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Cas:87-86-5
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
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Cas:87-86-5
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With chlorine; aluminum (III) chloride at 100 - 180℃; for 10.8333h; Product distribution / selectivity; | A 83% B 10% |
With chlorine; nickel; aluminum (III) chloride at 90 - 180℃; for 10h; Product distribution / selectivity; | A 79% B 20% |
Conditions | Yield |
---|---|
With chlorine; nickel; aluminum (III) chloride at 90 - 180℃; for 4.16667 - 4.66667h; Product distribution / selectivity; | A 80% B 10% |
Stage #1: 2,4,6-Trichlorophenol With chlorine; aluminum (III) chloride at 105 - 183℃; Stage #2: With phenol at 180 - 190℃; Product distribution / selectivity; | A 80% B 10% |
With chlorine; aluminum (III) chloride at 105 - 190℃; for 3.66667 - 4.83333h; Product distribution / selectivity; | A 77% B 10% |
pentachlorophenol-TMS
Pentachlorophenol
Conditions | Yield |
---|---|
With nano magnetic sulfated zirconia (Fe3O4 at ZrO2/SO42-) In neat (no solvent) at 20℃; for 0.833333h; Green chemistry; | 80% |
2,3,4,5,6-pentachloro-4-(pentachlorophenoxy)-2,5-cyclohexadienone
A
Pentachlorophenol
B
2,3,5,6-tetrachloro-4-(2,3,4,5,6-pentachlorophenoxy)phenol
C
3,4,5,6-tetrachloro-2-(2,3,4,5,6-pentachlorophenoxy)phenol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol; benzene for 1h; Ambient temperature; | A 4 % Chromat. B 52.6% C 26 % Chromat. |
Conditions | Yield |
---|---|
With sodium hydroxide In water for 3h; Heating; | 50% |
tetrachloromethane
3-Iodophenol
A
Pentachlorophenol
B
2,4,6-trichloro-3-iodo-phenol
Conditions | Yield |
---|---|
at 60 - 70℃; Einleiten von Chlor; |
Conditions | Yield |
---|---|
With chlorosulfonic acid at 150 - 160℃; |
Conditions | Yield |
---|---|
With tetrachloromethane; chlorine at 50℃; |
Conditions | Yield |
---|---|
With chlorine |
hexachlorobenzene
sodium methylate
A
Pentachlorophenol
B
Pentachloroanisole
Conditions | Yield |
---|---|
at 180℃; im Rohr; | |
at 180℃; im Rohr; |
Conditions | Yield |
---|---|
With sodium hydroxide; glycerol at 250 - 280℃; | |
With sodium hydroxide at 250℃; | |
With sodium hydroxide; tert-butyl alcohol at 135℃; | |
With sodium hydroxide; ethylene glycol at 200℃; | |
With sodium hydroxide at 135℃; |
Conditions | Yield |
---|---|
With sodium methylate at 180℃; im Rohr; |
Conditions | Yield |
---|---|
With tetrachloromethane at 60 - 70℃; Einleiten von Chlor; |
Conditions | Yield |
---|---|
With aluminium trichloride; chlorine; iron at 120 - 195℃; |
Conditions | Yield |
---|---|
With hydrogenchloride; acetic acid; tin(ll) chloride | |
With carbon disulfide; aluminium trichloride; acetyl chloride Verseifung des Reaktionsprodukts; | |
With potassium iodide |
2,3,4,4,5,6-hexachlorocyclohexa-2,5-dien-1-one
A
Pentachlorophenol
B
chloranil
Conditions | Yield |
---|---|
With hydrogenchloride | |
With aluminium trichloride at 160℃; im Druckrohr; |
Conditions | Yield |
---|---|
durch Reduktion; |
Conditions | Yield |
---|---|
With acetone | |
With potassium acetate; acetic acid | |
With sodium acetate; acetic acid |
Conditions | Yield |
---|---|
With sulfuric acid; sodium nitrite at 180℃; |
2,4,6-trichloro-3-iodo-phenol
A
Pentachlorophenol
Conditions | Yield |
---|---|
With tetrachloromethane at 60 - 70℃; Einleiten von Chlor; |
4,5,6-trihydroxy-benzene-1,3-disulfonic acid
Pentachlorophenol
Conditions | Yield |
---|---|
With thionyl chloride at 100℃; im Rohr; |
