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2,3-Dichlorophenol CAS: 576-24-9 Application:2,3-Dichlorophenol CAS: 576-24-9
2,3-Dichlorophenol CAS: 576-24-9Appearance:White powder Storage:Store in a dry, dark, ventilated place Package:As requested Application:Organic intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for small amount. By air
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inquiry2,3-Dichlorophenol Basic information Product Name: 2,3-Dichlorophenol Synonyms: 2,3-dichloro-pheno;2,3-DICHLOROPHENOL;2 3-DICHLOROPHENOL 1000MG NEAT;2,3-DICHLOR-PHENOL;2,3-Dichlorophenol,98+%;Phenol, 2,3-
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inquiryBaiFuChem is a Professional chemical raw material supplier in China, our main products include Biochemical , Pharma Intermediate and Organic chemical etc. BaiFuChem have wealth of products,experience , expertise and state-of-the-art
Conditions | Yield |
---|---|
With wild-type cytochrome P450cam In ethanol at 30℃; for 0.0333333h; pH=7.4; Enzyme kinetics; Further Variations:; Reagents; Oxidation; | A 10% B 90% |
With oxygen; titanium(IV) oxide In perchloric acid at 23℃; for 0.25h; pH=1; Kinetics; Further Variations:; Catalysts; reaction time; UV-irradiation; | |
With (difluoroboryl)dimethylglyoximatocobalt(II) bis(acetonitrile); water; 3-cyano-1-methylquinolinium perchlorate In acetonitrile at 20℃; for 5h; Inert atmosphere; Irradiation; | |
Stage #1: 1,2-dichloro-benzene With formic acid; CoO40W12(5-)*16H2O*5K(1+); lithium formate at 25℃; for 3h; Electrochemical reaction; Stage #2: With perchloric acid In diethyl ether; water at 20℃; for 0.166667h; Reagent/catalyst; |
2,3-dichlorobenzeneboronic acid
2,3-dichlorophenol
Conditions | Yield |
---|---|
With 10-methylacridine-3(10H)-one; oxygen; N-ethyl-N,N-diisopropylamine In water at 20℃; for 42h; Irradiation; Green chemistry; | 88% |
Conditions | Yield |
---|---|
With sodium methylate In N,N,N,N,N,N-hexamethylphosphoric triamide at 120℃; | 50% |
3-monochlorophenol
A
2,5-dichlorophenol
B
3,4-dichlorophenol
C
2,3-dichlorophenol
Conditions | Yield |
---|---|
With oxygen; silica gel; copper dichloride at 350℃; Formation of xenobiotics; Further byproducts.; | A 0.227% B 0.027% C 0.051% D 0.115% |
With oxygen; silica gel; copper dichloride at 375℃; Formation of xenobiotics; Further byproducts.; | A 0.139% B 0.019% C 0.032% D 0.2629% |
3-monochlorophenol
A
2,5-dichlorophenol
B
3,4-dichlorophenol
C
2,3-dichlorophenol
D
2,4,5-trichlorophenol
Conditions | Yield |
---|---|
With oxygen; silica gel; copper dichloride at 300℃; Product distribution; Further Variations:; Temperatures; | A 0.262% B 0.044% C 0.061% D 0.021% |
2-amino-3-chlorophenol
2,3-dichlorophenol
Conditions | Yield |
---|---|
With hydrogenchloride Diazotization.Behandlung der Diazoniumsalz-Loesung mit CuCl2 und konz. wss. HCl; |
2-chloro-3-aminophenol
2,3-dichlorophenol
Conditions | Yield |
---|---|
With hydrogenchloride Diazotization.Behandlung der Diazoniumsalz-Loesung mit Kupfer-Pulver und wss. HCl; |
methanol
sodium methylate
1,2,3-trichlorobenzene
A
2,6-Dichlorophenol
B
2,3-dichloroanisole
C
2,3-dichlorophenol
Conditions | Yield |
---|---|
at 180℃; im Rohr; |
Conditions | Yield |
---|---|
With methanol; sodium methylate at 180℃; |
Conditions | Yield |
---|---|
With N-chloro-3-methyl-2,6-diphenylpiperidin-4-one; hydrogen cation In ethanol; water at 30℃; Product distribution; Thermodynamic data; ΔH(excit.), ΔS(excit.); | |
With N-chloro-3-methyl-2,6-diphenylpiperidin-4-one; hydrogen cation In ethanol; water at 30℃; |
5,6-Dichlorcyclohexan-3,5-dien-1,2-diol
A
3,5-dichlorophenol
B
3,4-dichlorophenol
C
2,3-dichlorophenol
Conditions | Yield |
---|---|
With hydrogenchloride at 23℃; for 24h; different reagent; |
1,2-dichloro-benzene
A
2,6-Dichlorophenol
B
3,4-dichlorophenol
C
2,3-dichlorophenol
Conditions | Yield |
---|---|
