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product Name 9,10-didehydro-6-methylergoline-8β-methanol Alias 10-didehydro-6-methyl-(8-beta)-ergoline-8-methano;9,10-didehydro-8-hydroxymethyl-6-methyl-ergolin;LYSERGOL;(5β)-9,10-Didehydro-6-methylergoline-8β
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Min.Order:1 Gram
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inquirylysergol
Conditions | Yield |
---|---|
With magnesium In methanol Inert atmosphere; | 93% |
lysergic acid methyl ester
A
((6aR,9S)-7-methyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-yl)methanol
B
lysergol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 0.166667h; | A 24% B 49% |
Conditions | Yield |
---|---|
With sodium hydroxide; 9-borabicyclo[3.3.1]nonane dimer; dihydrogen peroxide 1.) THF, 60 deg C, 24 h, 2.) THF, 40 deg C, 2 h; Yield given. Multistep reaction; |
lysergol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; diethyl ether |
lysergol
Conditions | Yield |
---|---|
With sodium butanolate; butan-1-ol |
Conditions | Yield |
---|---|
With potassium hydroxide at 140℃; |
elymoclavine
sodium butanolate
butan-1-ol
A
((6aR,9S)-7-methyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-yl)methanol
B
lysergol
elymoclavine
A
((6aR,9S)-7-methyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinolin-9-yl)methanol
B
lysergol
Conditions | Yield |
---|---|
at 140℃; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 0.34 g / Woelm alumina / toluene / 2.5 h / Heating 2: 1.) 9-BBN, 2.) NaOH, 30percent aq. H2O2 / 1.) THF, 60 deg C, 24 h, 2.) THF, 40 deg C, 2 h View Scheme |
lysergol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium naphthalenide / tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere 2: sodium cyanoborohydride; acetic acid / methanol / 1 h / 25 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
With sodium cyanoborohydride; acetic acid In methanol at 25℃; for 1h; Inert atmosphere; | 5.2 mg |
lysergol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere 2: magnesium / methanol / Inert atmosphere View Scheme |
lysergol
9,10-dihydrolysergol
Conditions | Yield |
---|---|
With hydrogen; 5%-palladium/activated carbon In N,N-dimethyl-formamide at 50 - 60℃; under 2068.65 - 2585.81 Torr; | 97% |
With methanol; nickel In 1,4-dioxane Heating; | 90% |
With methanol; Ra-Ni In 1,4-dioxane for 0.25h; Product distribution; Heating; different ratio of the solvents and times; | |
With hydrogen; palladium on activated charcoal In pyridine; N,N-dimethyl-formamide under 3750.3 Torr; |
tert-butyldimethylsilyl chloride
lysergol
8β-(tert-butyldimethylsiloxymethyl)-9,10-didehydro-6-methyl-ergoline
Conditions | Yield |
---|---|
With triethylamine In water; N,N-dimethyl-formamide at 20℃; for 4 - 5h; | 96.5% |
acetic anhydride
lysergol
(5R)-6-methyl-(8R)-acetoxymethyl-Δ9,10-ergolene
Conditions | Yield |
---|---|
With pyridine Ambient temperature; | 90% |
In pyridine Ambient temperature; | 90% |
With pyridine | |
In pyridine Ambient temperature; Yield given; |
Conditions | Yield |
---|---|
With sulfuric acid at 20 - 40℃; for 6h; Inert atmosphere; UV-irradiation; | 85.3% |
With sulfuric acid at 30 - 40℃; for 48h; Temperature; Irradiation; | 49.7 g |
With sulfuric acid at 25 - 30℃; for 4h; Sealed tube; Irradiation; |
methanol
