Product Description Product website: http://www.finerchem.com/pro01en/id/1747.html Product Name 1,2,4,5-Benzenetetracarboxylic acid CAS No.
Cas:86-98-6
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:86-98-6
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inquiryItems Standard Result Appearance White to light yellow powder Complies Assay ≥99%
Cas:86-98-6
Min.Order:1 Gram
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inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:86-98-6
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inquiryHigh quality 4,7-Dichloroquinoline Cas 86-98-6 with low price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed additiv
Cas:86-98-6
Min.Order:10 Kilogram
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inquiry4,7-Dichloroquinoline CAS:86-98-6/1138471-54-1 HANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & d
Cas:86-98-6
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:86-98-6
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:86-98-6
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so
Cas:86-98-6
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:86-98-6
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:86-98-6
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inquiryProduct Name: 4,7-Dichloroquinoline Synonyms: HydroxychloroquineSulfateEPImpurityG;HydroxychloroquineSulfateImpurity7(HydroxychloroquineSulfateEPImpuriChemicalbooktyG);4,7-dichloro-quinolin;TL1473;tl1473;4,7-DICHLO
Appearance:White to off-white powder Storage:ln stock Package:25kg/Barrel Application:Amodiaquine intermediates Transportation:Express/Sea/Air Port:Any port in china
Cas:86-98-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:86-98-6
Min.Order:1 Kilogram
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inquiryAbout Product Details Items Specifications Test Results Appearance White to white crystalline powde
Cas:86-98-6
Min.Order:100 Kilogram
FOB Price: $1.0 / 2.0
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:86-98-6
Min.Order:1 Kilogram
FOB Price: $89.0 / 100.0
Type:Trading Company
inquiry4,7-Dichloroquinoline CAS:86-98-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm
Cas:86-98-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:86-98-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:86-98-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryChemical Formula: C9H5Cl2N Exact Mass: 196.980 Molecular Weight: 198.049 1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the custo
Cas:86-98-6
Min.Order:25 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Cas:86-98-6
Min.Order:0
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Type:Manufacturers
inquiry1.Prompt Goods; 2.Flexible payment terms; 3.Documents & Certificate support. Name: 4,7-Dichloroquinoline Structure: Formula: C9H5Cl2N Molecular Weight : 198.05 Synonyms: HydroxychloroquineSulfateImpurity7(HydroxychloroquineSulfateEPImpur
Cas:86-98-6
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:86-98-6
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:86-98-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Packing: According to customer requirements Delivery time: In stock or depands Port of shipment: Ningbo/Shanghai/Qingdao OEM/ODM:Welcome Sample:We can offer our existing samples at once Transportation:Express/Sea/Air Port:Ningbo/Shanghai/Qingd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:86-98-6
