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Cas:50446-44-1
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inquiryProduct Name: 1,3,5-Tri(4-carboxyphenyl)benzene Synonyms: 4-[3,5-bis(4-carboxyphenyl)phenyl]benzoic acid;1,3,5-Tri(4-carboxyphenyl)benzene;1,3,5-Tris(4-carboxyphenyl)benzene >=98%, <=20 wt. % solvent;H3BTB;4',4'',4''&#
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inquiry1,3,5-Tri(4-carboxyphenyl)benzene CAS:50446-44-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiryShanghai Massive Chemical Technology Co., Ltd. is engaged in development, production and marketing Specialty Chemicals to satisfy the changing needs of the chemical industry. We specialize in manufacturing high quality of Advanced Intermediates, Sp
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.
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inquirybulk productiongoods in stockswe have the best competitive price in the marketmeantime,we are committed to service to our every customer Chemsigma International Co.,Ltd. is a chemical manufacturer, specialize in custom synthesis and organic chemical
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiry1,3,5-Tri(4-carboxyphenyl)benzene cas 50446-44-1Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryWe product this chemical more than 797 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Organic catalyst
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inquiryR & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
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inquirygood quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:250mg Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any po
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryOur company's tenet is to treat every customer sincerely and be responsible for every product. The production of products according to customer demand for customized, in strict accordance with strict requirements, the production of products always wi
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inquiryBest Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP
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inquiry1,3,5-tris(4-methyl-phenyl)-benzene
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
With pyridine; ammonium cerium (IV) nitrate; dihydrogen peroxide; sodium carbonate; cobalt(II) nitrate at 110℃; under 15001.5 Torr; for 6h; Reagent/catalyst; Temperature; Pressure; Green chemistry; | 97% |
With 2-aminoisonicotinic acid; oxygen; antimony(III) acetate; acetic anhydride; acetic acid; potassium nitrate; 1-aza-adamantane-1-oxide; Dimethyl succinate In 1,2-dichloro-benzene at 180℃; under 7500.75 Torr; for 12h; Reagent/catalyst; Solvent; Temperature; Pressure; | 92% |
With dihydrogen peroxide; sodium carbonate at 100℃; under 7500.75 Torr; for 12h; Reagent/catalyst; Solvent; | 90% |
With nitric acid at 160 - 180℃; im geschlossenen Rohr; | |
With nitric acid at 170℃; |
dimethyl 5'-(4-(methoxycarbonyl)phenyl)-[1,1:3,1''-terphenyl]-4,4''-dicarboxylate
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
With methanol; sodium hydroxide In tetrahydrofuran | 92% |
With water; sodium hydroxide In tetrahydrofuran; methanol | 92% |
With water; sodium hydroxide In tetrahydrofuran; methanol | 92% |
carbon dioxide
1,3,5-tris(4-hydroxyphenyl)benzene
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
bis-triphenylphosphine-palladium(II) chloride In N,N-dimethyl-formamide at 90℃; electrochemical reaction; | 75% |
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
With bromine; sodium hydroxide In 1,4-dioxane; water at 60℃; for 2h; | 75% |
With sodium hypobromide In 1,4-dioxane at 60℃; for 2h; |
carbon dioxide
1,3,5-tris(4-bromophenyl)benzene
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; hexane at -60℃; | 60% |
Stage #1: 1,3,5-tris(4-bromophenyl)benzene With n-butyllithium In tetrahydrofuran; hexane at -60℃; Stage #2: carbon dioxide In tetrahydrofuran; hexane at -60 - 20℃; | 57% |
Stage #1: 1,3,5-tris(4-bromophenyl)benzene With n-butyllithium In tetrahydrofuran; hexane at -60℃; Inert atmosphere; Stage #2: carbon dioxide at -60℃; | 33% |
Stage #1: 1,3,5-tris(4-bromophenyl)benzene With n-butyllithium In tetrahydrofuran; hexane at -65 - -60℃; for 1h; Inert atmosphere; Stage #2: carbon dioxide With hydrogenchloride In tetrahydrofuran; hexane; water at -65 - -60℃; for 1h; Inert atmosphere; | 0.29 g |
carbon dioxide
1,3,5-tris(4-hydroxyphenyl)benzene
A
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
