Dayang Chem (Hangzhou) Co.,Ltd.
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:548-43-6
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryLIDE PHARMACEUTICALS LIMITED
Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
Cas:548-43-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Tianfu Chemical Co., Ltd.
High quality and best price of elymoclavine Ergoline-8-methanol,8,9-didehydro-6-methyl- FROM HENAN TIANFU CHEMICAL: Henan Tianfu Chemical Co.,LTD was built in 2009 with an ISO certificate in the past 5 years, we have grown up as a famous fine c
Hebei Nengqian Chemical Import and Export Co., LTD
With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Shanghai Upbio Tech Co.,Ltd
1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:548-43-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryQingdao Beluga Import and Export Co., LTD
elymoclavine CAS:548-43-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates,
Cas:548-43-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryShandong Hanjiang Chemical Co., Ltd.
Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:548-43-6
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co., Ltd.
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:548-43-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:548-43-6
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryHangzhou J&H Chemical Co., Ltd.
J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals
Wuhan Circle Star Chem-medical Technology co.,Ltd.
1,we produce and sell good chemicals around the world.2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%.3,our staff consists of highly qualified in
Antimex Chemical Limied
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:548-43-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryHangzhou Fandachem Co.,Ltd
Ergoline-8-methanol,8,9-didehydro-6-methyl- cas 548-43-6Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Cas:548-43-6
Min.Order:0
Negotiable
Type:Other
inquiryHenan Kanbei Chemical Co.,LTD
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Shanghai Chinqesen Biotechnology Co., Ltd.
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
ZHEJIANG JIUZHOU CHEM CO.,LTD
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Changzhou Extraordinary Pharmatech co.,LTD
Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa
HuBei Ipure Biotech CO.,ltd
HuBei ipure is a diversified product production and operation enterprise, with API, pharma intermediates, and other fine chemicals as well as R&D and pigments development and sales as one of the large enterprises, with more than 130 acres of pl
Cas:548-43-6
Min.Order:1 Gram
FOB Price: $1.0 / 2.0
Type:Trading Company
inquiryHenan Fine Chemicals Co., Ltd
Best quality & Attractive price & Professional service; Trial & Pilot & CommercialHenan Fine Chemicals Co., LTD. is a diversified technology - oriented integrated company, which mainly concentrates on fine chemicals. Our company is committed to becom
Cas:548-43-6
Min.Order:0
Negotiable
Type:Trading Company
inquiryShanghai united Scientific Co.,Ltd.
United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
Cas:548-43-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryShanghai Run-Biotech Co., Ltd.
1.We have rich experience in the development and production 2.Our factory is in Shanghai of China,We have convenient traffic conditions.3.We have advanced testing equipment and shipping line. Package:5g, 10g, 50g, 100g, 2kg Application:Pharmaceutical
Cas:548-43-6
Min.Order:0
Negotiable
Type:Trading Company
inquiryHebei Ruishun Trade Co.,Ltd
Supply top quality products with a reasonable price Application:api
Chemical Co.Ltd
Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en
Cas:548-43-6
Min.Order:0
Negotiable
Type:Trading Company
inquiryAnnecis Limited
Cas:548-43-6
Min.Order:0
Negotiable
Type:Trading Company
inquiryAngene International Limited
Cas:548-43-6
Min.Order:0
Negotiable
Type:Trading Company
inquirySynthetic route
-
-
1027016-28-9
(6aR,10aR)-9-(tert-Butyl-dimethyl-silanyloxymethyl)-7-methyl-4,6,6a,7,8,10a-hexahydro-indolo[4,3-fg]quinoline
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| With pyridinium p-toluenesulfonate In ethanol at 20℃; for 48h; | 95% |
