Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:13019-22-2
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Name 9-Decen-1-ol Molecular Structure Molecular Formula C10H20O Molecular Weight 156
Cas:13019-22-2
Min.Order:25 Kilogram
Negotiable
Type:Trading Company
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:13019-22-2
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
Cas:13019-22-2
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
Cas:13019-22-2
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:13019-22-2
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
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Cas:13019-22-2
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
PRODUCT DETAILS
Cas:13019-22-2
Min.Order:500 Kilogram
FOB Price: $1.0 / 2.0
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff
Product name: 9-Decen-1-ol CAS No.:13019-22-2 Molecule Formula:C10H20O Molecule Weight:156.27 Purity: 99.0% Package: 200kg/drum Description:Colorless liquid Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:13019-22-2
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:13019-22-2
Min.Order:1 Metric Ton
FOB Price: $7.0 / 8.0
Type:Trading Company
inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re
Cas:13019-22-2
Min.Order:0
Negotiable
Type:Other
inquiryAN ISO 9001, ISO 14001, ISO 22022 CERTIFIED FACTORY,HALAL 、KOSHER、FCC AND FDA CERTIFICATE ARE AVAILABLE. Storage:1000KG Package:25/170KG per drum Application:Daily flavor, food additives Transportation:by air /by sea or by courier like DHL or Fedex P
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:Powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary and sec
9-Decen-1-ol cas 13019-22-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
methyl 9-decenoate
9-Decen-1-ol
Conditions | Yield |
---|---|
Stage #1: methyl 9-decenoate With lithium aluminium tetrahydride In tetrahydrofuran at 20℃; for 5.5h; Cooling; Stage #2: With sodium hydroxide In tetrahydrofuran; water at 20℃; Reagent/catalyst; Concentration; Solvent; Temperature; Time; | 98.3% |
With lithium aluminium tetrahydride In tetrahydrofuran at 15 - 20℃; for 5.5h; Inert atmosphere; | 98.3% |
With sodium bis(2-methoxyethoxy)aluminium dihydride In toluene at 15 - 20℃; for 2h; Sealed tube; Cooling with ice; Inert atmosphere; | 97.14% |
1-(tetrahydro-2-pyranyloxy)-9-decene
9-Decen-1-ol
Conditions | Yield |
---|---|
With copper dichloride In methanol at 20℃; Hydrolysis; | 95% |
With CuCl2*2H2O In methanol at 20℃; for 1.25h; | 95% |
decane-1,2,10-triol
9-Decen-1-ol
Conditions | Yield |
---|---|
With rhenium(VII) oxide; triphenylphosphine at 165℃; for 1h; | 90% |
1,10-Decanediol
9-Decen-1-ol
Conditions | Yield |
---|---|
With 1-hexadecylcarboxylic acid at 340℃; for 5h; Temperature; Reagent/catalyst; Molecular sieve; | 88% |
With 1-hexadecylcarboxylic acid; stearic acid at 330 - 350℃; under 700 Torr; for 150h; | 80% |
Conditions | Yield |
---|---|
With 1-hexadecylcarboxylic acid at 340℃; for 6h; Molecular sieve; | A n/a B 88% |
9-decenal
9-Decen-1-ol
Conditions | Yield |
---|---|
With manganese; water; 2,4,6-collidine hydrochloride In tetrahydrofuran at 20℃; chemoselective reaction; | 84% |
trans-9-decenoic acid ethyl ester
9-Decen-1-ol
Conditions | Yield |
---|---|
With styrene; [RuCl2(N,N'-(ethane-1,2-diyl)bis(1-(2-(diphenylphosphaneyl)phenyl)methanimine))]; potassium methanolate; hydrogen at 80℃; under 37503.8 Torr; for 5h; Time; Inert atmosphere; Autoclave; chemoselective reaction; | 84% |
With styrene; [RuCl2(N,N'-(ethane-1,2-diyl)bis(1-(2-(diphenylphosphaneyl)phenyl)methanimine))]; potassium methanolate; hydrogen at 80℃; under 37503.8 Torr; for 5h; Inert atmosphere; Autoclave; | 84% |
dec-9-enoic acid
9-Decen-1-ol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; | 80% |
With lithium aluminium tetrahydride In tetrahydrofuran at 0 - 20℃; | 64% |