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:white crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:For medicine , pesticid
Conditions | Yield |
---|---|
With trichlorophosphate for 1h; Heating; | 94% |
With trichlorophosphate Reflux; | 89.5% |
With trichlorophosphate for 2h; Heating / reflux; | 88.5% |
7-chloro-4(1H)-oxoquinoline
4,7-dichloroquinoline
Conditions | Yield |
---|---|
With trichlorophosphate for 2h; Reflux; | 85% |
With trichlorophosphate for 2h; Reflux; | 85% |
With ((1,3,5-triazine-2,4,6-triyl)tris(oxy))tris(triphenylphosphonium) chloride at 140 - 150℃; for 2h; Solvent; Ionic liquid; | |
With trichlorophosphate Reflux; |
7-fluoro-1,4-dihydroquinolin-4-one
4,7-dichloroquinoline
Conditions | Yield |
---|---|
With trichlorophosphate for 1h; Reflux; | 85% |
Conditions | Yield |
---|---|
With Eosin Y; di-tert-butyl 1,4-dihydro-2,6-dimethyl-3,5-pyridine-dicarboxylate In acetonitrile at 20℃; for 1h; Inert atmosphere; Irradiation; chemoselective reaction; | 78% |
With tris(bipyridine)ruthenium(II) dichloride hexahydrate; di-tert-butyl 1,4-dihydro-2,6-dimethyl-3,5-pyridine-dicarboxylate In acetonitrile at 20℃; for 0.0833333h; Inert atmosphere; Irradiation; chemoselective reaction; | 73% |
4,7-dichloroquinoline
Conditions | Yield |
---|---|
With iron oxide surrounded by nitrogen doped graphene shell immobilized on carbon support In n-heptane at 100℃; under 11251.1 Torr; for 12h; Autoclave; | 62% |
7-chloro-4-quinolinesulfonyl chloride
A
4,7-dichloroquinoline
B
7-chloro-4-quinolinesulfonamide
Conditions | Yield |
---|---|
With ammonia In water at 20℃; | A 31% B 56% |
5-[(3-chloro-phenylamino)-methylene]-2,2-dimethyl-[1,3]dioxane-4,6-dione
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diphenyl ether / 0.08 h / 300 °C / microwave irradiation 2: POCl3 / 3 h / Heating View Scheme |
2-acetyl-5-chloroaniline
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 75 percent / pyridine / CH2Cl2 / 1 h / 20 °C 2: 95 percent / K2CO3 / dimethylformamide / 1 h / 80 °C 3: 98 percent / NaI; Et3N / acetonitrile / 1 h / Heating 4: 95 percent / Cl2Ru(PCy3)(=CHPh)(N,N'-(Mes)2-imidazolidin-2-yl) / CH2Cl2 / 1 h / 50 °C 5: 81 percent / aq. NaOH / methanol / Heating 6: 94 percent / POCl3 / 1 h / Heating View Scheme |
N-(2-acetyl-5-chlorophenyl)-4-methylbenzenesulfonamide
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 95 percent / K2CO3 / dimethylformamide / 1 h / 80 °C 2: 98 percent / NaI; Et3N / acetonitrile / 1 h / Heating 3: 95 percent / Cl2Ru(PCy3)(=CHPh)(N,N'-(Mes)2-imidazolidin-2-yl) / CH2Cl2 / 1 h / 50 °C 4: 81 percent / aq. NaOH / methanol / Heating 5: 94 percent / POCl3 / 1 h / Heating View Scheme |
N-allyl-N-p-toluenesulfonyl-2-acetyl-5-chloroaniline
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 98 percent / NaI; Et3N / acetonitrile / 1 h / Heating 2: 95 percent / Cl2Ru(PCy3)(=CHPh)(N,N'-(Mes)2-imidazolidin-2-yl) / CH2Cl2 / 1 h / 50 °C 3: 81 percent / aq. NaOH / methanol / Heating 4: 94 percent / POCl3 / 1 h / Heating View Scheme |
N-p-toluenesulfonyl-4-(t-butyldimethylsilyloxy)-7-chloro-1,2-dihydroquinoline
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 81 percent / aq. NaOH / methanol / Heating 2: 94 percent / POCl3 / 1 h / Heating View Scheme |
N-allyl-N-p-toluenesulfonyl-2-[1-(tert-butyldimethylsilyloxy)vinyl]-5-chloroaniline