| Conditions | Yield |
|---|---|
| for 168h; fermentative bioconversion by Ca-alginate immibilized cells of submerged cultures of C. fusiformis W1; | 90% |
-
-
63-68-3
L-methionine
-
-
150-97-0, 690-72-2, 17817-88-8, 32451-23-3
D,L-mevalonic acid
-
-
54-12-6
Trp
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| With phosphate buffer pH 7.3 In water for 48h; Claviceps sp., strain SD58, medium NL 406; |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 13 steps 1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver hexafluoroantimonate; copper diacetate / 4 h / 110 °C / Inert atmosphere 2: dmap / acetonitrile / 0.5 h / 40 °C 3: ammonium acetate / 2 h / 70 °C 4: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1 h / -78 °C 5: sodium tetrahydroborate / tetrahydrofuran; methanol / 1 h / 20 °C 6: triethylamine / dichloromethane / 1 h / 0 - 20 °C 7: potassium carbonate; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); palladium diacetate / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere 8: hydrogenchloride; zinc / methanol; water / 1 h 9: potassium carbonate / dichloromethane / 20 h / 20 °C 10: triethylamine / dichloromethane / 24 h / 20 °C 11: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / toluene / 12 h / 80 °C / Inert atmosphere 12: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Reflux 13: pyridinium p-toluenesulfonate / ethanol / 48 h / 20 °C View Scheme |
-
-
115698-38-9
(E)-methyl 3-(3-formyl-1H-indol-4-yl)acrylate
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| Multi-step reaction with 12 steps 1: dmap / acetonitrile / 0.5 h / 40 °C 2: ammonium acetate / 2 h / 70 °C 3: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1 h / -78 °C 4: sodium tetrahydroborate / tetrahydrofuran; methanol / 1 h / 20 °C 5: triethylamine / dichloromethane / 1 h / 0 - 20 °C 6: potassium carbonate; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); palladium diacetate / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere 7: hydrogenchloride; zinc / methanol; water / 1 h 8: potassium carbonate / dichloromethane / 20 h / 20 °C 9: triethylamine / dichloromethane / 24 h / 20 °C 10: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / toluene / 12 h / 80 °C / Inert atmosphere 11: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Reflux 12: pyridinium p-toluenesulfonate / ethanol / 48 h / 20 °C View Scheme |
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| Multi-step reaction with 11 steps 1: ammonium acetate / 2 h / 70 °C 2: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1 h / -78 °C 3: sodium tetrahydroborate / tetrahydrofuran; methanol / 1 h / 20 °C 4: triethylamine / dichloromethane / 1 h / 0 - 20 °C 5: potassium carbonate; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); palladium diacetate / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere 6: hydrogenchloride; zinc / methanol; water / 1 h 7: potassium carbonate / dichloromethane / 20 h / 20 °C 8: triethylamine / dichloromethane / 24 h / 20 °C 9: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / toluene / 12 h / 80 °C / Inert atmosphere 10: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Reflux 11: pyridinium p-toluenesulfonate / ethanol / 48 h / 20 °C View Scheme |
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| Multi-step reaction with 10 steps 1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1 h / -78 °C 2: sodium tetrahydroborate / tetrahydrofuran; methanol / 1 h / 20 °C 3: triethylamine / dichloromethane / 1 h / 0 - 20 °C 4: potassium carbonate; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); palladium diacetate / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere 5: hydrogenchloride; zinc / methanol; water / 1 h 6: potassium carbonate / dichloromethane / 20 h / 20 °C 7: triethylamine / dichloromethane / 24 h / 20 °C 8: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / toluene / 12 h / 80 °C / Inert atmosphere 9: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Reflux 10: pyridinium p-toluenesulfonate / ethanol / 48 h / 20 °C View Scheme |