bis-triphenylphosphine-palladium(II) chloride In N,N-dimethyl-formamide at 90℃; electrochemical reaction; | A 43% B 34% |
Conditions | Yield |
---|---|
at 125℃; for 72h; Title compound not separated from byproducts.; |
4-acetophenyl triflate
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 97 percent / triflic acid / 1.5 h / 140 - 150 °C / in vacuo 2: 67 percent / dimethylformamide / Ambient temperature; electrolysis 3: 75 percent / PdCl2(PPh3)2 / dimethylformamide / 90 °C / electrochemical reaction View Scheme | |
Multi-step reaction with 3 steps 1: 97 percent / triflic acid / 1.5 h / 140 - 150 °C / in vacuo 2: 67 percent / dimethylformamide / Ambient temperature; electrolysis 3: 43 percent / PdCl2(PPh3)2 / dimethylformamide / 90 °C / electrochemical reaction View Scheme |
4-Hydroxyacetophenone
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: triethylamine / CH2Cl2 / -50 deg C (1 h) to r.t (8 h) 2: 97 percent / triflic acid / 1.5 h / 140 - 150 °C / in vacuo 3: 67 percent / dimethylformamide / Ambient temperature; electrolysis 4: 75 percent / PdCl2(PPh3)2 / dimethylformamide / 90 °C / electrochemical reaction View Scheme | |
Multi-step reaction with 4 steps 1: triethylamine / CH2Cl2 / -50 deg C (1 h) to r.t (8 h) 2: 97 percent / triflic acid / 1.5 h / 140 - 150 °C / in vacuo 3: 67 percent / dimethylformamide / Ambient temperature; electrolysis 4: 43 percent / PdCl2(PPh3)2 / dimethylformamide / 90 °C / electrochemical reaction View Scheme |
1,3,5-tris[4-[(trifluoromethanesulfonyl)oxy]phenyl]benzene
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 67 percent / dimethylformamide / Ambient temperature; electrolysis 2: 75 percent / PdCl2(PPh3)2 / dimethylformamide / 90 °C / electrochemical reaction View Scheme | |
Multi-step reaction with 2 steps 1: 67 percent / dimethylformamide / Ambient temperature; electrolysis 2: 43 percent / PdCl2(PPh3)2 / dimethylformamide / 90 °C / electrochemical reaction View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 41 percent / triethyl orthoformate 2: 60 percent / 1.6 M n-BuLi / tetrahydrofuran; hexane / -60 °C View Scheme |
methyl 4-acetylbenzoate
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: toluene-4-sulfonic acid; toluene View Scheme | |
Multi-step reaction with 2 steps 1: toluene View Scheme |
toluene-4-sulfonic acid
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: toluene View Scheme |
para-methylacetophenone
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogen chloride 2: nitric acid / 160 - 180 °C / im geschlossenen Rohr View Scheme |
para-methylacetophenone
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: AlCl3 / 210 °C 2: aq. HNO3 / 170 °C View Scheme |
C33H30O6
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
With water; sodium hydroxide | 1.18 g |
carbon dioxide
para-bromoacetophenone
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
Stage #1: para-bromoacetophenone Stage #2: With n-butyllithium Stage #3: carbon dioxide |
para-bromoacetophenone
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sulfuric acid; potassium hydrogensulfate / 18 h / 180 °C 1.2: 7 h / Reflux 2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -65 - -60 °C / Inert atmosphere 2.2: 1 h / -65 - -60 °C / Inert atmosphere View Scheme |
1,3,5-trisbromobenzene
4-methoxycarbonylphenylboronic acid
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: cesium fluoride; tetrakis(triphenylphosphine) palladium(0) / 1,2-dimethoxyethane / 48 h / Schlenk technique; Inert atmosphere; Reflux 2: methanol; sodium hydroxide / tetrahydrofuran View Scheme | |
Multi-step reaction with 2 steps 1: tetrakis(triphenylphosphine) palladium(0); cesium fluoride / 1,2-dimethoxyethane / 48 h / Schlenk technique; Inert atmosphere; Reflux 2: water; sodium hydroxide / tetrahydrofuran; methanol View Scheme |
4-methoxycarbonylphenylboronic acid
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol / 4 h / 110 °C / 6000.6 Torr / Inert atmosphere; Microwave irradiation 2: sodium hydroxide / tetrahydrofuran; methanol / 16 h / 20 °C View Scheme |
4-carboxyphenylboronic acid
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: thionyl chloride / 2.5 h / 50 °C / Inert atmosphere 2: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol / 4 h / 110 °C / 6000.6 Torr / Inert atmosphere; Microwave irradiation 3: sodium hydroxide / tetrahydrofuran; methanol / 16 h / 20 °C View Scheme |
4,4'-bipyridine
1,3,5,-tris(4-carboxyphenyl)benzene