2,3,4,4,5,6,6-heptachloro-cyclohex-2-enone
potassium acetate
acetic acid
Pentachlorophenol
Conditions | Yield |
---|---|
With chlorosulfonic acid at 150 - 160℃; |
Conditions | Yield |
---|---|
With antimony(III) chloride; chlorine at 200 - 220℃; | |
With aluminium trichloride; chlorine; 1,2-dichloro-ethane at 70 - 85℃; | |
With aluminium trichloride; chlorine; 1,1,2,2-tetrachloroethane at 70 - 85℃; | |
With tetrachloromethane; chlorine; iron(III) chloride at 20 - 25℃; | |
With aluminium trichloride; chlorine at 100 - 190℃; |
Conditions | Yield |
---|---|
With chlorosulfonic acid at 150℃; |
Conditions | Yield |
---|---|
With hydrogenchloride; acetic acid Electrolysis; |
Pentachlorophenol
Succinic acid mono-[(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(4-hydroxy-2-oxo-2H-pyrimidin-1-yl)-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-3-yl] ester
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In N,N-dimethyl-formamide for 16h; Ambient temperature; | 100% |
2-methoxy-succinic acid 1-(6-tert-butoxycarbonylamino-hexyl) ester
Pentachlorophenol
pentachlorophenyl N-tert-butoxycarbonyl-3-methoxy-4-oxo-5-oxy-11-aminoundecanoate
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In ethyl acetate at 20℃; for 120h; | 100% |
(E)-[2-(phenylazo)phenyl]diphenylphosphine
Pentachlorophenol
C6Cl5O(1-)*C24H20N2P(1+)
Conditions | Yield |
---|---|
In tetrahydrofuran at -60℃; | 100% |
Conditions | Yield |
---|---|
Stage #1: Pentachlorophenol With potassium carbonate In butanone at 20℃; for 0.25h; Stage #2: α-bromoacetophenone In butanone at 80℃; | 100% |
Conditions | Yield |
---|---|
With silver trifluoromethanesulfonate at 60℃; for 0.0833333h; neat (no solvent); | 99% |
With dicyclohexyl-carbodiimide In acetonitrile at 25℃; for 1h; | 91% |
With sodium acetate |
Pentachlorophenol
pentachlorobenzenesulfonic anhydride
A
pentachlorobenzene
B
pentachlorobenzenesulfonic acid
Conditions | Yield |
---|---|
at 200 - 210℃; for 0.5h; | A 32% B 99% C 39% |
Pentachlorophenol
Succinic acid mono-[3-[bis-(4-methoxy-phenyl)-phenyl-methoxy]-2-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-ylmethoxy)-propyl] ester
1-<<2-dimethoxytrityl-hydroxy-1-(pentachlorophenylsuccinyl-hydroxy-methyl)ethoxy>-methyl>thymine
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide | 99% |
Pentachlorophenol
Diphenyliodonium triflate
2,3,4,5,6-Pentachlorobiphenyl ether
Conditions | Yield |
---|---|
Stage #1: Pentachlorophenol With potassium tert-butylate In tetrahydrofuran at 0℃; for 0.25h; Stage #2: Diphenyliodonium triflate In tetrahydrofuran at 40℃; for 2h; | 99% |
Stage #1: Pentachlorophenol With potassium tert-butylate In tetrahydrofuran at 0℃; for 0.25h; Stage #2: Diphenyliodonium triflate In tetrahydrofuran at 40℃; for 2h; | 99% |
Pentachlorophenol
tri-p-fluorophenylstibine
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In diethyl ether; water at 20℃; for 24h; | 99% |
Pentachlorophenol
1,2,2,2-tetrachloroethyl chloroformate
pentachlorophenyl 1,2,2,2-tetrachloroethyl carbonate
Conditions | Yield |
---|---|
With pyridine In dichloromethane for 3h; Ambient temperature; | 98% |
Pentachlorophenol
Succinic acid mono-[(2R,3R,4R,5R)-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(6-hydroxy-2-isobutyrylamino-purin-9-yl)-4-(tetrahydro-furan-2-yloxy)-tetrahydro-furan-3-yl] ester
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In N,N-dimethyl-formamide for 16h; Ambient temperature; | 98% |
Conditions | Yield |
---|---|
