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inquiryN1-(4,5-DICHLORO-2-NITROPHENYL)ACETAMIDE CAS:5462-30-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high q
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inquiryN-(4,5-dichloro-2-aminophenyl)AcetamideAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
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Acetamide,N-(4,5-dichloro-2-nitrophenyl)- cas 5462-30-6Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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Conditions | Yield |
---|---|
With sulfuric acid; sulfur trioxide; nitric acid at 3 - 13℃; for 6.5h; | 95.23% |
With sulfuric acid; nitric acid 1.) 0 deg C, 10 min, 2.) RT, 30 min; |
Conditions | Yield |
---|---|
With sulfuric acid; sulfur trioxide; nitric acid at 3 - 13℃; for 6.5h; | A 92% B 6% |
ethyl nitrate
N-(3,4-dichlorophenyl)acetamide
N-(4,5-dichloro-2-nitrophenyl)acetamide
Conditions | Yield |
---|---|
With sulfuric acid |
acetic anhydride
m,p-dichloroaniline
N-(4,5-dichloro-2-nitrophenyl)acetamide
Conditions | Yield |
---|---|
With nitric acid |
Conditions | Yield |
---|---|
With nitric acid mann trennt durch fraktionierte Krystallisation aus Alkohol; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: acetic acid / 0.25 h / Heating 2: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min View Scheme |
N-(4,5-dichloro-2-nitrophenyl)acetamide
Conditions | Yield |
---|---|
With hydrogen In tetrahydrofuran; water at 120℃; under 37503.8 Torr; for 15h; chemoselective reaction; | 93% |
With formic acid; triethylamine In tetrahydrofuran at 100℃; for 15h; Inert atmosphere; Sealed tube; chemoselective reaction; | 93% |
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 100℃; for 3h; | 88% |
N-(4,5-dichloro-2-nitrophenyl)acetamide
4-hydroxy-benzoic acid
4-(2'-Chloro-4'-nitro-5'-acetamidophenoxy)benzoic acid
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 100℃; for 2.5h; | 87% |
Stage #1: 4-hydroxy-benzoic acid With potassium carbonate In dimethyl sulfoxide at 75℃; for 0.25h; Stage #2: N-(4,5-dichloro-2-nitrophenyl)acetamide In dimethyl sulfoxide at 110℃; for 6h; | 3.1 g |
N-(4,5-dichloro-2-nitrophenyl)acetamide
C14H19ClN4O3
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 90℃; for 16h; | 79% |
N-(4,5-dichloro-2-nitrophenyl)acetamide
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 100℃; for 2h; | A 17% B 68% |
Conditions | Yield |
---|---|
With sulfuric acid at 120℃; | |
With sulfuric acid at 100℃; for 0.25h; |
N-(4,5-dichloro-2-nitrophenyl)acetamide
4,5-Dichlor-2-nitro-N-nitroso-acetanilid
Conditions | Yield |
---|---|
With nitrosylsulfuric acid; sodium acetate |
N-(4,5-dichloro-2-nitrophenyl)acetamide
benzene
4.5-Dichlor-2-nitro-biphenyl
Conditions | Yield |
---|---|
(i) NaOAc, P2O5, Ac2O, AcOH, NOHSO4, (ii) /BRN= 969212/; Multistep reaction; |
N-(4,5-dichloro-2-nitrophenyl)acetamide
4,5-dichloro-2-nitrophenylazide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: conc. sulfuric acid / 0.25 h / 100 °C 2: 1.) aq. HCl, NaNO2, 2.) aq. NaN3, sodium acetate / 1.) 0 deg C, 15 min View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: conc. sulfuric acid / 0.25 h / 100 °C 2: 1.) aq. HCl, NaNO2, 2.) aq. NaN3, sodium acetate / 1.) 0 deg C, 15 min 3: toluene / 2 h / Heating View Scheme |
Conditions | Yield |
---|---|
With sulfuric acid; sulfur trioxide; nitric acid at 3 - 13℃; for 6.5h; | 95.23% |
With sulfuric acid; nitric acid 1.) 0 deg C, 10 min, 2.) RT, 30 min; |
Conditions | Yield |
---|---|
With sulfuric acid; sulfur trioxide; nitric acid at 3 - 13℃; for 6.5h; | A 92% B 6% |
ethyl nitrate
N-(3,4-dichlorophenyl)acetamide
N-(4,5-dichloro-2-nitrophenyl)acetamide
Conditions | Yield |
---|---|
With sulfuric acid |
acetic anhydride
m,p-dichloroaniline
N-(4,5-dichloro-2-nitrophenyl)acetamide
Conditions | Yield |
---|---|
With nitric acid |
Conditions | Yield |
---|---|
With nitric acid mann trennt durch fraktionierte Krystallisation aus Alkohol; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: acetic acid / 0.25 h / Heating 2: 60percent nitric acid, conc. sulfuric acid / 1.) 0 deg C, 10 min, 2.) RT, 30 min View Scheme |