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
at 100℃; for 72h; | 95.2% |
1,3,5,-tris(4-carboxyphenyl)benzene
cobalt(II) chloride
Conditions | Yield |
---|---|
In methanol at 85℃; for 12h; | 95% |
1,3,5,-tris(4-carboxyphenyl)benzene
water
Conditions | Yield |
---|---|
Stage #1: europium(III) nitrate hexahydrate; 1,3,5,-tris(4-carboxyphenyl)benzene With 3-ethyl-1-methyl-1H-imidazol-3-ium bromide at 100℃; Heating; Stage #2: water In N,N-dimethyl-formamide at 160℃; for 72h; Reagent/catalyst; Solvent; Autoclave; | 94% |
In N,N-dimethyl-formamide at 150℃; for 72h; High pressure; Autoclave; | 44% |
1,3,5,-tris(4-carboxyphenyl)benzene
water
Conditions | Yield |
---|---|
Stage #1: terbium(III) nitrate hexahydrate; 1,3,5,-tris(4-carboxyphenyl)benzene With 3-ethyl-1-methyl-1H-imidazol-3-ium bromide at 100℃; Heating; Stage #2: water In N,N-dimethyl-formamide at 160℃; for 72h; Reagent/catalyst; Solvent; Autoclave; | 94% |
Conditions | Yield |
---|---|
With (S)-Malic acid at 100℃; | 94% |
4,4'-bipyridine
1,3,5,-tris(4-carboxyphenyl)benzene
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
at 100℃; for 72h; | 93.5% |
1,3,5,-tris(4-carboxyphenyl)benzene
water
1,4-bis(4-pyridyl)benzene
N,N-dimethyl-formamide
cobalt(II) chloride
Conditions | Yield |
---|---|
at 120℃; for 72h; pH=5; Autoclave; High pressure; | 92% |
1,4-diaza-bicyclo[2.2.2]octane
1,3,5,-tris(4-carboxyphenyl)benzene
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
With HCl In 1,4-dioxane; water; N,N-dimethyl-formamide High Pressure; mixt. Cu(NO3)2*3H2O, (1,1':3',1''-terphenyl)-4,4'',5'-tricarboxylic acid, DABCO, concd. HCl, DMF, dioxane and water was treated by ultrasonic vibration, sealed in Teflon-lined stainless steel container and heated at 358 K for 3 days; react. mixt. was cooled to room temp.; elem. anal.; | 90% |
1,3,5,-tris(4-carboxyphenyl)benzene
water
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
at 100℃; for 120h; Sonication; | 90% |
1,3,5,-tris(4-carboxyphenyl)benzene
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
at 80℃; for 48h; Autoclave; High pressure; | 90% |
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide at 100℃; for 72h; High pressure; Autoclave; | 88% |
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
In ethanol; water; N,N-dimethyl-formamide at 130℃; for 24h; Autoclave; | 87% |
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide at 100℃; for 72h; High pressure; Autoclave; | 87% |
lithium hydroxide monohydrate
1,3,5,-tris(4-carboxyphenyl)benzene
nickel(II) acetate tetrahydrate
cobalt(II) diacetate tetrahydrate
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In water at 20℃; for 48h; Sealed tube; | 86% |
1,3,5,-tris(4-carboxyphenyl)benzene
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
With lithium hydroxide monohydrate In water at 130℃; for 72h; Autoclave; High pressure; | 85% |
1,10-Phenanthroline
1,3,5,-tris(4-carboxyphenyl)benzene
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In water at 100℃; for 72h; Autoclave; | 85% |
Conditions | Yield |
---|---|
at 90℃; for 72h; Sealed tube; | 85% |
1,3,5,-tris(4-carboxyphenyl)benzene
water
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
at 90℃; for 72h; | 85% |
1,3,5,-tris(4-carboxyphenyl)benzene
water
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
at 80℃; for 48h; Autoclave; High pressure; | 85% |
lithium hydroxide monohydrate
N,N-dimethyl acetamide
1,3,5,-tris(4-carboxyphenyl)benzene
water
Conditions | Yield |
---|---|
at 130℃; for 72h; Autoclave; | 83% |
lithium hydroxide monohydrate
1,3,5,-tris(4-carboxyphenyl)benzene
nickel(II) acetate tetrahydrate
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In water at 20℃; for 48h; Sealed tube; | 82% |
1-methyl-pyrrolidin-2-one
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
With water; calcium chloride at 120℃; for 120h; Autoclave; | 82% |
1-hydroxy-pyrrolidine-2,5-dione
1,3,5,-tris(4-carboxyphenyl)benzene
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 24h; Inert atmosphere; | 82% |
1,3,5,-tris(4-carboxyphenyl)benzene
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
Stage #1: cobalt(II) nitrate hexahydrate; 1,3,5,-tris(4-carboxyphenyl)benzene; 1,7-bis{(pyridin-4′-yl)methanol}-1,7-dicarba-closo-dodecaborane; N,N-dimethyl-formamide With air In ethanol; water Sonication; Stage #2: With air In ethanol; water at 100℃; for 48h; | 81.7% |
Conditions | Yield |
---|---|
With zinc(II) nitrate at 100℃; for 16h; | 81% |
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