As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for
Cas:2783-17-7
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inquiryProduct Description Product website: http://www.finerchem.com Product Name 1,12-Dodecanediamine CAS No. 220-
Cas:2783-17-7
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryProduct Name: 1,12-Dodecanediamine Synonyms: 1,12-DODECAMETHYLENEDIAMINE;1,12-DODECANEDIAME;1,12-DODECANEDIAMINE;1,12-DIAMINODODECANE;DODECAMETHYLENEDIAMINE;DODECANEDIAMINE;DODECANEDIAMINE(1,12-);RARECHEM AL BW 0116 CAS: 2783-17-
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Min.Order:1 Kilogram
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inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
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We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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Min.Order:1 Metric Ton
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
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Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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Conditions | Yield |
---|---|
With hydrogen; sodium methylate In methanol at 130℃; under 37503.8 Torr; for 5h; | 91.7% |
With lithium aluminium tetrahydride | |
With triisobutylaluminum |
1,12-diazido-dodecane
1,12-Diaminododecane
Conditions | Yield |
---|---|
With cerium(III) chloride; sodium iodide In acetonitrile for 24h; Heating; | 55% |
With trimethylphosphane In water-d2 at 20℃; for 25h; Staudinger Azide Reduction; |
Conditions | Yield |
---|---|
In water-d2 at 24.85℃; pH=7.3; Equilibrium constant; Decomposition; |
Conditions | Yield |
---|---|
In water-d2 at 24.85℃; pH=7.3; Equilibrium constant; Decomposition; |
1,12-Diaminododecane
Conditions | Yield |
---|---|
With ethanol; sodium |
1,12-Diaminododecane
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
With tris-(2-chloro-ethyl)-amine; sulfuric acid at 35 - 45℃; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dimethylformamide 2: H2, NH3 / Raney-Ni / methanol View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Na / methanol / (electrolysis) 2: dimethylformamide 3: H2, NH3 / Raney-Ni / methanol View Scheme |
dodecanedial
1,12-Diaminododecane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: ozone / acetic acid methyl ester / 1.5 h / 5 °C 1.2: 15 - 20 °C 2.1: 5%-palladium/activated carbon; hydrogen / acetic acid methyl ester; water / 5.5 h / 15 - 25 °C / 11103.3 Torr / Autoclave 3.1: ammonium hydroxide / water; isopropyl alcohol / 10 - 60 °C / 31789.8 Torr / Autoclave View Scheme | |
Multi-step reaction with 3 steps 1.1: ozone / acetic acid methyl ester / 1.67 h / 4.9 °C 1.2: 15 - 20 °C 2.1: 5%-palladium/activated carbon; hydrogen / acetic acid methyl ester; water / 5.5 h / 15 - 25 °C / 11103.3 Torr / Autoclave 3.1: ammonium hydroxide / water; isopropyl alcohol / 10 - 60 °C / 31789.8 Torr / Autoclave View Scheme | |
Multi-step reaction with 3 steps 1.1: ozone / 3.5 h / 5 °C 1.2: 5 - 20 °C 2.1: 5%-palladium/activated carbon; hydrogen / acetic acid methyl ester; water / 5.5 h / 15 - 25 °C / 11103.3 Torr / Autoclave 3.1: ammonium hydroxide / water; isopropyl alcohol / 10 - 60 °C / 31789.8 Torr / Autoclave View Scheme |
dodeca-4,8-diene-1,12-dialdehyde
1,12-Diaminododecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 5%-palladium/activated carbon; hydrogen / acetic acid methyl ester; water / 5.5 h / 15 - 25 °C / 11103.3 Torr / Autoclave 2: ammonium hydroxide / water; isopropyl alcohol / 10 - 60 °C / 31789.8 Torr / Autoclave View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: acetic acid; ozone / 2.5 h / 5 °C / Inert atmosphere 1.2: 2 h / 10 - 20 °C 2.1: ammonium hydroxide / water; isopropyl alcohol / 60 °C / 11103.3 - 31789.8 Torr / Inert atmosphere; Autoclave View Scheme | |
