

molybdenum
7439-98-7

molybdenum

Mo12O40PH3Zn4*3C12H10N2

Mo12O40PH3Zn4*3C12H10N2

Conditions
ConditionsYield
Stage #1: sodium molybdate dihydrate; zinc(II) acetate dihydrate; trans-1,2-bis(pyridin-4-yl)ethene; tetrapropylammonium hydroxide; phosphorous acid; molybdenum In water for 1h; Sealed tube;
Stage #2: With hydrogenchloride In water for 0.5h; pH=4.2; Sealed tube;
Stage #3: In water at 180℃; for 72h; Sealed tube;
67.11%
gallium(III) sulfate

gallium(III) sulfate

potassium carbonate
584-08-7

potassium carbonate

phosphorous acid
10294-56-1

phosphorous acid

2HO3P(2-)*Ga(3+)*K(1+)

2HO3P(2-)*Ga(3+)*K(1+)

Conditions
ConditionsYield
In water at 179.84℃; for 72h; High pressure; Autoclave;67%
rubidium carbonate

rubidium carbonate

gallium(III) sulfate

gallium(III) sulfate

phosphorous acid
10294-56-1

phosphorous acid

2HO3P(2-)*Ga(3+)*Rb(1+)

2HO3P(2-)*Ga(3+)*Rb(1+)

Conditions
ConditionsYield
In water at 179.84℃; for 72h; High pressure; Autoclave;67%
gallium(III) sulfate

gallium(III) sulfate

ammonium carbonate
506-87-6

ammonium carbonate

phosphorous acid
10294-56-1

phosphorous acid

H2O3P(1-)*Ga(3+)*H3N*HO3P(2-)

H2O3P(1-)*Ga(3+)*H3N*HO3P(2-)

Conditions
ConditionsYield
In water at 179.84℃; for 72h; High pressure; Autoclave;67%
zinc(II) nitrate hexahydrate

zinc(II) nitrate hexahydrate

n-Octylamine
111-86-4

n-Octylamine

terephthalic acid
100-21-0

terephthalic acid

hydrogen fluoride
7664-39-3

hydrogen fluoride

phosphorous acid
10294-56-1

phosphorous acid

(HOCA)Zn(1,4-benzenedicarboxylate)0.5(HPO3)

(HOCA)Zn(1,4-benzenedicarboxylate)0.5(HPO3)

Conditions
ConditionsYield
In water; N,N-dimethyl-formamide at 150℃; for 48h;67%
K[Gd(ethylenediaminetetraacetate)(trihydrate)]*5H2O

K[Gd(ethylenediaminetetraacetate)(trihydrate)]*5H2O

phosphorous acid
10294-56-1

phosphorous acid

K3n[Gd(ethylenediaminetetraacetate)(phosphite)]n*7nH2O

K3n[Gd(ethylenediaminetetraacetate)(phosphite)]n*7nH2O

Conditions
ConditionsYield
With potassium hydroxide In water at 70℃; for 168h; pH=7.2;65%
1,4-diaza-bicyclo[2.2.2]octane
280-57-9

1,4-diaza-bicyclo[2.2.2]octane

cobalt(II) chloride hexahydrate

cobalt(II) chloride hexahydrate

phosphorous acid
10294-56-1

phosphorous acid

Co(2+)*2HO3P(2-)*C6H12N2*2H(1+)

Co(2+)*2HO3P(2-)*C6H12N2*2H(1+)

Conditions
ConditionsYield
Stage #1: 1,4-diaza-bicyclo[2.2.2]octane; cobalt(II) chloride hexahydrate In N,N-dimethyl-formamide for 3h;
Stage #2: phosphorous acid In N,N-dimethyl-formamide at 60℃; for 72h; Sealed tube;
65%
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