With nonan-1-al; samarium diiodide; samarium(III) trifluoromethanesulfonate In tetrahydrofuran; methanol; potassium hydroxide at 20℃; for 0.0833333h; Reduction; | 96 % Chromat. |
9-Decen-1-ol
Conditions | Yield |
---|---|
With ammonium peroxydisulfate; 9-(2-mesityl)-10-methylacridinium perchlorate In dichloromethane; water at 20 - 30℃; for 2h; Irradiation; Green chemistry; | 80% |
Stage #1: 1-((dec-9-en-1-yloxy)methyl)-4-methoxybenzene With sodium hydrogencarbonate; bis-[(trifluoroacetoxy)iodo]benzene; meso-2,5-bis(methoxycarbonyl)-2,5-dimethylpyrrolidine-1-oxyl In dichloromethane at 20℃; for 2h; Stage #2: With water In dichloromethane chemoselective reaction; | 79% |
((dec-9-en-1-yloxy)methyl)benzene
A
9-Decen-1-ol
B
9-bromo-decane-1-ol
Conditions | Yield |
---|---|
With triphenylphosphine hydrobromide In acetonitrile for 12h; Reflux; | A 63% B 8% |
((dec-9-en-1-yloxy)methyl)benzene
9-Decen-1-ol
Conditions | Yield |
---|---|
With barium carbonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile at 20℃; for 16h; Irradiation; | 52% |
11-hydroxyundecanoic acid
A
1-Decanol
B
9-Decen-1-ol
C
1,20-eicosanediol
Conditions | Yield |
---|---|
With potassium methanolate In methanol at 40℃; electrolysis: anode: platinum foil; current source: galvanostat; current density 200 mA cm-2; current consumption: 3.03 F mol-1; cell voltage 50-60 V; Yield given; | A n/a B n/a C 42% |
With potassium methanolate In methanol at 40℃; electrolysis: anode: platinum foil; current source: galvanostat; current density 200 mA cm-2; current consumption: 3.03 F mol-1; cell voltage 50-60 V; Yields of byproduct given; | A n/a B n/a C 42% |
1-bromo-10-decanol
9-Decen-1-ol
Conditions | Yield |
---|---|
With potassium tert-butylate In tetrahydrofuran; toluene at 0℃; for 0.5h; | 20% |
2,13-dioxa-tetradecanedioic acid diethyl ester
A
1,10-decadiene
B
1,10-Decanediol
C
9-Decen-1-ol
D
carbonic acid ethyl ester-(10-hydroxy-decyl ester)
Conditions | Yield |
---|---|
at 500℃; Produkt 5-7:Aethanol,Kohlensaeure-aethylester-dec-9-enylester,Aethylen.Pyrolysis; |
2,13-dioxa-tetradecanedioic acid diethyl ester
9-Decen-1-ol
Conditions | Yield |
---|---|
at 500℃; |
10-hydroxy-2-decanone
9-Decen-1-ol
Conditions | Yield |
---|---|
aluminum oxide Heating; |
9-decen-1-yl acetate
9-Decen-1-ol
Conditions | Yield |
---|---|
With sodium hydroxide In methanol |
Conditions | Yield |
---|---|
With copper(I) bromide dimethylsulfide complex; lithium bromide 1.) Et2O; 2.) -50 deg C, then 30 min, -30 deg C; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With hydrogenchloride; Schwartz's reagent Yield given; Multistep reaction. Yields of byproduct given; |
9-Decen-1-ol
Conditions | Yield |
---|---|
at 290℃; |
Conditions | Yield |
---|---|
With sodium hydroxide |
10-chlorodecanol
A
9-Decen-1-ol
Conditions | Yield |
---|---|
bei Destillation; |
1,10-decadiene
A
1,10-Decanediol
B
1-Decanol
C
9-Decen-1-ol
D
8-decene-1-ol
Conditions | Yield |
---|---|
Stage #1: 1,10-decadiene With triisobutylaluminum; bis-triphenylphosphine-palladium(II) chloride In dichloromethane at 25℃; for 12h; Stage #2: With sodium hydroxide; oxygen In dichloromethane | A 16 % Spectr. B 27 % Spectr. C 11 % Spectr. D 24 % Spectr. |
Methyl 10-undecenoate
9-Decen-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydroboration-oxidation 2: 1M potassium methoxide / methanol / 40 °C / electrolysis: anode: platinum foil; current source: galvanostat; current density 200 mA cm-2; current consumption: 3.03 F mol-1; cell voltage 50-60 V View Scheme |
12-methoxy-12-oxododecanoic acid
9-Decen-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1M potassium methoxide / methanol / 40 - 45 °C / electrolysis: anode: platinum foil; current source: galvanostat; current density 220 mA cm-2; current consumption: 1.25 F mol-1; cell voltage 40-70 V 2: hydroboration-oxidation 3: 1M potassium methoxide / methanol / 40 °C / electrolysis: anode: platinum foil; current source: galvanostat; current density 200 mA cm-2; current consumption: 3.03 F mol-1; cell voltage 50-60 V View Scheme |
