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Hunan Longxianng Runhui Trading Co.,Ltd

R & D enterprises have their own stock in stock Runhui Chem supplies the compounds with the most competitive price and the best quality; specializes in custom synthesis & building blocks. welcome the enquiries & orders around the wo

Lysergol

Cas:602-85-7

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

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Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as:

Lysergol

Cas:602-85-7

Min.Order:0 Metric Ton

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Type:Trading Company

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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

Lysergol Manufacturer/High quality/Best price/In stock

Cas:602-85-7

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Wuhan Fortuna Chemical Co.,Ltd

Manufacturer supply Lysergol CAS 602-85-7 with attractive price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, Food/Feed addit

Manufacturer supply Lysergol CAS 602-85-7 with attractive price

Cas:602-85-7

Min.Order:10 Gram

FOB Price: $10.0

Type:Trading Company

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Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality 99% Ergoline-8-methanol,9,10-didehydro-6-methyl-, (8β)- 602-85-7 ISO Producer

Cas:602-85-7

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Shanghai Seasonsgreen Chemical Co.,Ltd

Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu

lower price High quality LYSERGOL

Cas:602-85-7

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Manufacturers

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LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

Lysergol/ LIDE PHARMA- Factory supply / Best price

Cas:602-85-7

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

tianfu-chem_LYSERGOL 602-85-7

Cas:602-85-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

LYSERGOL

Cas:602-85-7

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

product Name 9,10-didehydro-6-methylergoline-8β-methanol Alias 10-didehydro-6-methyl-(8-beta)-ergoline-8-methano;9,10-didehydro-8-hydroxymethyl-6-methyl-ergolin;LYSERGOL;(5β)-9,10-Didehydro-6-methylergoline-8β

9,10-didehydro-6-methylergoline-8β-methanol

Cas:602-85-7

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Ergoline-8-methanol,9,10-didehydro-6-methyl-, (8β)- 602-85-7

Cas:602-85-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

LYSERGOL CAS:602-85-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates, ste

LYSERGOL CAS:602-85-7

Cas:602-85-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Ergoline-8-methanol,9,10-didehydro-6-methyl-, (8β)-

Cas:602-85-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

We can provide GMP validation service that complies with SFDA, FDA, WHO and EU EMPA.Excellent registration team could help us easlily to register our products in different countries.If you and your customer are interested in some products or need C

LYSERGOL manufacturer with low price

Cas:602-85-7

Min.Order:1 Gram

Negotiable

Type:Trading Company

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Shanxi Ankesi Biotechnology Co., Ltd

Our Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual

High Quality 99% Lysergol CAS 602-85-7 AKS

Cas:602-85-7

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Ergoline-8-methanol,9,10-didehydro-6-methyl-, (8β)-

Cas:602-85-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

LYSERGOL

Cas:602-85-7

Min.Order:1 Kilogram

FOB Price: $10.0 / 100.0

Type:Lab/Research institutions

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Triumph International Development Limilted

Appearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:By Sea/Air/Courier Port:Qingdao

LYSERGOL 602-85-7

Cas:602-85-7

Min.Order:1 Kilogram

FOB Price: $16.0 / 20.0

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

LYSERGOL

Cas:602-85-7

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Ergoline-8-methanol,9,10-didehydro-6-methyl-, (8β)-

Cas:602-85-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Shaanxi New nine Material Technology Co., Ltd.

Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purchase to assembly. 2 Professional R&D

Lysergol CAS NO.602-85-7

Cas:602-85-7

Min.Order:10 Gram

FOB Price: $5.0 / 10.0

Type:Trading Company

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Ergoline-8-methanol,9,10-didehydro-6-methyl

Cas:602-85-7

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:Off-white to beige crystalline powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Appli

Ergoline-8-methanol,9,10-didehydro-6-methyl-, (8β)-

Cas:602-85-7

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Wuhan Circle Star Chem-medical Technology co.,Ltd.