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 95 percent / Cl2Ru(PCy3)(=CHPh)(N,N'-(Mes)2-imidazolidin-2-yl) / CH2Cl2 / 1 h / 50 °C 2: 81 percent / aq. NaOH / methanol / Heating 3: 94 percent / POCl3 / 1 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diphenyl ether / 1 h / Heating 2: POCl3 / 100 °C View Scheme |
7-chloro-4-hydroxyquinoline-3-carboxylic acid,ethyl ester
A
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 2 N aq. NaOH / 1 h / Heating 2: diphenyl ether / 1 h / Heating 3: POCl3 / 100 °C View Scheme |
2-(3-chlorophenylamino)methylenemalonic acid diethyl ester
A
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: diphenyl ether / 1 h / Heating 2: 2 N aq. NaOH / 1 h / Heating 3: diphenyl ether / 1 h / Heating 4: POCl3 / 100 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 1.5 h / 165 °C 2: diphenyl ether / 1 h / Heating 3: 2 N aq. NaOH / 1 h / Heating 4: diphenyl ether / 1 h / Heating 5: POCl3 / 100 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 250 - 270 °C / oder in einem Gemisch von Diphenylaether und Biphenyl 2: phosphoryl chloride View Scheme |
7-chlorokynurenic acid
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: mineral oil / 270 °C 2: phosphoryl chloride View Scheme | |
Multi-step reaction with 2 steps 1: 1-chloro-naphthalene 2: phosphoryl chloride View Scheme |
7-chloro-4-hydroxy-quinoline-2-carboxylic acid ethyl ester
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aqueous NaOH 2: mineral oil / 270 °C 3: phosphoryl chloride View Scheme | |
Multi-step reaction with 3 steps 1: aqueous NaOH 2: 1-chloro-naphthalene 3: phosphoryl chloride View Scheme |
7-chloro-4-hydroxyquinoline-3-carboxylic acid,ethyl ester
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aqueous NaOH 2: 250 - 270 °C / oder in einem Gemisch von Diphenylaether und Biphenyl 3: phosphoryl chloride View Scheme | |
Multi-step reaction with 3 steps 1: sodium hydroxide; water / diphenylether / 0.5 h 2: paraffin oil / 0.83 h / 230 °C 3: trichlorophosphate / Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 2: aqueous NaOH 3: 250 - 270 °C / oder in einem Gemisch von Diphenylaether und Biphenyl 4: phosphoryl chloride View Scheme | |
Multi-step reaction with 2 steps 1: dowtherm / 4 h 2: trichlorophosphate / 6 h / Reflux View Scheme | |
Multi-step reaction with 4 steps 1: diphenylether / Reflux 2: sodium hydroxide; ethanol / Reflux 3: diphenylether / Reflux 4: trichlorophosphate / 2 h / Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: acetic acid / Erhitzen des Reaktionsprodukts in Paraffinoel auf 250grad 2: aqueous NaOH 3: mineral oil / 270 °C 4: phosphoryl chloride View Scheme | |
Multi-step reaction with 5 steps 3: aqueous NaOH 4: 250 - 270 °C / oder in einem Gemisch von Diphenylaether und Biphenyl 5: phosphoryl chloride View Scheme | |
Multi-step reaction with 4 steps 1: acetic acid / Erhitzen des Reaktionsprodukts in Paraffinoel auf 250grad 2: aqueous NaOH 3: mineral oil / 270 °C 4: phosphoryl chloride View Scheme |
Conditions | Yield |
---|---|
Stage #1: 3-chloro-aniline; diethyl 2-ethoxymethylenemalonate Heating; Stage #2: With trichlorophosphate |
7-fluoro-1,4-dihydro-4-oxo-3-quinoline carboxylic acid ethyl ester
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium hydroxide / 1 h / Reflux 2: diphenylether / 0.5 h / Reflux 3: trichlorophosphate / 1 h / Reflux View Scheme |
7-fluoro-1,4-dihydro-4-oxo-3-quinolinecarboxylic acid
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diphenylether / 0.5 h / Reflux 2: trichlorophosphate / 1 h / Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 2 h / 100 °C 2: diphenylether / 0.25 h / Reflux 3: sodium hydroxide / 1 h / Reflux 4: diphenylether / 0.5 h / Reflux 5: trichlorophosphate / 1 h / Reflux View Scheme |