dodecanedioic acid dimethyl ester
9-Decen-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: barium hydroxide octahydrate / methanol / 4 d, -10 deg C; 10 h, RT 2: 1M potassium methoxide / methanol / 40 - 45 °C / electrolysis: anode: platinum foil; current source: galvanostat; current density 220 mA cm-2; current consumption: 1.25 F mol-1; cell voltage 40-70 V 3: hydroboration-oxidation 4: 1M potassium methoxide / methanol / 40 °C / electrolysis: anode: platinum foil; current source: galvanostat; current density 200 mA cm-2; current consumption: 3.03 F mol-1; cell voltage 50-60 V View Scheme |
oleyl acetate
9-Decen-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: (i) O3, CH2Cl2, (ii) Ph3P 2: (i) K, HMPT, (ii) /BRN= 1769551/ 3: aq. NaOH / methanol View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 2: (i) O3, CH2Cl2, (ii) Ph3P 3: (i) K, HMPT, (ii) /BRN= 1769551/ 4: aq. NaOH / methanol View Scheme |
9-acetoxynonal
9-Decen-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i) K, HMPT, (ii) /BRN= 1769551/ 2: aq. NaOH / methanol View Scheme |
9-Decen-1-ol
9-decenal
Conditions | Yield |
---|---|
With oxalyl dichloride; dimethyl sulfoxide; triethylamine In dichloromethane at -60 - 20℃; for 0.333333h; | 100% |
With Bu4N In 1,2-dichloro-ethane at 50℃; for 9h; | 99% |
With aluminum oxide; pyridinium chlorochromate In dichloromethane at 20℃; for 3h; | 97% |
9-Decen-1-ol
10-bromodec-1-ene
Conditions | Yield |
---|---|
With carbon tetrabromide; triphenylphosphine at 20℃; for 22h; Bromination; | 100% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 0 - 20℃; | 100% |
With carbon tetrabromide; triphenylphosphine In dichloromethane at 0 - 20℃; for 15h; | 100% |
9-Decen-1-ol
9,10-dibromodecan-1-ol
Conditions | Yield |
---|---|
With bromine In dichloromethane at -45 - 20℃; | 100% |
With bromine In tetrachloromethane at -5℃; for 1h; | 95% |
With bromine In dichloromethane |
9-Decen-1-ol
methanesulfonyl chloride
dec-9-en-1-yl methanesulfonate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane; water; sodium sulfate | 100% |
With triethylamine In dichloromethane; water; sodium sulfate | 100% |
With triethylamine In dichloromethane at 0℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; | 100% |
With dmap; triethylamine In dichloromethane at 20℃; Inert atmosphere; | 100% |
With pyridine at 0 - 5℃; for 3.5h; Inert atmosphere; | 97% |
9-Decen-1-ol
tert-butyldimethylsilyl chloride
tert-butyl(dec-9-en-1-yloxy)dimethylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; | 100% |
With 1H-imidazole; dmap In dichloromethane at 0 - 20℃; Inert atmosphere; | 99% |
With 1H-imidazole; dmap | 98% |
9-Decen-1-ol
10-iodo-1-decene
Conditions | Yield |
---|---|
With 1H-imidazole; iodine; triphenylphosphine In diethyl ether; acetonitrile at 20℃; for 4h; | 100% |
With 1H-imidazole; iodine; triphenylphosphine In dichloromethane for 2h; Darkness; Inert atmosphere; | 91% |
With 1H-imidazole; iodine | 88% |
Conditions | Yield |
---|---|
AuCl(xanthphos) In acetone at 50℃; for 8h; | 100% |
With copper (I) tert-butoxide; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In toluene at 25℃; for 2h; | 95% |
9-Decen-1-ol
dec-9-en-1-yl methanesulfonate
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 100% |
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; for 2h; | 100% |
Stage #1: 9-Decen-1-ol With triethylamine In dichloromethane at 0℃; for 0.166667h; Inert atmosphere; Stage #2: benzoyl chloride In dichloromethane at 0℃; for 0.5h; Inert atmosphere; | 94% |
With pyridine In dichloromethane |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; Steglich Esterification; | 100% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With pyridine at 60℃; for 3h; | 99% |
zeolite HSZ-360 In neat (no solvent) at 60℃; for 1h; | 97% |
With sodium acetate at 68℃; for 4h; Schlenk technique; Inert atmosphere; | 95.6% |
9-Decen-1-ol
10-chloro-1-decene
Conditions | Yield |
