1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:204-02-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryperimidine CAS:204-02-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
Cas:204-02-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:204-02-4
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiry1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
perimidine Basic information Product Name: perimidine Synonyms: perimidine;1,3-Diaza-1H-phenalene;Benzo[de]quinazoline CAS:
1H-PerimidineAppearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL
Supply top quality products with a reasonable price Application:api
Our company provides the best service for our customers. Under the premise of ensuring quality and delivery date, give customers the best price. The company is more willing to meet our customers. If you want to visit our factories and warehouses, we
Conditions | Yield |
---|---|
Stage #1: orthoformic acid triethyl ester at 20℃; for 0.25h; Stage #2: naphthalene-1,8-diamine at 20℃; for 3h; | 100% |
Conditions | Yield |
---|---|
In formic acid; hydrogen bromide for 1.5h; Heating; | 97% |
Conditions | Yield |
---|---|
In ethanol | 96% |
In ethanol for 0.666667h; Heating; | 95% |
With hydrogen bromide In acetone Reflux; | 95% |
2,3-dihydroperimidine
1-H-perimidine
Conditions | Yield |
---|---|
With sodium disulfite In ethanol; water for 2h; Heating; | 95% |
Conditions | Yield |
---|---|
With carbon dioxide In water at 150℃; under 37503.8 Torr; for 5h; | 93.1% |
With 1,1,1,3,3,3-hexamethyl-disilazane at 120℃; for 12h; Green chemistry; | 50% |
With zinc(II) acetate dihydrate In neat (no solvent) at 120℃; under 7600.51 Torr; for 18h; Autoclave; Inert atmosphere; Green chemistry; | 41% |
benzylpenicilloic acid α-phenylethylamide
naphthalene-1,8-diamine
A
1-H-perimidine
B
3,3-dimethyl-D-cysteine
C
phenaceturic acid α-phenethylamide
Conditions | Yield |
---|---|
In water; acetic acid for 2h; Heating; | A 85% B 69% C 74% |
Conditions | Yield |
---|---|
With [(N,N′-bis(diisopropylphosphino)-2,6-diaminopyridine)Mn(CO)3][Br]; potassium tert-butylate In toluene at 120℃; for 24h; Inert atmosphere; Glovebox; Schlenk technique; | 69% |
Conditions | Yield |
---|---|
With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In toluene at 100℃; under 22502.3 Torr; for 48h; Autoclave; | 66% |
Conditions | Yield |
---|---|
In toluene at 100℃; for 48h; | 44% |
Conditions | Yield |
---|---|
With 1,1,1,3,3,3-hexamethyl-disilazane at 120℃; for 12h; Green chemistry; | 38% |
Conditions | Yield |
---|---|
With phenylsilane; 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene at 70℃; for 24h; | 35% |
With diphenylsilane; C33H36BO6(3-)*Eu(3+)*H2O*2C3H7NO In acetonitrile at 120℃; under 7500.75 Torr; for 24h; Autoclave; | 34% |
With N,N′-bis(2,6-diisopropylphenyl)imidazol-2-ylidene hydrochloride; phenylsilane In tetrahydrofuran at 70℃; under 750.075 - 2250.23 Torr; for 24h; Schlenk technique; Inert atmosphere; Glovebox; |
2,3-dihydro-2,2-dimethylperimidine
N,N-dimethyl-formamide
A
perimidine-9-carbaldehyde
C
1-H-perimidine
Conditions | Yield |
---|---|
With trichlorophosphate at 65 - 70℃; for 2h; | A 4% B 13% C 0.07% |
Conditions | Yield |
---|---|
oder mit anderen hochsiedenden Loesungsmitteln; |
ethyl 1H-perimidine-2-carboxylate
1-H-perimidine
Conditions | Yield |
---|---|
With hydrogenchloride at 140 - 160℃; |
oxalic acid
naphthalene-1,8-diamine
A
1-H-perimidine
B
2,2'-diperimidinyl
Conditions | Yield |
---|---|
at 160℃; |
oxalic acid diethyl ester
naphthalene-1,8-diamine
A
1-H-perimidine
B
2,2'-diperimidinyl
Conditions | Yield |
---|---|
With calcium oxide at 140℃; im Rohr; |
Conditions | Yield |
---|---|
12-36-stuendiges Kochen; | |
at 140 - 160℃; |
1-H-perimidine
Conditions | Yield |
---|---|
With hydrogenchloride at 140 - 160℃; | |
With nitrobenzene |
water
oxalic acid
naphthalene-1,8-diamine
A
1-H-perimidine
B
perimidine-2-carboxylic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 97 percent / aq. HBr; formic acid / 1.5 h / Heating View Scheme | |
Multi-step reaction with 2 steps 2: concentrated hydrochloric acid / 140 - 160 °C View Scheme | |
With formic acid In water |
6(7)-acetylperimidine
1-H-perimidine
Conditions | Yield |
---|---|
With PPA |
6(7)-acetylperimidine
1-H-perimidine
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride In PPA |
1-H-perimidine
1H,1'H-[6,6']biperimidinyl
Conditions | Yield |
---|---|
With aluminum (III) chloride In nitromethane at 20℃; | 96% |
Conditions | Yield |
---|---|