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualified

Factory Supply LYSERGOL Supplier Manufacturer With Competitive Price

Cas:602-85-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Buy LYSERGOL

Cas:602-85-7

Min.Order:0

Negotiable

Type:Trading Company

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Lysergol CAS NO.602-85-7

Cas:602-85-7

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

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Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

LYSERGOL

Cas:602-85-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

LYSERGOL

Cas:602-85-7

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Lysergol CAS NO.602-85-7

Cas:602-85-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Lysergol CAS NO.602-85-7

Cas:602-85-7

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Synthetic route

((6aR,9R)-7-methyl-4-tosyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-yl)methanol

((6aR,9R)-7-methyl-4-tosyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-yl)methanol

lysergol
602-85-7

lysergol

Conditions
ConditionsYield
With magnesium In methanol Inert atmosphere;93%
lysergic acid methyl ester
1159774-79-4

lysergic acid methyl ester

A

((6aR,9S)-7-methyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-yl)methanol
478-93-3

((6aR,9S)-7-methyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-yl)methanol

B

lysergol
602-85-7

lysergol

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 0.166667h;A 24%
B 49%
Lysergen
478-91-1

Lysergen

lysergol
602-85-7

lysergol

Conditions
ConditionsYield
With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide 1.) THF, 60 deg C, 24 h, 2.) THF, 40 deg C, 2 h; Yield given. Multistep reaction;
6-methyl-9,10-didehydro-ergoline-8β-carboxylic acid methyl ester

6-methyl-9,10-didehydro-ergoline-8β-carboxylic acid methyl ester

lysergol
602-85-7

lysergol

Conditions
ConditionsYield
With lithium aluminium tetrahydride; diethyl ether
elymoclavine

elymoclavine

lysergol
602-85-7

lysergol

Conditions
ConditionsYield
With sodium butanolate; butan-1-ol
elymoclavine

elymoclavine

A

lysergol
602-85-7

lysergol

B

isolysergol, lysergene

isolysergol, lysergene

Conditions
ConditionsYield
With potassium hydroxide at 140℃;
elymoclavine
548-43-6

elymoclavine

sodium butanolate
2372-45-4

sodium butanolate

butan-1-ol
71-36-3

butan-1-ol

A

((6aR,9S)-7-methyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-yl)methanol
478-93-3

((6aR,9S)-7-methyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-yl)methanol

B

lysergol
602-85-7

lysergol

C

lysergene

lysergene

elymoclavine
548-43-6

elymoclavine

methanol. KOH

methanol. KOH

A

((6aR,9S)-7-methyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-yl)methanol
478-93-3

((6aR,9S)-7-methyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-yl)methanol

B

lysergol
602-85-7

lysergol

C

lysergene

lysergene

Conditions
ConditionsYield
at 140℃;
(+)-setoclavine
519-12-0

(+)-setoclavine

lysergol
602-85-7

lysergol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 0.34 g / Woelm alumina / toluene / 2.5 h / Heating
2: 1.) 9-BBN, 2.) NaOH, 30percent aq. H2O2 / 1.) THF, 60 deg C, 24 h, 2.) THF, 40 deg C, 2 h
View Scheme
((6aR,9R)-4,7-ditosyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-yl)methanol

((6aR,9R)-4,7-ditosyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-yl)methanol

lysergol
602-85-7

lysergol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium naphthalenide / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere
2: sodium cyanoborohydride; acetic acid / methanol / 1 h / 25 °C / Inert atmosphere
View Scheme
formaldehyd
50-00-0

formaldehyd

lysergol
80233-17-6

lysergol

lysergol
602-85-7

lysergol

Conditions
ConditionsYield
With sodium cyanoborohydride; acetic acid In methanol at 25℃; for 1h; Inert atmosphere;5.2 mg
C25H26N2O4S