With Pseudomonas putida 50802 at 30℃; for 100h; Mechanism; different reagents; |
2,3-dichlorophenol
Conditions | Yield |
---|---|
With sulfuric acid Durchleiten von Wasserdampf; |
2,3-dichlorophenol
Conditions | Yield |
---|---|
With sulfuric acid |
Conditions | Yield |
---|---|
Diazotierung des gebildeten Amins und Behandlung der Diazoniumsalz-Loesung mit Kupfer-Pulver und wss. HCl; |
1H-imidazole
2,3-dichlorophenyl acetate
A
N-Acetylimidazole
B
2,3-dichlorophenol
Conditions | Yield |
---|---|
With sodium dodecyl-sulfate In water; acetonitrile at 25℃; pH=8.92; Kinetics; Acetylation; |
3-monochlorophenol
A
2,5-dichlorophenol
B
3,4-dichlorophenol
C
2,3-dichlorophenol
Conditions | Yield |
---|---|
With sodium hydroxide; sodium hypochlorite; sodium nitrate at 24.85℃; Kinetics; | |
With sodium hydroxide; tert-butylhypochlorite; sodium chloride at 24.85℃; Kinetics; Further Variations:; pH-values; conc.; | |
With 1,3-dichloro-5,5-dimethylhydantoin; diisopropylamine hydrochloride In toluene at 0℃; for 4h; Darkness; Overall yield = 59 %; regioselective reaction; |
2,3,5,6-tetrachlorophenol
A
2,6-Dichlorophenol
B
2,3,6-trichlorophenol
C
2-monochlorophenol
D
2,3-dichlorophenol
Conditions | Yield |
---|---|
With tetraethylammonium bromide In methanol Electrolysis; Further byproducts given. Title compound not separated from byproducts; |
2,3-dichlorophenol
Conditions | Yield |
---|---|
With hydrogenchloride; air; sewage sludge ash at 400℃; Formation of xenobiotics; |
Conditions | Yield |
---|---|
With potassium chloride; water at 25℃; pH=12.7; Kinetics; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tetraethylmmonium bromide / methanol / Electrolysis 2: tetraethylmmonium bromide / methanol / Electrolysis View Scheme |
N-benzyl-N-ethylaniline
2,3-dichlorophenyl picolinate
A
2,3-dichlorophenol
B
N-ethyl-N-phenylpicolinamide
D
benzaldehyde
Conditions | Yield |
---|---|
In chlorobenzene at 115℃; for 24h; Green chemistry; |
2,3-dichlorophenol
chloromethyl methyl ether
2,3-dichlorophenyl methoxymethyl ether
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 50 - 60℃; for 0.666667h; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In 1,4-dioxane at 60℃; for 48h; Green chemistry; | 100% |
Conditions | Yield |
---|---|
Stage #1: 2,3-dichlorophenol With potassium carbonate In acetone for 0.5h; Stage #2: dimethyl sulfate In acetone at 60℃; for 3h; | 99.1% |
Stage #1: 2,3-dichlorophenol With potassium hydroxide In toluene for 0.5h; Stage #2: dimethyl sulfate In toluene at 100℃; for 5h; Stage #3: With potassium hydroxide In toluene for 1h; Reflux; | 96.6% |
With alkali |
Conditions | Yield |
---|---|
With 9,10-dihydroanthracene; water at 356.85℃; for 3h; Kinetics; | A 99% B 0.3% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 25℃; for 18h; | 99% |
Conditions | Yield |
---|---|
With potassium methanolate In N,N-dimethyl-formamide at 155℃; for 0.5h; Temperature; Reagent/catalyst; Microwave irradiation; | 98.5% |
2,3-dichlorophenol
ethyl bromoacetate
(dichloro-2,3 phenoxy)acetate d'ethyle
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 50℃; for 3h; | 98% |
With sodium ethanolate In ethanol for 2.5h; Heating; | 86% |
Stage #1: 2,3-dichlorophenol With water; potassium carbonate for 0.2h; Metallation; Irradiation; Stage #2: ethyl bromoacetate In benzene at 50℃; for 0.25h; Substitution; Irradiation; | 82% |
Conditions | Yield |
---|---|
With potassium carbonate In butanone for 24h; Heating; | 98% |
2,3-dichlorophenol
chloroformic acid ethyl ester
Carbonic acid 2,3-dichloro-phenyl ester ethyl ester
Conditions | Yield |
---|---|
With sodium hydroxide In water for 1.5h; Ambient temperature; | 98% |
2,3-dichlorophenol
(2s)-(+)-glycidyl 3-nitrobenzenesulfonate
(2S)-2-([(2,3-dichlorophenyl)oxy]methyl)oxirane
Conditions | Yield |
---|---|