N-(4,5-dichloro-2-nitrophenyl)acetamide
Conditions | Yield |
---|---|
With hydrogen In tetrahydrofuran; water at 120℃; under 37503.8 Torr; for 15h; chemoselective reaction; | 93% |
With formic acid; triethylamine In tetrahydrofuran at 100℃; for 15h; Inert atmosphere; Sealed tube; chemoselective reaction; | 93% |
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 100℃; for 3h; | 88% |
N-(4,5-dichloro-2-nitrophenyl)acetamide
4-hydroxy-benzoic acid
4-(2'-Chloro-4'-nitro-5'-acetamidophenoxy)benzoic acid
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 100℃; for 2.5h; | 87% |
Stage #1: 4-hydroxy-benzoic acid With potassium carbonate In dimethyl sulfoxide at 75℃; for 0.25h; Stage #2: N-(4,5-dichloro-2-nitrophenyl)acetamide In dimethyl sulfoxide at 110℃; for 6h; | 3.1 g |
N-(4,5-dichloro-2-nitrophenyl)acetamide
C14H19ClN4O3
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 90℃; for 16h; | 79% |
N-(4,5-dichloro-2-nitrophenyl)acetamide
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide at 100℃; for 2h; | A 17% B 68% |
Conditions | Yield |
---|---|
With sulfuric acid at 120℃; | |
With sulfuric acid at 100℃; for 0.25h; |
N-(4,5-dichloro-2-nitrophenyl)acetamide
4,5-Dichlor-2-nitro-N-nitroso-acetanilid
Conditions | Yield |
---|---|
With nitrosylsulfuric acid; sodium acetate |
N-(4,5-dichloro-2-nitrophenyl)acetamide
benzene
4.5-Dichlor-2-nitro-biphenyl
Conditions | Yield |
---|---|
(i) NaOAc, P2O5, Ac2O, AcOH, NOHSO4, (ii) /BRN= 969212/; Multistep reaction; |
N-(4,5-dichloro-2-nitrophenyl)acetamide
4,5-dichloro-2-nitrophenylazide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: conc. sulfuric acid / 0.25 h / 100 °C 2: 1.) aq. HCl, NaNO2, 2.) aq. NaN3, sodium acetate / 1.) 0 deg C, 15 min View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: conc. sulfuric acid / 0.25 h / 100 °C 2: 1.) aq. HCl, NaNO2, 2.) aq. NaN3, sodium acetate / 1.) 0 deg C, 15 min 3: toluene / 2 h / Heating View Scheme |
N-(4,5-dichloro-2-nitrophenyl)acetamide
3-amino-6,7-dichloro-2-quinoxalinecarbonitrile 1,4-di-N-oxide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: conc. sulfuric acid / 0.25 h / 100 °C 2: 1.) aq. HCl, NaNO2, 2.) aq. NaN3, sodium acetate / 1.) 0 deg C, 15 min 3: toluene / 2 h / Heating 4: 48 percent / triethylamine / dimethylformamide / 24 h / 0 - 20 °C View Scheme |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 12h; Industry scale; |
N-(4,5-dichloro-2-nitrophenyl)acetamide
4-chloro-5-(2,3-dichlorophenoxy)-2-nitroaniline
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C / Industry scale 2: sodium hydroxide; water / methanol / 4 h / 50 °C / Industry scale View Scheme |
N-(4,5-dichloro-2-nitrophenyl)acetamide
6-chloro-5-(2,3-dichlorophenoxy)-2-(methylthio)-1H-benzo[d]imidazole
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C / Industry scale 2.1: sodium hydroxide; water / methanol / 4 h / 50 °C / Industry scale 3.1: hydrogen; sodium hydroxide / Raney nickel / methanol / 12 h / 100 °C / Industry scale 4.1: sodium hydroxide / methanol / 6 h / Reflux; Industry scale 4.2: 4 h / 60 - 90 °C / Industry scale 5.1: sodium carbonate / water; methanol / 2 h / 60 °C View Scheme | |
Multi-step reaction with 7 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C / Industry scale 2.1: sodium hydroxide; water / methanol / 4 h / 50 °C / Industry scale 3.1: hydrogen; sodium hydroxide / Raney nickel / methanol / 12 h / 100 °C / Industry scale 4.1: sodium hydroxide / methanol / 6 h / Reflux; Industry scale 4.2: 4 h / 60 - 90 °C / Industry scale 5.1: methanol / 6 h / 40 - 65 °C / Industry scale 6.1: hydrogenchloride / water; methanol / 1 h / 20 °C 7.1: ammonia / water View Scheme |
N-(4,5-dichloro-2-nitrophenyl)acetamide
6-chloro-5-(2,3-dichlorophenoxy)-1H-benzimidazole-2-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C / Industry scale 2.1: sodium hydroxide; water / methanol / 4 h / 50 °C / Industry scale 3.1: hydrogen; sodium hydroxide / Raney nickel / methanol / 12 h / 100 °C / Industry scale 4.1: sodium hydroxide / methanol / 6 h / Reflux; Industry scale 4.2: 4 h / 60 - 90 °C / Industry scale View Scheme | |