---|---|
With 2-chloro-1,3-dimethylimidazolinium chloride; triethylamine In dichloromethane at 20℃; for 21h; Chlorination; | 99% |
With thionyl chloride In dichloromethane; N,N-dimethyl-formamide at 55℃; for 16h; | 93% |
With N-chloro-succinimide; triphenylphosphine In tetrahydrofuran for 9h; Inert atmosphere; | 80% |
9-Decen-1-ol
triisopropylsilyl trifluoromethanesulfonate
(dec-9-en-1-yloxy)triisopropylsilane
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; Substitution; | 99% |
9-Decen-1-ol
2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyl chloride
dec-9-enyl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate
Conditions | Yield |
---|---|
Stage #1: 9-Decen-1-ol With sodium hydride In tetrahydrofuran; mineral oil at 20℃; for 0.5h; Stage #2: 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carbonyl chloride In tetrahydrofuran; mineral oil at 80℃; | 99% |
9-Decen-1-ol
Conditions | Yield |
---|---|
Stage #1: 9-Decen-1-ol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodine In dichloromethane at 0 - 20℃; for 1h; Inert atmosphere; Stage #2: With ammonia; iodine In dichloromethane; water at 20℃; for 2h; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 1.5h; | 99% |
Conditions | Yield |
---|---|
With 1H-imidazole In dichloromethane at 0 - 20℃; | 99% |
9-Decen-1-ol
tert-butylchlorodiphenylsilane
Conditions | Yield |
---|---|
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 48h; Inert atmosphere; | 99% |
Stage #1: 9-Decen-1-ol With 1H-imidazole; dmap In dichloromethane at 0℃; for 0.0833333h; Inert atmosphere; Stage #2: tert-butylchlorodiphenylsilane In dichloromethane at 0 - 20℃; for 3h; Inert atmosphere; | 81% |
Conditions | Yield |
---|---|
With dmap In dichloromethane at 0 - 20℃; Inert atmosphere; | 99% |
9-Decen-1-ol
1-Decanol
Conditions | Yield |
---|---|
With hydrogen; TMSB; palladium In ethanol at 20℃; under 760 Torr; for 17h; | 98% |
Hydrogenation; | |
With amine functionalized polymer; carboxylic acid-derived silica colloids; hydrogen; carbocyclic acid-derived Pd-MMPC |
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; for 2.25h; | 98% |
With sodium hydride In tetrahydrofuran at 0 - 20℃; for 4h; | 95% |
Stage #1: 9-Decen-1-ol With sodium hydride In nujol; N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere; Stage #2: benzyl bromide In nujol; N,N-dimethyl-formamide at 20℃; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With iodine for 2.5h; Reflux; chemoselective reaction; | 98% |
titanium(IV) tetraethanolate for 24h; | 94% |
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In dichloromethane at 20℃; for 0.25h; Inert atmosphere; | 98% |
With pyridinium p-toluenesulfonate In dichloromethane at 20℃; for 16h; | 98% |
With pyridinium p-toluenesulfonate In dichloromethane at 20℃; for 1.5h; Alkylation; | 92% |
Conditions | Yield |
---|---|
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In potassium hydroxide at 20 - 25℃; for 1.5h; pH=11.5; Schotten-Baumann-type reaction; | 98% |
With 1-methyl-1H-imidazole; N,N,N,N,-tetramethylethylenediamine; potassium carbonate In acetonitrile at 0 - 5℃; for 1h; | 98% |
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 98% |
9-Decen-1-ol
3-phenylpropanoic acid methyl ester
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; diphenylammonium trifluoromethanesulfonate In toluene at 80 - 110℃; for 24h; Esterification; | 97% |
With sulfonated polypyrene In n-heptane at 80℃; for 16h; | 91% |
With high p-toluenesulfonate content diphenylamine and terephthalaldehyde resin In neat (no solvent) at 110℃; for 6h; | 83% |
Conditions | Yield |
---|---|
Stage #1: 9-Decen-1-ol With sodium In tetrahydrofuran Heating; Stage #2: 2,6-Dibromopyridine In N,N-dimethyl-formamide at 95℃; | 97% |
Stage #1: 9-Decen-1-ol With sodium In tetrahydrofuran Heating; Stage #2: 2,6-Dibromopyridine In N,N-dimethyl-formamide at 95℃; for 16h; | 97% |
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