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: diphenylether / 0.25 h / Reflux 2: sodium hydroxide / 1 h / Reflux 3: diphenylether / 0.5 h / Reflux 4: trichlorophosphate / 1 h / Reflux View Scheme |
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diphenylether / Reflux 2: trichlorophosphate / 2 h / Reflux View Scheme |
ethyl 7-chloro-1,4-dihydro-4-oxo-3-quinolinecarboxylate
4,7-dichloroquinoline
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium hydroxide; ethanol / Reflux 2: diphenylether / Reflux 3: trichlorophosphate / 2 h / Reflux View Scheme |
4,7-dichloroquinoline
heptane-1,7-diamine
N-(7-chloro-[4]quinolyl)-heptanediyldiamine
Conditions | Yield |
---|---|
Inert atmosphere; | 100% |
In pentan-1-ol at 120℃; for 16h; | 80% |
With N-ethyl-N,N-diisopropylamine In pentan-1-ol for 18h; Heating; | 80% |
4,7-dichloroquinoline
ethylenediamine
N-(7-chloroquinolin-4-yl)ethylenediamine
Conditions | Yield |
---|---|
at 80 - 140℃; for 13h; | 100% |
at 80 - 135℃; for 4h; neat (no solvent); | 100% |
In neat (no solvent) at 110℃; | 100% |
Conditions | Yield |
---|---|
In ethanol for 24h; Reflux; | 100% |
for 0.166667h; microwave irradiation; | 95% |
With ethanol |
Conditions | Yield |
---|---|
In isopropyl alcohol at 100℃; for 20h; | 100% |
With triethylamine at 130℃; for 4h; Inert atmosphere; | 98% |
With potassium carbonate In isopropyl alcohol for 36h; Reflux; | 95% |
4,7-dichloroquinoline
1,8-diaminooctan
N-(7-chloroquinolin-4-yl)octane-1,8-diamine
Conditions | Yield |
---|---|
Inert atmosphere; | 100% |
at 80 - 140℃; for 2.75h; Microwave irradiation; | 69% |
at 80 - 135℃; for 4h; | 51% |
4,7-dichloroquinoline
diaminodecane
N-(7-chloroquinolin-4-yl)decane-1,10-diamine
Conditions | Yield |
---|---|
Inert atmosphere; | 100% |
at 80 - 135℃; for 4h; | 60% |
1.) 80 deg C, 1 h, 2.) 135-145 deg C, 3 h; |
4,7-dichloroquinoline
1,12-Diaminododecane
N1-(7-Chloro-quinolin-4-yl)-dodecane-1,12-diamine
Conditions | Yield |
---|---|
Inert atmosphere; | 100% |
1.) 80 deg C, 1 h, 2.) 135-145 deg C, 3 h; |
4,7-dichloroquinoline
Trimethylenediamine
N-(7-chloroquinolin-4-yl)propane-1,3-diamine
Conditions | Yield |
---|---|
In neat (no solvent) at 110℃; | 100% |
Inert atmosphere; | 100% |
In isopropyl alcohol at 100℃; for 20h; | 98% |
4,7-dichloroquinoline
1,4-diaminobutane
N1-(7-chloroquinolin-4-yl)butane-1,4-diamine
Conditions | Yield |
---|---|
Inert atmosphere; | 100% |
at 95℃; for 1h; Microwave irradiation; | 100% |
In isopropyl alcohol at 100℃; for 20h; | 99% |
4,7-dichloroquinoline
silver thiocyanate
7-chloro-4-isothiocyanatoquinoline
Conditions | Yield |
---|---|
In toluene at 110℃; for 12h; | 100% |
In toluene at 115℃; for 18h; | 89% |
In toluene at 90 - 120℃; for 18h; | 68% |
In toluene for 12h; Heating; | |
In toluene at 120℃; for 18h; |
4,7-dichloroquinoline
propan-1-ol-3-amine
3-[(7-chloroquinolin-4-yl)amino]propan-1-ol
Conditions | Yield |
---|---|
Inert atmosphere; | 100% |
With triethylamine In ethanol at 90℃; | 99% |
With triethylamine In N,N-dimethyl-formamide at 60 - 120℃; for 24h; | 96% |
5-amino-4'-trifluoromethyl-biphenyl-3-ol
4,7-dichloroquinoline
5-(7-chloro-quinolin-4-ylamino)-4'-trifluoromethyl-biphenyl-3-ol
Conditions | Yield |
---|---|
In ethanol for 2h; Heating; | 100% |
Conditions | Yield |
---|---|
In ethanol for 24h; Reflux; | 100% |
