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inquiry10-Bromodecanol CAS:53463-68-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermedi
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiry10-Bromodecanol Basic information Product Name: 10-Bromodecanol Synonyms: 10-Bromo-1-decan;DECAMETHYLENE BROMOHYDRIN;10-bromo-1-decano;10-Hydroxydecyl bromide;10-Bromo-1-decanol,95%;10-BROMO-1-DECANOL 85+%;10-BROMO-1-DECANOL, TECH., 90%;10-BRO
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:1g Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any port
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C14H29BrO3
1-bromo-10-decanol
Conditions | Yield |
---|---|
Stage #1: C14H29BrO3 With [2,2]bipyridinyl; trimethylsilyl trifluoromethanesulfonate In dichloromethane at 0℃; for 0.5h; Inert atmosphere; Stage #2: With water In diethyl ether; dichloromethane at 20℃; for 5h; Inert atmosphere; chemoselective reaction; | 95% |
1,10-Decanediol
1-bromo-10-decanol
Conditions | Yield |
---|---|
With hydrogen bromide In water; toluene for 16h; Inert atmosphere; Reflux; Dean-Stark; | 93% |
With hydrogen bromide In water; toluene Reflux; Inert atmosphere; | 92% |
With hydrogen bromide In water; toluene Reflux; | 92% |
C16H35BrO2Si
1-bromo-10-decanol
Conditions | Yield |
---|---|
Stage #1: C16H35BrO2Si With [2,2]bipyridinyl; trimethylsilyl trifluoromethanesulfonate In dichloromethane at 0℃; for 0.5h; Inert atmosphere; Stage #2: With water In dichloromethane at 20℃; for 3h; Inert atmosphere; chemoselective reaction; | 92% |
Conditions | Yield |
---|---|
With hydrogen bromide In cyclohexane for 6h; Heating; | A 88% B 9% |
With hydrogen bromide In toluene for 48h; Substitution; Heating; | A 87% B n/a |
With hydrogen bromide In water; toluene Reflux; | A 87% B n/a |
C18H29BrO2
1-bromo-10-decanol
Conditions | Yield |
---|---|
Stage #1: C18H29BrO2 With [2,2]bipyridinyl; trimethylsilyl trifluoromethanesulfonate In dichloromethane at 0℃; for 0.5h; Inert atmosphere; Stage #2: With water In dichloromethane at 20℃; for 5h; Inert atmosphere; chemoselective reaction; | 88% |
1-bromo-10-(methoxymethoxy)decane
1-bromo-10-decanol
Conditions | Yield |
---|---|
Stage #1: 1-bromo-10-(methoxymethoxy)decane With [2,2]bipyridinyl; trimethylsilyl trifluoromethanesulfonate In dichloromethane at 0℃; for 0.5h; Inert atmosphere; Stage #2: With water In diethyl ether; dichloromethane at 20℃; for 7h; Inert atmosphere; chemoselective reaction; | 88% |
Multi-step reaction with 3 steps 1.1: dichloromethane / 0.5 h / 0 °C / Inert atmosphere 2.1: dichloromethane / 20 °C / Inert atmosphere 3.1: [2,2]bipyridinyl; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere 3.2: 5 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: dichloromethane / 0.5 h / 0 °C / Inert atmosphere 2.1: dichloromethane / 24 h / 20 °C / Inert atmosphere 3.1: [2,2]bipyridinyl; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere 3.2: 5 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: dichloromethane / 0.5 h / 0 °C / Inert atmosphere 2.1: dichloromethane / 6 h / 20 °C / Inert atmosphere 3.1: [2,2]bipyridinyl; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere 3.2: 3 h / 20 °C / Inert atmosphere View Scheme |
1-bromo-10-decanol
Conditions | Yield |
---|---|