Multi-step reaction with 2 steps 1.1: ozone / acetic acid methyl ester / 4.4 °C / Inert atmosphere 1.2: 20 °C 2.1: ammonium hydroxide / water; isopropyl alcohol / 60 °C / 11103.3 - 31789.8 Torr / Inert atmosphere; Autoclave View Scheme |
1,12-Diaminododecane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: trifluoroacetic acid / 5 h / 20 °C 2.1: trimethylphosphane / water-d2; deuteromethanol / 25 h 2.2: 24 h View Scheme |
12-azidododecan-1-amine
1,12-Diaminododecane
Conditions | Yield |
---|---|
Stage #1: 12-azidododecan-1-amine With trimethylphosphane In deuteromethanol; water-d2 for 25h; Staudinger Azide Reduction; Stage #2: for 24h; |
N-(tent-butoxycarbonyl)-12-bromododecylamine
1,12-Diaminododecane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium azide / N,N-dimethyl-formamide / 20 h / 85 °C 2.1: trifluoroacetic acid / 5 h / 20 °C 3.1: trimethylphosphane / water-d2; deuteromethanol / 25 h 3.2: 24 h View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C 2: tris(2,4-pentanedionato)ruthenium(III); [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine]; hydrogen; ammonia / 1,4-dioxane; water / 20 h / 220 °C / 7500.75 Torr / Autoclave; Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: ammonium / 0.5 h / Heating 2: phosphorus pentoxide / 1 h / 15 - 37.5 Torr / Heating 3: hydrogen / ethanol / 1 h / 100 °C / 60006 Torr View Scheme | |
Multi-step reaction with 3 steps 1: ammonium / 0.5 h / Heating 2: 1 h / 15 - 37.5 Torr / Heating 3: hydrogen / ethanol / 1 h / 100 °C / 60006 Torr View Scheme |
Conditions | Yield |
---|---|
With tris(2,4-pentanedionato)ruthenium(III); ammonia; hydrogen; [2-((diphenylphospino)methyl)-2-methyl-1,3-propanediyl]bis[diphenylphosphine] In 1,4-dioxane; water at 220℃; under 7500.75 Torr; for 20h; Temperature; Autoclave; Inert atmosphere; | 87 %Spectr. |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: phosphorus pentoxide / 1 h / 315 °C / 15001.5 - 37503.8 Torr 2: hydrogen / ethanol / 1 h / 100 °C / 60006 Torr View Scheme | |
Multi-step reaction with 2 steps 1: phosphorus pentoxide / 1 h / 15 - 37.5 Torr / Heating 2: hydrogen / ethanol / 1 h / 100 °C / 60006 Torr View Scheme | |
Multi-step reaction with 2 steps 1: 1 h / 15 - 37.5 Torr / Heating 2: hydrogen / ethanol / 1 h / 100 °C / 60006 Torr View Scheme |
Conditions | Yield |
---|---|
With pyridoxal 5'-phosphate; MATITNHMPTAELQALDAAHHLHPFSANNALGEEGTRVITRARGVWLNDSEGEEILDAMAGLWCVNIGYGRDELAEVAARQMRELPYYNTFFKTTHVPAIALAQKLAELAPGDLNHVFFAGGGSEANDTNIRMVRTYWQNKGQPEKTVIISRKNAYHGSTVASSALGGMAGMHAQSGLIPDVHHINQPNWWAEGGDMDPEEFGLARARELEEAILELGENRVAAFIAEPVQGAGGVIVAPDSYWPEIQRICDKYDILLIADEVICGFGRTGNWFGTQTMGIRPHIMTIAKGLSSGYAPIGGSIVCDEVAHVIGKDEFNHGYTYSGHPVAAAVALENLRILEEENILDHVRNVAAPYLKEKWEALTDHPLVGEAKIVGMMASIALTPNKASRAKFASEPGTIGYICRERCFANNLIMRHVGDRMIISPPLVITPAEIDEMFVRIRKSLDEAQAEIEKQGLMKSA; MIKAYAALEANGKLQPFEYDPGALGANEVEIEVQYCGVCHSDLSMINNEWGISNYPLVPGHEVVGTVAAMGEGVNHVEVGDLVGLGWHSGYCMTCHSCLSGYHNLCATAESTIVGHYGGFGDRVRAKGVSVVKLPKGIDLASAGPLFCGGITVFSPMVELSLKPTAKVAVIGIGGLGHLAVQFLRAWGCEVTAFTSSARKQTEVLELGAHHILDSTNPEAIASAEGKFDYIISTVNLKLDWNLYISTLAPQGHFHFVGVVLEPLDLNLFPLLMGQRSVSASPVGSPATIATMLDFAVRHDIKPVVEQFSFDQINEAIAHLESGKAHYRVVLSHSKN; nicotinamide adenine dinucleotide phosphate; benzylamine In dimethyl sulfoxide at 37℃; for 24h; pH=8; Solvent; Microbiological reaction; Enzymatic reaction; |
Conditions | Yield |
---|---|
With hydrogen chloride In dimethylsulfoxide-d6 |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 2h; Inert atmosphere; | 100% |
With potassium hydroxide In 1,2-dichloro-ethane | |
With potassium hydroxide |
lactobionic acid
1,12-Diaminododecane
Conditions | Yield |
---|---|
In methanol for 24h; Heating; | 100% |
4,7-dichloroquinoline
1,12-Diaminododecane
N1-(7-Chloro-quinolin-4-yl)-dodecane-1,12-diamine
Conditions | Yield |
---|---|
Inert atmosphere; | 100% |
1.) 80 deg C, 1 h, 2.) 135-145 deg C, 3 h; |