With nickel dichloride; RedAl In tetrahydrofuran at 68℃; for 2h; Product distribution; other dehalogenating systems, other reaction times and temperatures; | A n/a B 98% |
Pentachlorophenol
Ru(CH2C(CH3)CH2)2(((CH3)2CH)2PCH2P(C6H5)2)
Ru(OC6Cl5)2(((CH3)2CH)2PCH2P(C6H5)2)
Conditions | Yield |
---|---|
In toluene (Ar); stirring a soln. of ruthenium complex and pentachlorophenol in toluene for 30 min at room temp.; evapn., washing with EtOH and pentane, drying; elem. anal.; | 98% |
Conditions | Yield |
---|---|
In diethyl ether at 20℃; for 24h; | 98% |
morpholine-4-carboxylic acid amide
Pentachlorophenol
2,3,4,5,6-Pentachloro-phenol; compound with morpholine-4-carboxylic acid amide
Conditions | Yield |
---|---|
96% |
Pentachlorophenol
N,N-Dimethylthiocarbamoyl chloride
O-pentachlorophenyl dimethylthiocarbamate
Conditions | Yield |
---|---|
With potassium hydroxide In 1,4-dioxane 1.) 30 deg C, 1 h; 2.) 85 deg C, 3 h; | 96% |
Pentachlorophenol
Pentaerythritol
3,9-bis(2',3',4',5',6'-pentachlorophenoxy)-2,4,8,10-tetraoxa-3,9-diphosphaspiro(5.5)undecane-3,9-dioxide
Conditions | Yield |
---|---|
With potassium chloride; trichlorophosphate In toluene | 95.3% |
Conditions | Yield |
---|---|
With bis-[(trifluoroacetoxy)iodo]benzene In various solvent(s) at 20℃; for 1h; pH=1.4; Oxidation; | 95% |
With nitric acid | |
With hydrogenchloride; chlorine |
Pentachlorophenol
Ru(CH2C(CH3)CH2)2((C6H11)2PCH2P(C6H5)2)
Ru(OC6Cl5)2((C6H11)2PCH2P(C6H5)2)
Conditions | Yield |
---|---|
In toluene (Ar); stirring a soln. of ruthenium complex and pentachlorophenol in toluene for 30 min at room temp.; evapn., washing with EtOH and pentane, drying; elem. anal.; | 95% |
Pentachlorophenol
triphenylantimony
di(pentachlorophenolato)triphenylantimony(V)
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In diethyl ether at 20℃; for 24h; | 95% |
Conditions | Yield |
---|---|
In toluene at 24℃; for 0.25h; | 95% |
Pentachlorophenol
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In diethyl ether; water at 20℃; for 24h; | 95% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide In diethyl ether at 20℃; for 24h; | 94% |
Conditions | Yield |
---|---|
With 3-(5-nitro-2-oxo-1,2-dihydro-1-pyridyl)-1,2-benzisothiazole 1,1,-dioxide; triethylamine In dichloromethane -10 deg C -> r.t., overnight; | 93% |
With TEA; 3-(5-nitro-2-oxo-1,2-dihydro-1-pyridyl)-1,2-benzisothiazole 1,1,-dioxide In dichloromethane -10 deg C to room temperature; | 93% |
With acetic anhydride |
Pentachlorophenol
Succinic acid (3aR,4R,6R,6aR)-6-(2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-2-methoxy-tetrahydro-furo[3,4-d][1,3]dioxol-4-ylmethyl ester pentachlorophenyl ester
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In N,N-dimethyl-formamide | 93% |
Pentachlorophenol
penta(p-tolyl)antimony(V)
Conditions | Yield |
---|---|
In toluene at 24℃; for 0.25h; | 93% |
Pentachlorophenol
Conditions | Yield |
---|---|
In hexane at -30 - 20℃; for 14.5h; Sealed tube; | 93% |
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In acetonitrile at 25℃; for 1h; | 92% |
Pentachlorophenol
phosphorus pentachloride
phenylmalonic acid
dipentachlorophenyl phenylmalonate
Conditions | Yield |
---|---|
With pyridine In methanol; dichloromethane | 92% |
Pentachlorophenol
[Ru(η3-2-MeC3H4)2(κ2-Ph2PCH2CH2PiPr2)]
Conditions | Yield |
---|---|
In toluene (Ar); -30°C; warmed to room temp.; stirred (10 min); solvent evapd. (vac.); washed (pentane); dried; elem. anal.; | 92% |
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