With montmorillonite K 10 supported ammonium nitrate In neat (no solvent) for 0.05h; Irradiation; | 86% |
9-Decen-1-ol
A
1-bromo-10-decanol
B
9-bromo-decane-1-ol
C
8-(oxiran-2-yl)octan-1-ol
D
decane-1,2,10-triol
Conditions | Yield |
---|---|
With [VIVO(sal-l-val)(1,10-phenanthroline)]; dihydrogen peroxide; potassium bromide at 20℃; for 8h; Catalytic behavior; Acidic conditions; | A 41% B 2% C n/a D n/a |
9-Decen-1-ol
A
1-bromo-10-decanol
B
9-bromo-decane-1-ol
C
8-(oxiran-2-yl)octan-1-ol
Conditions | Yield |
---|---|
With [VO(O)2(PAH)(Phen)]; dihydrogen peroxide; nitric acid; potassium bromide In N,N-dimethyl-formamide; acetonitrile at 20℃; for 5h; | A 15% B 8% C 10% |
10-bromodecanoic acid
1-bromo-10-decanol
Conditions | Yield |
---|---|
With borane In tetrahydrofuran |
10-chlorodecanol
1-bromo-10-decanol
Conditions | Yield |
---|---|
With lithium bromide In various solvent(s) at 120℃; for 2h; Yield given; |
1Z,5E-cyclodecadiene
1-bromo-10-decanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: 48percent HBr / H2O / 60 h / Heating View Scheme |
1-bromo-10-decanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: dichloromethane / 6 h / 20 °C / Inert atmosphere 2.1: [2,2]bipyridinyl; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere 2.2: 3 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: dichloromethane / 20 °C / Inert atmosphere 2.1: [2,2]bipyridinyl; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere 2.2: 5 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1.1: dichloromethane / 24 h / 20 °C / Inert atmosphere 2.1: [2,2]bipyridinyl; trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.5 h / 0 °C / Inert atmosphere 2.2: 5 h / 20 °C / Inert atmosphere View Scheme |
10-Undecen-1-ol
1-bromo-10-decanol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: carbon tetrabromide; triphenylphosphine / dichloromethane / 2 h / 0 - 20 °C 2: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 3 h / 20 °C 3: sodium periodate / tetrahydrofuran; water / 1 h / 0 °C 4: sodium tetrahydroborate; water / tetrahydrofuran / 20 °C View Scheme |
1-undecen-11-ylbromide
1-bromo-10-decanol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: osmium(VIII) oxide; water; 4-methylmorpholine N-oxide / acetone / 3 h / 20 °C 2: sodium periodate / tetrahydrofuran; water / 1 h / 0 °C 3: sodium tetrahydroborate; water / tetrahydrofuran / 20 °C View Scheme |
10-bromodecanal
1-bromo-10-decanol
Conditions | Yield |
---|---|
With sodium tetrahydroborate; water In tetrahydrofuran at 20℃; |
11-bromoundecane-1,2-diol
1-bromo-10-decanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium periodate / tetrahydrofuran; water / 1 h / 0 °C 2: sodium tetrahydroborate; water / tetrahydrofuran / 20 °C View Scheme |
Conditions | Yield |
---|---|
With water In dimethylsulfoxide-d6; [(2)H6]acetone at 50℃; |
3,4-dihydro-2H-pyran
1-bromo-10-decanol
1-bromo-10-(tetrahydropyranyloxy)decane
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid for 0.5h; | 100% |
With toluene-4-sulfonic acid In dichloromethane 1) 0 deg C, 15 min; 2) 25 deg C, 1 h; | 100% |
With toluene-4-sulfonic acid at 20℃; for 24h; | 100% |
1-bromo-10-decanol
10-bromodecanal
Conditions | Yield |
---|---|
With pyridinium chlorochromate In dichloromethane for 3h; Ambient temperature; | 100% |
With pyridinium chlorochromate In dichloromethane for 4h; Ambient temperature; | 95% |