Stage #1: 2,3-dichlorophenol With potassium carbonate In acetone for 0.5h; Reflux; Stage #2: (2s)-(+)-glycidyl 3-nitrobenzenesulfonate Cooling; Reflux; | 96% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 7h; Heating; | 95% |
2,3-dichlorophenol
4-Fluoronitrobenzene
1,2-dichloro-3-(4-nitrophenoxy)benzene
Conditions | Yield |
---|---|
With potassium carbonate In water; N,N-dimethyl-formamide at 110℃; for 5h; | 95% |
Conditions | Yield |
---|---|
With sodium hydroxide In neat (no solvent) at 90℃; for 6h; Green chemistry; | 95% |
Conditions | Yield |
---|---|
With N,N-dimethyl acetamide; triethylamine at 100℃; under 15001.5 Torr; for 4h; Autoclave; | 94% |
Conditions | Yield |
---|---|
With caesium carbonate In dimethyl sulfoxide at 95℃; for 12h; | 93% |
Stage #1: 2,3-dichlorophenol With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.5h; Stage #2: Bromoacetaldehyde diethyl acetal In N,N-dimethyl-formamide for 72h; Reflux; |
2,3-dichlorophenol
(R)-glycidyl nosylate
(2R)-2-([(2,3-dichlorophenyl)oxy]methyl)oxirane
Conditions | Yield |
---|---|
Stage #1: 2,3-dichlorophenol With potassium carbonate In acetone for 0.5h; Reflux; Stage #2: (R)-glycidyl nosylate Cooling; Reflux; | 92% |
2,3-dichlorophenol
chloroacetic acid ethyl ester
2,3-dichlorophenoxyacetic acid
Conditions | Yield |
---|---|
Stage #1: 2,3-dichlorophenol; chloroacetic acid ethyl ester With potassium carbonate; potassium iodide In water; N,N-dimethyl-formamide at 100℃; for 0.0666667h; Microwave irradiation; Stage #2: With sodium hydroxide for 0.0833333h; Microwave irradiation; | 91% |
2-Thiophenecarbonyl chloride
2,3-dichlorophenol
Thiophen-2-carbonsaeure-(2,3-dichlor)-phenylester
Conditions | Yield |
---|---|
With pyridine In tetrahydrofuran for 1h; Heating; | 90% |
2-[2-(vinyloxy)ethoxymethyl]oxirane
2,3-dichlorophenol
2-{2-[1-(2,3-Dichloro-phenoxy)-ethoxy]-ethoxymethyl}-oxirane
Conditions | Yield |
---|---|
With heptafluorobutyric Acid at 50 - 80℃; | 90% |
Conditions | Yield |
---|---|
With sodium In methanol for 7h; Heating; | 90% |
2,3-dichlorophenol
chloromethyl sodium sulfonate
Conditions | Yield |
---|---|
With sodium hydroxide; water for 0.00833333h; Condensation; Irradiation; | 90% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 70℃; for 3h; Inert atmosphere; | 90% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 5h; Inert atmosphere; |
Conditions | Yield |
---|---|
With borane-ammonia complex In water; isopropyl alcohol at 50℃; for 5h; Sealed tube; | 90% |
In cyclohexane for 24h; UV-irradiation; | 9 %Chromat. |
2,3-dichlorophenol
Chloroacetamide
8-chloro-3,4-dihydro-2H-1,4-benzoxazin-3-one
Conditions | Yield |
---|---|
With caesium carbonate at 130℃; Microwave irradiation; | 89% |
2,3-dichlorophenol
2-chloro-N-(2-(3,4-dimethoxyphenyl)ethyl)acetamide
2-(2,3-dichloro-phenoxy)-N-[2-(3,4-dimethoxy-phenyl)-ethyl]-acetamide
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 6h; Heating; | 88% |
2,3-dichlorophenol
N,N-diethylcarbamyl chloride
2,3-dichlorophenyl N,N-diethyl O-carbamate
Conditions | Yield |
---|---|
Stage #1: 2,3-dichlorophenol With potassium carbonate In acetonitrile for 0.5h; Stage #2: N,N-diethylcarbamyl chloride In acetonitrile for 5h; Reflux; | 87% |
2-bromo-2-methylpropanamide
2,3-dichlorophenol
2-(2,3-dichlorophenoxy)-2-methylpropanamide
Conditions | Yield |
---|---|
Stage #1: 2,3-dichlorophenol With sodium hydroxide In N,N-dimethyl-formamide at 20℃; for 1h; Inert atmosphere; Stage #2: 2-bromo-2-methylpropanamide In N,N-dimethyl-formamide at 20℃; for 2h; Inert atmosphere; | 87% |
3-chloro-4-fluoronitrobenzene
2,3-dichlorophenol
3.chloro-4-(2,3-dichlorophenoxy)phenylamine
Conditions | Yield |
---|---|
Stage #1: 3-chloro-4-fluoronitrobenzene; 2,3-dichlorophenol With potassium hydrogencarbonate In N,N-dimethyl-formamide at 100℃; for 1.5h; Stage #2: With hydrogenchloride; iron In ethanol; water at 110℃; for 3h; Stage #3: With sodium hydrogencarbonate In water | 86% |
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