lysergol
((6aR,9R)-9-Hydroxymethyl-7-methyl-6a,7,8,9-tetrahydro-6H-indolo[4,3-fg]quinolin-4-yl)-methanol
Conditions | Yield |
---|---|
With potassium hydroxide at 23℃; electrolysis at 1.2 V vs standard calomel electrode at graphite electrodes; | 80% |
4-methoxy-benzoyl chloride
lysergol
O-4-Methoxybenzoyl-lysergol-hydrochlorid
Conditions | Yield |
---|---|
With pyridine Ambient temperature; | 80% |
Conditions | Yield |
---|---|
With pyridine Ambient temperature; | 77% |
chlorure d'acide ethyl-2 butyrique
lysergol
9,10-didehydro-6-methyl-8β-ergolinylmethyl-2-ethylbutyrate
Conditions | Yield |
---|---|
dmap In pyridine; chloroform at 0 - 20℃; Acylation; | 76% |
With pyridine at 70℃; | |
With pyridine; dmap |
Conditions | Yield |
---|---|
With pyridine Ambient temperature; | 75% |
lysergol
Conditions | Yield |
---|---|
dmap In pyridine; chloroform at 0 - 20℃; Acylation; | 71% |
3,4,5-Trimethoxybenzoyl chloride
lysergol
O-3,4,5-Trimethoxybenzoyl-lysergol-hydrochlorid
Conditions | Yield |
---|---|
With pyridine at 100℃; for 1h; | 69% |
(S)-2-methylbutanoyl chloride
lysergol
9,10-didehydro-6-methyl-8β-ergolinylmethyl S-2-methylbutyrate
Conditions | Yield |
---|---|
dmap In pyridine; chloroform at 0 - 20℃; Acylation; | 67% |
With pyridine; dmap |
4-chloro-benzoyl chloride
lysergol
O-4-Chlorbenzoyl-lysergol-hydrochlorid
Conditions | Yield |
---|---|
With pyridine Ambient temperature; | 65% |
Conditions | Yield |
---|---|
With pyridine at 100℃; | 63% |
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 20℃; for 3h; | 63% |
3-Methylbenzoyl chloride
lysergol
O-3-Methylbenzoyl-lysergol-hydrochlorid
Conditions | Yield |
---|---|
With pyridine at 100℃; for 1h; | 57% |
Conditions | Yield |
---|---|
With pyridine Ambient temperature; | 53% |
2-Fluorobenzoyl chloride
lysergol
O-2-Fluorbenzoyl-lysergol-hydrochlorid
Conditions | Yield |
---|---|
With pyridine Ambient temperature; | 40% |
ortho-toluoyl chloride
lysergol
O-2-Methylbenzoyl-lysergol-hydrochlorid
Conditions | Yield |
---|---|
With pyridine at 100℃; | 31% |
lysergol
(3β)-2,3-dihydrolysergole
Conditions | Yield |
---|---|
With triethylsilane; trifluoroacetic acid for 3h; Ambient temperature; | 25% |
Conditions | Yield |
---|---|
With 2-hydroxyethanethiol; citric acid; magnesium chloride at 24℃; β-galactosidase from Aspergillus oryzae, K-Pi buffer; | 22% |
Conditions | Yield |
---|---|
With potassium amide; ferric nitrate In diethyl ether; ammonia at -50 - -40℃; for 0.5h; | 17% |
Stage #1: lysergol With potassium hydroxide In 1-methyl-pyrrolidin-2-one at 20℃; for 0.75h; Stage #2: methyl iodide In 1-methyl-pyrrolidin-2-one for 2h; Solvent; | 48.2 g |
Conditions | Yield |
---|---|
With succinic acid; DL-5-fluorotryptophan In water at 24℃; for 1296h; Claviceps purpurea 88-EP-47; | A 9.2% B n/a |
Conditions | Yield |
---|---|
With succinic acid; DL-5-fluorotryptophan; Sucrose In water at 24℃; for 1296h; Claviceps purpurea 88-EP-47; | A 9.2% B n/a |
lysergol
Conditions | Yield |
---|---|
With hydrogenchloride; acetic acid Behandeln des Reaktionsprodukts mit Acetanhydrid in Pyridin; |
Conditions | Yield |
---|---|
(i) MeSO2Cl, MeCN, (ii) /BRN= 508810/, HMPT, H2O; Multistep reaction; |
Conditions | Yield |
---|---|
With pyridine at 70℃; |
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