1,12-Diaminododecane
Conditions | Yield |
---|---|
In dimethyl sulfoxide; toluene at 145 - 150℃; for 24h; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.25h; | 100% |
In tetrahydrofuran at 20℃; for 0.25h; | 100% |
Conditions | Yield |
---|---|
In water for 13h; Reflux; | 100% |
In water at 20℃; Reflux; | |
In water at 20℃; Reflux; |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.25h; | 100% |
In tetrahydrofuran at 20℃; for 0.25h; | 100% |
Conditions | Yield |
---|---|
Stage #1: 2,3,4-tris(benzyloxy)benzoic acid With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate In dichloromethane for 0.0833333h; Stage #2: 1,12-Diaminododecane With triethylamine In dichloromethane at 20℃; | 100% |
Conditions | Yield |
---|---|
In methanol at 20℃; | 100% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 2h; Inert atmosphere; | 100% |
1,12-Diaminododecane
1,12-Dodecanediamine, dihydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In 1,4-dioxane; methanol for 0.166667h; | 100% |
1,12-Diaminododecane
Conditions | Yield |
---|---|
With trihydroxy amine In water | 100% |
1,12-Diaminododecane
di-tert-butyl dicarbonate
tert-butyl (12-aminododecyl)carbamate
Conditions | Yield |
---|---|
With sodium hydroxide In dichloromethane; water for 1.08333h; | 99% |
In chloroform at 0 - 20℃; | 90% |
In chloroform | 81% |
Conditions | Yield |
---|---|
Stage #1: 1,12-Diaminododecane; pentaerythritol tetraacrylate In methanol at 25℃; for 18h; Michael addition; Stage #2: morpholine In methanol at 20℃; for 18h; Further stages.; | 99% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 14h; | 98% |
Conditions | Yield |
---|---|
lipase from Candida antarctica In toluene at 70℃; for 19h; Product distribution / selectivity; | 98% |
Conditions | Yield |
---|---|
for 3h; Milling; Green chemistry; | 98% |
1,12-Diaminododecane
Conditions | Yield |
---|---|
Stage #1: 1,12-Diaminododecane; bis(calix[4]imidazolylidene[2]pyrazolato)octakissilver(I) tetrakis(trifluoromethanesulfonate) In N,N-dimethyl-formamide at 20℃; for 0.166667h; Schlenk technique; Inert atmosphere; Stage #2: 3,5-di-tert-butylbenzoic anhydride With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at -50 - 20℃; for 16h; Schlenk technique; Inert atmosphere; | 98% |
1,12-Diaminododecane
acetic anhydride
N,N'-Diacetyl-1,12-dodecandiamin
Conditions | Yield |
---|---|
With pyridine at 20℃; | 97% |
Conditions | Yield |
---|---|
Stage #1: N-Cbz-L-Phe With 1,1'-carbonyldiimidazole In chloroform at 20℃; for 1.5h; Stage #2: 1,12-Diaminododecane In chloroform at 20℃; | 97% |
With dmap; dicyclohexyl-carbodiimide In chloroform for 20h; Ambient temperature; | 74% |
Conditions | Yield |
---|---|
In neat (no solvent) at 20℃; for 24h; | 97% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 2h; Inert atmosphere; | 97% |
1,12-Diaminododecane
ethyl 2-(1-ethoxyethylidene)hydrazinecarboxylate
Conditions | Yield |
---|---|
In water for 5.5h; Heating; | 96% |
Conditions | Yield |
---|---|
In water for 5.5h; Heating; | 96% |
Conditions | Yield |
---|---|
In tetrahydrofuran Heating; | 96% |
Conditions | Yield |
---|---|
In neat (no solvent) for 1.5h; Milling; Green chemistry; | 96% |
1,12-Diaminododecane
Boc-Trp-OH
Conditions | Yield |
---|---|
With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
Stage #1: Z-Leu-OH With 1,1'-carbonyldiimidazole In chloroform at 20℃; for 1.5h; Stage #2: 1,12-Diaminododecane In chloroform at 20℃; | 95.7% |
1,12-Diaminododecane
9,10-dioxo-9,10-dihydro-2-anthracenesulfonyl chloride
C40H40N2O8S2
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran; water at 60 - 65℃; for 2h; | 95% |
1,12-Diaminododecane
hexan-1-ol
Hexanoic acid (12-hexanoylamino-dodecyl)-amide
Conditions | Yield |
---|---|
With C29H44Cl2N2Ru; potassium tert-butylate In toluene for 24h; Reflux; | 95% |
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