With 1-methyl-1H-imidazole; [2,2]bipyridinyl; tetrakis(actonitrile)copper(I) hexafluorophosphate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In acetonitrile at 20℃; for 14h; | 91% |
1-bromo-10-decanol
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid at 0℃; for 1h; | 100% |
Conditions | Yield |
---|---|
With copper(l) chloride In tetrahydrofuran at 0 - 20℃; for 2h; Inert atmosphere; | 100% |
With dilithium tetrachlorocuprate In tetrahydrofuran at -78℃; for 20h; | 94% |
1-bromo-10-decanol
triphenylphosphine
(10-Hydroxydecyl)-triohenylphosphonium-bromid
Conditions | Yield |
---|---|
In acetonitrile at 120℃; for 0.0833333h; Flow reactor; | 99% |
In acetonitrile for 16h; Heating; | 96% |
In acetonitrile | 91% |
1-bromo-10-decanol
tert-butyldimethylsilyl chloride
((10-bromodecyl)oxy)(tert-butyl)dimethylsilane
Conditions | Yield |
---|---|
With 1H-imidazole; dmap In dichloromethane at 0 - 20℃; Inert atmosphere; | 99% |
With 1H-imidazole In dichloromethane for 48h; Ambient temperature; | 98% |
With 1H-imidazole In dichloromethane Cooling with ice; | 94.21% |
1-bromo-10-decanol
10-azido-decan-1-ol
Conditions | Yield |
---|---|
With sodium azide; tetrabutyl ammonium fluoride In tetrahydrofuran; water at 25 - 34℃; for 60h; | 99% |
With sodium azide; sodium iodide In N,N-dimethyl-formamide at 80℃; for 18h; | 98% |
With sodium azide In N,N-dimethyl-formamide at 50℃; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With triethylamine In diethyl ether at 20℃; for 2h; | 99% |
1-bromo-10-decanol
potassium phtalimide
2-(10-hydroxydecyl)-1H-isoindole-1,3(2H)-dione
Conditions | Yield |
---|---|
With cetyltributylphosphonium bromide In toluene at 110℃; for 1.5h; | 98% |
In N,N-dimethyl-formamide at 80℃; for 2h; | 98% |
In N,N-dimethyl-formamide at 100℃; for 20h; | 97% |
In N,N-dimethyl-formamide at 100℃; for 20h; | 97% |
Conditions | Yield |
---|---|
With sodium hydroxide; selenium; hydrazine hydrate In methanol Condensation; | 98% |
Conditions | Yield |
---|---|
With ammonia; lithium In dimethyl sulfoxide | 97% |
1-bromo-10-decanol
1,1-(ethylenedioxy)-3-(10-hydroxydecyl)-4-methyl-3-(phenylsulfonyl)-cyclohexane
Conditions | Yield |
---|---|
Stage #1: 1,1-(ethylenedioxy)-4-methyl-3-(phenylsulfonyl)-cyclohexane With n-butyllithium; triphenylmethane In tetrahydrofuran at -78 - 20℃; for 1.16667h; Stage #2: 1-bromo-10-decanol With Hexamethylphosphorous triamide In tetrahydrofuran at -78 - -20℃; for 2h; | 97% |
1-bromo-10-decanol
triphenylmethane
1,1-(ethylenedioxy)-4-methyl-3-(phenylsulfonyl)-cyclohexane
1,1-(ethylenedioxy)-3-(10-hydroxydecyl)-4-methyl-3-(phenylsulfonyl)-cyclohexane
Conditions | Yield |
---|---|
With n-butyllithium; ammonium chloride In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide | 97% |
With n-butyllithium; ammonium chloride In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide | 97% |
With n-butyllithium In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide | 97% |
1-bromo-10-decanol
2-mercaptothiazoline
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol; water at 25 - 60℃; for 0.3h; Microwave irradiation; | 97% |
1-bromo-10-decanol
(3-methylbutyl)magnesium bromide
13-methyltetradecan-1-ol
Conditions | Yield |
---|---|
With dilithium tetrachlorocuprate In tetrahydrofuran | 96% |