Stage #1: 1-H-perimidine With potassium tert-butylate In dimethyl sulfoxide at 20℃; for 0.5h; Stage #2: 1-chloromethyl-3-methyl-benzene In dimethyl sulfoxide at 110℃; for 0.5h; Microwave irradiation; | 95% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 20℃; Reflux; | 94% |
Conditions | Yield |
---|---|
Stage #1: 1-H-perimidine With sodium hydride In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; Schlenk technique; Stage #2: methyl iodide In N,N-dimethyl-formamide for 12h; Inert atmosphere; Schlenk technique; Reflux; | 93% |
Stage #1: 1-H-perimidine With potassium hydroxide In acetonitrile at 20℃; for 1h; Stage #2: methyl iodide In acetonitrile for 12h; Reflux; | 78% |
With potassium carbonate In acetonitrile for 6h; Reflux; | 32% |
Conditions | Yield |
---|---|
Stage #1: 1-H-perimidine With sodium hydride In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; Schlenk technique; Stage #2: 1-iodo-propane In N,N-dimethyl-formamide for 12h; Inert atmosphere; Schlenk technique; Reflux; | 92% |
Conditions | Yield |
---|---|
With aq. PPA at 55 - 60℃; for 1h; | 91% |
1,3,5-Triazine
1-H-perimidine
benzaldehyde
6-phenyl-1,3,7-triazapyrene
Conditions | Yield |
---|---|
With polyphosphoric acid at 60 - 70℃; for 9h; | 91% |
Conditions | Yield |
---|---|
With benzyl chloride In acetonitrile; mineral oil at 0 - 20℃; for 25h; | 89% |
Stage #1: 1-H-perimidine With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0℃; Stage #2: 1-bromo-butane In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 25h; | 87% |
With sodium hydride In tetrahydrofuran at 20℃; Reflux; | 86% |
1,3,5-Triazine
1-H-perimidine
4-bromo-benzaldehyde
6-(4-bromophenyl)-1,3,7-triazapyrene
Conditions | Yield |
---|---|
With polyphosphoric acid at 60 - 70℃; for 9h; | 89% |
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide for 3h; | 88% |
With sodium hydride In acetonitrile; mineral oil at 0 - 20℃; for 25h; Inert atmosphere; |
Conditions | Yield |
---|---|
Stage #1: 1-H-perimidine With sodium hydride In tetrahydrofuran for 24h; Inert atmosphere; Schlenk technique; Reflux; Stage #2: 2-(bromomethyl)-1,3,5-triisopropylbenzene In tetrahydrofuran for 24h; Inert atmosphere; Schlenk technique; Reflux; | 87% |
Conditions | Yield |
---|---|
With methanesulfonic acid at 20℃; for 0.25h; | 87% |
With methanesulfonic acid at 20℃; |
Conditions | Yield |
---|---|
With copper(l) iodide; N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 86% |
Conditions | Yield |
---|---|
With aluminum tri-bromide In 1,2-dichloro-ethane at 20℃; for 0.5h; | 84% |
With aluminum tri-bromide In 1,2-dichloro-ethane at 20℃; for 0.5h; Friedel-Crafts reaction; | 45% |
2,4,6-trimethyl-s-triazine
1-H-perimidine
benzaldehyde
6(8)-oxo-8(6)-phenyl-1,6,7,8-tetrahydro-1,3-diazapyrene
Conditions | Yield |
---|---|
Stage #1: 2,4,6-trimethyl-s-triazine; 1-H-perimidine; benzaldehyde at 60 - 70℃; for 8h; Stage #2: With water for 0.0833333h; Reflux; | 84% |
1-H-perimidine
(2-nitroethenyl)benzene
8-phenyl-1,8-dihydropyrido[2,3,4-gh]perimidin-7(6H)-one
Conditions | Yield |
---|---|
With 80 percent polyphosphoric acid at 65 - 70℃; for 5h; | 84% |
1-H-perimidine
6(7)-nitroperimidine
Conditions | Yield |
---|---|
With ammonium nitrate; acetic acid Reflux; | 83% |
1,3,5-Triazine
1-H-perimidine
4-nitrobenzaldehdye
6-(4-nitrophenyl)-1,3,7-triazapyrene
Conditions | Yield |
---|---|
With polyphosphoric acid at 60 - 70℃; for 9h; | 83% |
1-H-perimidine
2,4,6-triphenyl-1,3,5-triazine
6,9-dibenzoylperimidine
Conditions | Yield |
---|---|
With PPA; water at 70 - 75℃; for 2.5h; | 82% |
1-H-perimidine
1,3-diphenylpropanedione
6,8-diphenylbenzo[gh]perimidine
Conditions | Yield |
---|---|
With sulfuric acid In water at 95 - 100℃; regioselective reaction; | 82% |
Conditions | Yield |
---|---|
With sulfuric acid In water at 95 - 100℃; regioselective reaction; | 82% |
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide for 2h; Ambient temperature; | 81% |
With potassium hydroxide In chlorobenzene; toluene for 3h; Heating; | 71% |
Stage #1: 1-H-perimidine With potassium hydroxide In ethanol at 20℃; for 1h; Reflux; Darkness; Stage #2: methyl iodide In ethanol for 3h; Reflux; | 61% |
1-H-perimidine
perimidine-6(7)-sulfonic acid
Conditions | Yield |
---|---|
With sulfuric acid for 0.25h; Ambient temperature; | 81% |
2,4,6-trimethyl-s-triazine
1-H-perimidine
4-nitrobenzaldehdye
8(6)-(4-nitrophenyl)-6(8)-oxo-1,6,7,8-tetrahydro-1,3-diazapyrene
Conditions | Yield |
---|---|
Stage #1: 2,4,6-trimethyl-s-triazine; 1-H-perimidine; 4-nitrobenzaldehdye at 60 - 70℃; for 8h; Stage #2: With water for 0.0833333h; Reflux; | 81% |
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