Multi-step reaction with 3 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 - 90 °C / Large scale 1.2: 4 h / 50 °C / Large scale 2.1: sodium hydroxide; hydrogen / methanol / 12 h / 100 °C / Inert atmosphere 3.1: methanol / 6 h / Reflux 3.2: 4 h / 60 - 90 °C View Scheme |
N-(4,5-dichloro-2-nitrophenyl)acetamide
6-chloro-5-(2,3-dichlorophenoxy)-2-(methylthio)-1H-benzimidazole hydrochloride
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C / Industry scale 2.1: sodium hydroxide; water / methanol / 4 h / 50 °C / Industry scale 3.1: hydrogen; sodium hydroxide / Raney nickel / methanol / 12 h / 100 °C / Industry scale 4.1: sodium hydroxide / methanol / 6 h / Reflux; Industry scale 4.2: 4 h / 60 - 90 °C / Industry scale 5.1: methanol / 6 h / 40 - 65 °C / Industry scale 6.1: hydrogenchloride / water; methanol / 1 h / 20 °C View Scheme |
N-(4,5-dichloro-2-nitrophenyl)acetamide
4-chloro-5-(2,3-dichlorophenoxy)-1,2-phenylenediamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C / Industry scale 2: sodium hydroxide; water / methanol / 4 h / 50 °C / Industry scale 3: hydrogen; sodium hydroxide / Raney nickel / methanol / 12 h / 100 °C / Industry scale View Scheme |
N-(4,5-dichloro-2-nitrophenyl)acetamide
6-chloro-5-(2,3-dichlorophenoxy)-2-(methylthio)-1H-benzimidazole methylsulfate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 90 °C / Industry scale 2.1: sodium hydroxide; water / methanol / 4 h / 50 °C / Industry scale 3.1: hydrogen; sodium hydroxide / Raney nickel / methanol / 12 h / 100 °C / Industry scale 4.1: sodium hydroxide / methanol / 6 h / Reflux; Industry scale 4.2: 4 h / 60 - 90 °C / Industry scale 5.1: methanol / 6 h / 40 - 65 °C / Industry scale View Scheme |
2,3-dichlorophenol
N-(4,5-dichloro-2-nitrophenyl)acetamide
4-chloro-5-(2,3-dichlorophenoxy)-2-nitroaniline
Conditions | Yield |
---|---|
Stage #1: 2,3-dichlorophenol; N-(4,5-dichloro-2-nitrophenyl)acetamide With potassium carbonate In N,N-dimethyl-formamide at 20 - 90℃; for 12h; Large scale; Stage #2: With sodium hydroxide In methanol; water; N,N-dimethyl-formamide at 50℃; for 4h; Large scale; | 2 kg |
N-(4,5-dichloro-2-nitrophenyl)acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 - 90 °C / Large scale 1.2: 4 h / 50 °C / Large scale 2.1: sodium hydroxide; hydrogen / methanol / 12 h / 100 °C / Inert atmosphere 3.1: methanol / 6 h / Reflux 3.2: 4 h / 60 - 90 °C 4.1: methanol / 6 h / 40 - 65 °C / Large scale View Scheme |
N-(4,5-dichloro-2-nitrophenyl)acetamide
triclabendazole
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 - 90 °C / Large scale 1.2: 4 h / 50 °C / Large scale 2.1: sodium hydroxide; hydrogen / methanol / 12 h / 100 °C / Inert atmosphere 3.1: methanol / 6 h / Reflux 3.2: 4 h / 60 - 90 °C 4.1: methanol; water / 0.5 h / 60 °C 4.2: 1.5 h / 60 °C View Scheme |
N-(4,5-dichloro-2-nitrophenyl)acetamide
4-(2'-Chloro-4'-nitro-5'-aminophenoxy)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: potassium carbonate / dimethyl sulfoxide / 0.25 h / 75 °C 1.2: 6 h / 110 °C 2.1: potassium hydroxide / water / 60 °C View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / dimethyl sulfoxide / 2.5 h / 100 °C 2: potassium hydroxide; water / 1 h / 60 °C View Scheme |
N-(4,5-dichloro-2-nitrophenyl)acetamide
4-(2'-Chloro-4',5'-diaminophenoxy)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: potassium carbonate / dimethyl sulfoxide / 0.25 h / 75 °C 1.2: 6 h / 110 °C 2.1: potassium hydroxide / water / 60 °C 3.1: tin(II) chloride dihdyrate; hydrogenchloride / water / 1 h / 90 °C View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / dimethyl sulfoxide / 2.5 h / 100 °C 2: potassium hydroxide; water / 1 h / 60 °C 3: tin(II) chloride dihdyrate; hydrogenchloride / water / 1 h / 90 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate / dimethyl sulfoxide / 3 h / 100 °C 2: tin(II) chloride dihdyrate; hydrogenchloride; acetic acid / water / 1 h / 100 °C View Scheme |
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