With dilithium tetrachlorocuprate In tetrahydrofuran at -78 - 20℃; Grignard reaction; | 96% |
With dilithium tetrachlorocuprate In tetrahydrofuran at -78 - 20℃; for 12h; | 95% |
With dilithium tetrachlorocuprate In tetrahydrofuran at -78 - 20℃; for 12h; | 94% |
4,4'-bipyridine
1-bromo-10-decanol
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 140℃; for 16h; | 96% |
1-bromo-10-decanol
methyl 2-hydroxy-4-benzyloxybenzoate
methyl 2-[(10-hydroxy)decyloxy]-4-benzyloxybenzoate
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 80℃; for 20h; | 96% |
1-bromo-10-decanol
3-methoxy-4-methylthiophene
3-(10-bromodecyloxy)-4-methylthiophene
Conditions | Yield |
---|---|
With sodium hydrogen sulfate In toluene at 100℃; for 24h; | 96% |
With sodium hydrogen sulfate In toluene at 100℃; for 24h; | 96% |
1-bromo-10-decanol
10-iododecan-1-ol
Conditions | Yield |
---|---|
With sodium iodide In acetone Reflux; Inert atmosphere; | 95% |
With sodium iodide In acetone Ambient temperature; | 94% |
With sodium iodide In acetone for 24h; Finkelstein Reaction; Reflux; Inert atmosphere; | 88% |
Conditions | Yield |
---|---|
Stage #1: i-pentyl bromide With magnesium In tetrahydrofuran at 20℃; Stage #2: 1-bromo-10-decanol With dilithium tetrachlorocuprate In tetrahydrofuran at -78 - 20℃; Further stages.; | 95% |
Conditions | Yield |
---|---|
Stage #1: isopropyl bromide With magnesium In tetrahydrofuran for 0.5h; Inert atmosphere; Stage #2: 1-bromo-10-decanol With dilithium tetrachlorocuprate In tetrahydrofuran at -78 - 20℃; for 1h; Inert atmosphere; | 95% |
Stage #1: isopropyl bromide With dilithium tetrachlorocuprate; magnesium In tetrahydrofuran Stage #2: 1-bromo-10-decanol In tetrahydrofuran at -78 - 0℃; | 89% |
1-bromo-10-decanol
4,4-dimethyl-1,1-(ethylenedioxy)-3-(10-hydroxydecyl)-3-(phenylsulfonyl)-cyclohexane
Conditions | Yield |
---|---|
Stage #1: 4,4-dimethyl-1,1-(ethylenedioxy)-3-(phenylsulfonyl)-cyclohexane With n-butyllithium; triphenylmethane In tetrahydrofuran at -78 - 20℃; for 1.16667h; Stage #2: 1-bromo-10-decanol With Hexamethylphosphorous triamide In tetrahydrofuran at -78 - -20℃; for 2h; | 94% |
1-bromo-10-decanol
triphenylmethane
4,4-dimethyl-1,1-(ethylenedioxy)-3-(phenylsulfonyl)-cyclohexane
4,4-dimethyl-1,1-(ethylenedioxy)-3-(10-hydroxydecyl)-3-(phenylsulfonyl)-cyclohexane
Conditions | Yield |
---|---|
With n-butyllithium; ammonium chloride In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide | 94% |
With n-butyllithium; ammonium chloride In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide | 94% |
With n-butyllithium In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide | 94% |
1-methyl-1H-imidazole
1-bromo-10-decanol
1-(10-hydroxydecyl)-3-methylimidazolium bromide
Conditions | Yield |
---|---|
at 20℃; Inert atmosphere; | 94% |
Conditions | Yield |
---|---|
With melamine-N2,N4,N6-trisulfonic acid In dichloromethane at 20℃; Inert atmosphere; | 94% |
1-bromo-10-decanol
[bromo(difluoro)methyl](trimethyl)silane
Conditions | Yield |
---|---|
With potassium hydrogenfluoride In water at 20℃; for 12h; | 94% |
Conditions | Yield |
---|---|
In ammonia; N,N-dimethyl-formamide at 50℃; for 2h; | 93.4% |
Conditions | Yield |
---|---|
In acetonitrile at 80℃; for 22h; | 93.1% |
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