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| Multi-step reaction with 8 steps 1: triethylamine / dichloromethane / 1 h / 0 - 20 °C 2: potassium carbonate; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); palladium diacetate / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere 3: hydrogenchloride; zinc / methanol; water / 1 h 4: potassium carbonate / dichloromethane / 20 h / 20 °C 5: triethylamine / dichloromethane / 24 h / 20 °C 6: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / toluene / 12 h / 80 °C / Inert atmosphere 7: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Reflux 8: pyridinium p-toluenesulfonate / ethanol / 48 h / 20 °C View Scheme |
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| Multi-step reaction with 7 steps 1: potassium carbonate; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); palladium diacetate / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere 2: hydrogenchloride; zinc / methanol; water / 1 h 3: potassium carbonate / dichloromethane / 20 h / 20 °C 4: triethylamine / dichloromethane / 24 h / 20 °C 5: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / toluene / 12 h / 80 °C / Inert atmosphere 6: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Reflux 7: pyridinium p-toluenesulfonate / ethanol / 48 h / 20 °C View Scheme |
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| Multi-step reaction with 6 steps 1: hydrogenchloride; zinc / methanol; water / 1 h 2: potassium carbonate / dichloromethane / 20 h / 20 °C 3: triethylamine / dichloromethane / 24 h / 20 °C 4: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / toluene / 12 h / 80 °C / Inert atmosphere 5: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Reflux 6: pyridinium p-toluenesulfonate / ethanol / 48 h / 20 °C View Scheme |
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / toluene / 12 h / 80 °C / Inert atmosphere 2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Reflux 3: pyridinium p-toluenesulfonate / ethanol / 48 h / 20 °C View Scheme |
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| Multi-step reaction with 9 steps 1: sodium tetrahydroborate / tetrahydrofuran; methanol / 1 h / 20 °C 2: triethylamine / dichloromethane / 1 h / 0 - 20 °C 3: potassium carbonate; (S)-(1,1'-binaphthalene)-2,2'-diylbis(diphenylphosphine); palladium diacetate / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere 4: hydrogenchloride; zinc / methanol; water / 1 h 5: potassium carbonate / dichloromethane / 20 h / 20 °C 6: triethylamine / dichloromethane / 24 h / 20 °C 7: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / toluene / 12 h / 80 °C / Inert atmosphere 8: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Reflux 9: pyridinium p-toluenesulfonate / ethanol / 48 h / 20 °C View Scheme |
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| Multi-step reaction with 5 steps 1: potassium carbonate / dichloromethane / 20 h / 20 °C 2: triethylamine / dichloromethane / 24 h / 20 °C 3: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / toluene / 12 h / 80 °C / Inert atmosphere 4: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Reflux 5: pyridinium p-toluenesulfonate / ethanol / 48 h / 20 °C View Scheme |
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| Multi-step reaction with 4 steps 1: triethylamine / dichloromethane / 24 h / 20 °C 2: 1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene[2-(iso-propoxy)-5-(N,N-dimethylaminosulfonyl)phenyl]methylene ruthenium(II) dichloride / toluene / 12 h / 80 °C / Inert atmosphere 3: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Reflux 4: pyridinium p-toluenesulfonate / ethanol / 48 h / 20 °C View Scheme |
-
-
548-43-6
elymoclavine
-
-
108-24-7
acetic anhydride
-
-
5080-45-5
8-acetoxymethyl-6-methyl-8,9-didehydro-ergoline
| Conditions | Yield |
|---|---|
| In pyridine Ambient temperature; | 90% |
| In pyridine Ambient temperature; Yield given; |
-
-
548-43-6
elymoclavine
-
-
18051-16-6
9,10-dihydrolysergol
| Conditions | Yield |
|---|---|
| With methanol; nickel In 1,4-dioxane Heating; | 86% |
-
-
548-43-6
elymoclavine
-
-
618-46-2
m-Chlorobenzoyl chloride
-
-
85893-06-7
O-3-Chlorobenzoyl-elymoclavin-hydrochlorid
| Conditions | Yield |
|---|---|
| With pyridine Ambient temperature; | 77% |
-
-
548-43-6
elymoclavine
-
-
122-01-0
4-chloro-benzoyl chloride
-
-
85893-07-8