C25H26N2O4S

lysergol
602-85-7

lysergol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere
2: magnesium / methanol / Inert atmosphere
View Scheme
lysergol
602-85-7

lysergol

9,10-dihydrolysergol
18051-16-6

9,10-dihydrolysergol

Conditions
ConditionsYield
With hydrogen; 5%-palladium/activated carbon In N,N-dimethyl-formamide at 50 - 60℃; under 2068.65 - 2585.81 Torr;97%
With methanol; nickel In 1,4-dioxane Heating;90%
With methanol; Ra-Ni In 1,4-dioxane for 0.25h; Product distribution; Heating; different ratio of the solvents and times;
With hydrogen; palladium on activated charcoal In pyridine; N,N-dimethyl-formamide under 3750.3 Torr;
tert-butyldimethylsilyl chloride
18162-48-6

tert-butyldimethylsilyl chloride

lysergol
602-85-7

lysergol

8β-(tert-butyldimethylsiloxymethyl)-9,10-didehydro-6-methyl-ergoline
1075250-72-4

8β-(tert-butyldimethylsiloxymethyl)-9,10-didehydro-6-methyl-ergoline

Conditions
ConditionsYield
With triethylamine In water; N,N-dimethyl-formamide at 20℃; for 4 - 5h;96.5%
acetic anhydride
108-24-7

acetic anhydride

lysergol
602-85-7

lysergol

(5R)-6-methyl-(8R)-acetoxymethyl-Δ9,10-ergolene
85892-92-8

(5R)-6-methyl-(8R)-acetoxymethyl-Δ9,10-ergolene

Conditions
ConditionsYield
With pyridine Ambient temperature;90%
In pyridine Ambient temperature;90%
With pyridine
In pyridine Ambient temperature; Yield given;
methanol
67-56-1

methanol

lysergol
602-85-7

lysergol

10alpha-methoxy-9,10-dihydrolysergol
35121-60-9

10alpha-methoxy-9,10-dihydrolysergol

Conditions
ConditionsYield
With sulfuric acid at 20 - 40℃; for 6h; Inert atmosphere; UV-irradiation;85.3%
With sulfuric acid at 30 - 40℃; for 48h; Temperature; Irradiation;49.7 g
With sulfuric acid at 25 - 30℃; for 4h; Sealed tube; Irradiation;
methanol
67-56-1

methanol

lysergol
602-85-7

lysergol

((6aR,9R)-9-Hydroxymethyl-7-methyl-6a,7,8,9-tetrahydro-6H-indolo[4,3-fg]quinolin-4-yl)-methanol
86749-38-4

((6aR,9R)-9-Hydroxymethyl-7-methyl-6a,7,8,9-tetrahydro-6H-indolo[4,3-fg]quinolin-4-yl)-methanol

Conditions
ConditionsYield
With potassium hydroxide at 23℃; electrolysis at 1.2 V vs standard calomel electrode at graphite electrodes;80%
4-methoxy-benzoyl chloride
100-07-2

4-methoxy-benzoyl chloride

lysergol
602-85-7

lysergol

O-4-Methoxybenzoyl-lysergol-hydrochlorid
85893-19-2

O-4-Methoxybenzoyl-lysergol-hydrochlorid

Conditions
ConditionsYield
With pyridine Ambient temperature;80%
m-Chlorobenzoyl chloride
618-46-2

m-Chlorobenzoyl chloride

lysergol
602-85-7

lysergol

O-3-Chlorbenzoyl-lysergol
85893-12-5

O-3-Chlorbenzoyl-lysergol

Conditions
ConditionsYield
With pyridine Ambient temperature;77%
chlorure d'acide ethyl-2 butyrique
2736-40-5

chlorure d'acide ethyl-2 butyrique

lysergol
602-85-7

lysergol

9,10-didehydro-6-methyl-8β-ergolinylmethyl-2-ethylbutyrate
31955-01-8

9,10-didehydro-6-methyl-8β-ergolinylmethyl-2-ethylbutyrate

Conditions
ConditionsYield
dmap In pyridine; chloroform at 0 - 20℃; Acylation;76%
With pyridine at 70℃;
With pyridine; dmap
4-chlorobenzoyl chloride
586-75-4