In neat (no solvent) at 120℃; under 1500.15 Torr; for 0.166667h; Microwave irradiation; | 96% |
for 0.116667h; microwave irradiation; | 95% |
4,7-dichloroquinoline
7-amino-3-ethylquinazolin-4(3H)-one
C19H15ClN4O
Conditions | Yield |
---|---|
In ethanol for 48h; Reflux; | 100% |
4,7-dichloroquinoline
7-amino-3-propylquinazolin-4(3H)-one
C20H17ClN4O
Conditions | Yield |
---|---|
In ethanol for 48h; Reflux; | 100% |
4,7-dichloroquinoline
7-amino-3-benzylquinazolin-4(3H)-one
C24H17ClN4O
Conditions | Yield |
---|---|
In ethanol for 48h; Reflux; | 100% |
4,7-dichloroquinoline
4-methoxy-aniline
7-chloro-N-(4-methoxyphenyl)quinolin-4-amine
Conditions | Yield |
---|---|
With trifluoroacetic acid In 1,1,2-Trichloro-1,2,2-trifluoroethane for 8.53333h; Inert atmosphere; Reflux; | 99% |
With phenol at 120℃; for 0.5h; | 98% |
for 0.25h; microwave irradiation; | 78% |
With silica gel-loaded acidic ionic liquid IL/TFA at SiO2 In 1-methyl-pyrrolidin-2-one at 70℃; | 36.8% |
With hydrogenchloride |
4,7-dichloroquinoline
ethanolamine
3-(7-chloroquinolin-4-ylamino)propyl alcohol
Conditions | Yield |
---|---|
With triethylamine In ethanol at 90℃; | 99% |
at 130 - 140℃; for 24h; | 97% |
In neat (no solvent) at 130℃; | 95% |
Conditions | Yield |
---|---|
With ammonium carbonate; phenol at 110 - 165℃; | 99% |
With ammonia In phenol at 170℃; for 2h; | 92% |
With ammonia; phenol at 150℃; for 2h; | 89% |
Conditions | Yield |
---|---|
In ethanol Reflux; | 99% |
With hydrogenchloride; potassium iodide In ethanol for 12h; Heating; |
4,7-dichloroquinoline
dimethyl amine
7-chloro-4-N,N-dimethylamino-quinoline
Conditions | Yield |
---|---|
In water; acetonitrile at 50℃; for 48h; | 99% |
In water; acetonitrile at 50℃; for 48h; | 90% |
With acetic acid at 130 - 135℃; for 3h; | 40% |
4,7-dichloroquinoline
m-Hydroxyaniline
4-(3'-hydroxyphenyl)amino-7-chloroquinoline
Conditions | Yield |
---|---|
In ethanol Reflux; | 99% |
for 0.25h; microwave irradiation; | 75% |
With hydrogenchloride; potassium iodide In ethanol Heating; |
1H-imidazole
4,7-dichloroquinoline
7-chloro-4-(1H-imidazol-1-yl)quinoline
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 150℃; for 2h; Inert atmosphere; Green chemistry; | 99% |
for 0.0333333h; microwave irradiation; | 85% |
4,7-dichloroquinoline
1 ,5-pentanediol
O-(7-chloro-4-quinolyl)-1,5-pentanediol
Conditions | Yield |
---|---|
With potassium tert-butylate In tert-butyl alcohol at 80℃; for 18h; Inert atmosphere; | 99% |
4,7-dichloroquinoline
trimethyleneglycol
O-(7-chloro-4-quinolyl)-1,3-propanediol
Conditions | Yield |
---|---|
With potassium tert-butylate In tert-butyl alcohol at 80℃; for 18h; Inert atmosphere; | 99% |
With potassium tert-butylate In tert-butyl alcohol at 80℃; for 18h; |
4,7-dichloroquinoline
5-amino-4'-chloro<1,1'-biphenyl>-2-ol
4’-chloro-5-[(7-chloro-4-quinolinyl)amino]-[1,1’-biphenyl]-2-ol
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol; water for 10h; Reflux; | 99% |
With hydrogenchloride In ethanol; water for 4h; Inert atmosphere; Reflux; | 87% |
4,7-dichloroquinoline
methyl trifluoromethanesulfonate
4,7-dichloro-1-methylquinolinium triflate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 18h; | 99% |
In toluene at 20℃; for 24h; | 65% |
Conditions | Yield |
---|---|
In ethanol Reflux; | 99% |
Conditions | Yield |
---|---|
In ethanol Reflux; | 99% |
Conditions | Yield |
---|---|
In ethanol Reflux; | 99% |
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