O-4-Chlorobenzoyl-elymoclavin-hydrochlorid
| Conditions | Yield |
|---|---|
| With pyridine Ambient temperature; | 69% |
-
-
548-43-6
elymoclavine
-
-
100-07-2
4-methoxy-benzoyl chloride
-
-
85893-09-0
O-4-Methoxybenzoyl-elymoclavin-hydrochlorid
| Conditions | Yield |
|---|---|
| With pyridine at 70℃; | 63% |
-
-
548-43-6
elymoclavine
-
-
4521-61-3
3,4,5-Trimethoxybenzoyl chloride
-
-
85893-10-3
O-3,4,5-Trimethoxybenzoyl-elymoclavin-hydrochlorid
| Conditions | Yield |
|---|---|
| With pyridine at 100℃; | 62% |
-
-
548-43-6
elymoclavine
-
-
874-60-2
4-methyl-benzoyl chloride
-
-
85893-08-9
O-4-Methylbenzoyl-elymoclavin-hydrochlorid
| Conditions | Yield |
|---|---|
| With pyridine at 70℃; | 62% |
-
-
548-43-6
elymoclavine
-
-
73621-60-0
N-((4aR,10bR)-2-Hydroxymethyl-4-methyl-6-oxo-3,4,4a,5,6,10b-hexahydro-benzo[f]quinolin-7-yl)-formamide
| Conditions | Yield |
|---|---|
| With sodium periodate; methanesulfonic acid In methanol at 25℃; for 2.75h; | 50% |
-
-
548-43-6
elymoclavine
-
-
604-69-3
β-D-glucose pentaacetate
-
-
180144-99-4
Acetic acid (2R,3R,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-((6aR,10aR)-7-methyl-4,6,6a,7,8,10a-hexahydro-indolo[4,3-fg]quinolin-9-ylmethoxy)-tetrahydro-pyran-3-yl ester
| Conditions | Yield |
|---|---|
| With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve In nitromethane; dichloromethane for 3h; Ambient temperature; | 46% |
-
-
548-43-6
elymoclavine
-
-
3150-24-1
4-nitrophenyl-β-D-galactopyranoside
-
A
-
145603-56-1
elymoclavine-β-D-galactoside
-
B
-
145603-59-4
GAL-β(1-6)-GAL-β-O-elymoclavine
| Conditions | Yield |
|---|---|
| In various solvent(s) at 24℃; for 3h; β-galactosidase from Aspergillus orizae or from Escherichia coli; other ergot alkaloids; | A 37% B n/a |
| With 2-hydroxyethanethiol; citric acid; magnesium chloride at 24℃; for 3h; β-galactosidase from Aspergillus oryzae, K-Pi-buffer; | A 37% B n/a |
| With 2-hydroxyethanethiol; citric acid; magnesium chloride at 24℃; β-galactosidase from Aspergillus oryzae, K-Pi buffer; | A n/a B 1% |
| Conditions | Yield |
|---|---|
| With succinic acid; DL-5-fluorotryptophan In water at 24℃; for 1296h; Claviceps purpurea 88-EP-47; | 24% |
| Conditions | Yield |
|---|---|
| With α-galactosidase form A. oryzae; citric acid at 30℃; pH 5; | A 3% B 23% |
| Conditions | Yield |
|---|---|
| With potassium amide; ferric nitrate In diethyl ether; ammonia at -50 - -40℃; for 0.5h; | 14% |
-
-
548-43-6
elymoclavine
-
-
10357-27-4
4-nitrophenyl-α-D-mannopyranoside
| Conditions | Yield |
|---|---|
| With α-mannosidase (almond); citric acid at 30℃; pH 5; | 3% |
| Conditions | Yield |
|---|---|
| With sodium; butan-1-ol |
| Conditions | Yield |
|---|---|
| With sodium; butan-1-ol |
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| With sodium; butan-1-ol | |
| Multi-step reaction with 2 steps 1: sodium; butan-1-ol 2: sodium; butan-1-ol View Scheme |
-
-
548-43-6
elymoclavine
-
-
18162-48-6
tert-butyldimethylsilyl chloride
-
-
1027016-28-9
(6aR,10aR)-9-(tert-Butyl-dimethyl-silanyloxymethyl)-7-methyl-4,6,6a,7,8,10a-hexahydro-indolo[4,3-fg]quinoline
| Conditions | Yield |
|---|---|
| With 1H-imidazole In N,N-dimethyl-formamide for 1h; Ambient temperature; |
-
-
548-43-6
elymoclavine
-
-
56862-50-1
8-chloromethyl-6-methyl-8,9-didehydro-ergoline
| Conditions | Yield |
|---|---|
| With trichlorophosphate for 1.5h; Heating; | |
| With oxalyl dichloride In N,N-dimethyl-formamide; acetonitrile at -70℃; |
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| With dihydrogen peroxide In isopropyl alcohol at 60℃; for 2h; Yield given. Yields of byproduct given; |
| Conditions | Yield |
|---|---|
| With pyridine; dmap for 12h; Ambient temperature; |
| Conditions | Yield |
|---|---|
| With potassium hydroxide; 18-crown-6 ether In dimethyl sulfoxide for 1h; |
| Conditions | Yield |
|---|---|
| With pyridine; dmap for 12h; Ambient temperature; |
| Conditions | Yield |
|---|---|
| With pyridine; dmap for 12h; Ambient temperature; |
-
-
548-43-6
elymoclavine
| Conditions | Yield |
|---|---|
| With pyridine; dmap for 12h; Ambient temperature; |
| Conditions | Yield |
|---|---|
| With pyridine; dmap for 12h; Ambient temperature; |
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