4-chlorobenzoyl chloride

lysergol
602-85-7

lysergol

O-4-Brombenzoyl-lysergol
85893-14-7

O-4-Brombenzoyl-lysergol

Conditions
ConditionsYield
With pyridine Ambient temperature;75%
(R,S)-(+/-)-2-methylbutyrochloride

(R,S)-(+/-)-2-methylbutyrochloride

lysergol
602-85-7

lysergol

9,10-didehydro-6-methyl-8β-ergolinylmethyl R,S-2-methylbutyrate

9,10-didehydro-6-methyl-8β-ergolinylmethyl R,S-2-methylbutyrate

Conditions
ConditionsYield
dmap In pyridine; chloroform at 0 - 20℃; Acylation;71%
3,4,5-Trimethoxybenzoyl chloride
4521-61-3

3,4,5-Trimethoxybenzoyl chloride

lysergol
602-85-7

lysergol

O-3,4,5-Trimethoxybenzoyl-lysergol-hydrochlorid
85893-20-5

O-3,4,5-Trimethoxybenzoyl-lysergol-hydrochlorid

Conditions
ConditionsYield
With pyridine at 100℃; for 1h;69%
(S)-2-methylbutanoyl chloride
27763-54-8

(S)-2-methylbutanoyl chloride

lysergol
602-85-7

lysergol

9,10-didehydro-6-methyl-8β-ergolinylmethyl S-2-methylbutyrate
141978-81-6

9,10-didehydro-6-methyl-8β-ergolinylmethyl S-2-methylbutyrate

Conditions
ConditionsYield
dmap In pyridine; chloroform at 0 - 20℃; Acylation;67%
With pyridine; dmap
4-chloro-benzoyl chloride
122-01-0

4-chloro-benzoyl chloride

lysergol
602-85-7

lysergol

O-4-Chlorbenzoyl-lysergol-hydrochlorid
85893-13-6

O-4-Chlorbenzoyl-lysergol-hydrochlorid

Conditions
ConditionsYield
With pyridine Ambient temperature;65%
m-anisoyl chloride
1711-05-3

m-anisoyl chloride

lysergol
602-85-7

lysergol

O-3-Methoxybenzoyl-lysergol-hydrochlorid
85893-18-1

O-3-Methoxybenzoyl-lysergol-hydrochlorid

Conditions
ConditionsYield
With pyridine at 100℃;63%
benzyl bromide
100-39-0

benzyl bromide

lysergol
602-85-7

lysergol

1-benzyl-lysergol

1-benzyl-lysergol

Conditions
ConditionsYield
With potassium hydroxide In dimethyl sulfoxide at 20℃; for 3h;63%
3-Methylbenzoyl chloride
1711-06-4

3-Methylbenzoyl chloride

lysergol
602-85-7

lysergol

O-3-Methylbenzoyl-lysergol-hydrochlorid
85893-16-9

O-3-Methylbenzoyl-lysergol-hydrochlorid

Conditions
ConditionsYield
With pyridine at 100℃; for 1h;57%
4-methyl-benzoyl chloride
874-60-2

4-methyl-benzoyl chloride

lysergol
602-85-7

lysergol

O-4-Methylbenzoyl-lysergol
85893-17-0

O-4-Methylbenzoyl-lysergol

Conditions
ConditionsYield
With pyridine Ambient temperature;53%
2-Fluorobenzoyl chloride
393-52-2

2-Fluorobenzoyl chloride

lysergol
602-85-7

lysergol

O-2-Fluorbenzoyl-lysergol-hydrochlorid
85893-11-4

O-2-Fluorbenzoyl-lysergol-hydrochlorid

Conditions
ConditionsYield
With pyridine Ambient temperature;40%
ortho-toluoyl chloride
933-88-0

ortho-toluoyl chloride

lysergol
602-85-7

lysergol

O-2-Methylbenzoyl-lysergol-hydrochlorid
85893-15-8

O-2-Methylbenzoyl-lysergol-hydrochlorid

Conditions
ConditionsYield
With pyridine at 100℃;31%
lysergol
602-85-7

lysergol

(3β)-2,3-dihydrolysergole
114249-76-2

(3β)-2,3-dihydrolysergole

Conditions
ConditionsYield
With triethylsilane; trifluoroacetic acid for 3h; Ambient temperature;25%
lysergol
602-85-7

lysergol

4-nitrophenyl-β-D-galactopyranoside
3150-24-1

4-nitrophenyl-β-D-galactopyranoside

lysergol-β-D-galactoside

lysergol-β-D-galactoside

Conditions
ConditionsYield
With 2-hydroxyethanethiol; citric acid; magnesium chloride at 24℃; β-galactosidase from Aspergillus oryzae, K-Pi buffer;22%
lysergol
602-85-7

lysergol

methyl iodide
74-88-4

methyl iodide

1-Methyllysergol
5572-96-3

1-Methyllysergol

Conditions
ConditionsYield
With potassium amide; ferric nitrate In diethyl ether; ammonia at -50 - -40℃; for 0.5h;17%
Stage #1: lysergol With potassium hydroxide In 1-methyl-pyrrolidin-2-one at 20℃; for 0.75h;
Stage #2: methyl iodide In 1-methyl-pyrrolidin-2-one for 2h; Solvent;
48.2 g
lysergol
602-85-7

lysergol

Sucrose
57-50-1

Sucrose

A

(2R,3S,4S,5R)-2,5-Bis-hydroxymethyl-2-((6aR,9R)-7-methyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinolin-9-ylmethoxy)-tetrahydro-furan-3,4-diol

(2R,3S,4S,5R)-2,5-Bis-hydroxymethyl-2-((6aR,9R)-7-methyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinolin-9-ylmethoxy)-tetrahydro-furan-3,4-diol

B

penniclavine
519-13-1

penniclavine

Conditions
ConditionsYield
With succinic acid; DL-5-fluorotryptophan In water at 24℃; for 1296h; Claviceps purpurea 88-EP-47;A 9.2%
B n/a
lysergol
602-85-7

lysergol

A

(2R,3S,4S,5R)-2,5-Bis-hydroxymethyl-2-((6aR,9R)-7-methyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinolin-9-ylmethoxy)-tetrahydro-furan-3,4-diol

(2R,3S,4S,5R)-2,5-Bis-hydroxymethyl-2-((6aR,9R)-7-methyl-4,6,6a,7,8,9-hexahydro-indolo[4,3-fg]quinolin-9-ylmethoxy)-tetrahydro-furan-3,4-diol

B

penniclavine
519-13-1

penniclavine

Conditions
ConditionsYield
With succinic acid; DL-5-fluorotryptophan; Sucrose In water at 24℃; for 1296h; Claviceps purpurea 88-EP-47;A 9.2%
B n/a
lysergol
602-85-7

lysergol

(9R)-9-acetoxymethyl-4-acetyl-7-methyl-4,5,7,8,9,10-hexahydro-indolo[4,3-fg]quinoline

(9R)-9-acetoxymethyl-4-acetyl-7-methyl-4,5,7,8,9,10-hexahydro-indolo[4,3-fg]quinoline

Conditions
ConditionsYield
With hydrogenchloride; acetic acid Behandeln des Reaktionsprodukts mit Acetanhydrid in Pyridin;
2-Mercaptobenzothiazole
149-30-4

2-Mercaptobenzothiazole

lysergol
602-85-7

lysergol

8β-benzothiazol-2-ylsulfanylmethyl-6-methyl-9,10-didehydro-ergoline

8β-benzothiazol-2-ylsulfanylmethyl-6-methyl-9,10-didehydro-ergoline

Conditions
ConditionsYield
(i) MeSO2Cl, MeCN, (ii) /BRN= 508810/, HMPT, H2O; Multistep reaction;
2-furancarbonyl chloride
527-69-5

2-furancarbonyl chloride

lysergol
602-85-7

lysergol

O-Furfuroyl-2'-lysergol
87633-44-1

O-Furfuroyl-2'-lysergol

Conditions
ConditionsYield
With pyridine at 70℃;

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