Hangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting Capstone 62-AL;Perfluorohexyl ethanol;2-(perfluorohexyl)ethanol, CAS No.:647-42-7, Please contact us by email freely. We are leading export
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inquiryHigh quality 2-(Perfluorohexyl) Ethyl Alcohol CAS 647-42-7 with factory price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermediates, F
Cas:647-42-7
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inquiryhigh quality Appearance:Colorless liquid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
Cas:647-42-7
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:647-42-7
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:647-42-7
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inquiryProduct Name: 3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluoro-1-octanol Synonyms: 1,1,2,2-Tetrahydroperfluoro-1-octanol;3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octano;3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluoro-octan-1-ol;3,3,4,4,5,5,6,6,7,7,8,8
Cas:647-42-7
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inquiryOur advantages: 1. High quality and competitive price: 1) Standard: BP/USP/EP/ enterprise standard 2) All purity ≥99% 3) We are manufacturers and can provide high quality products at factory prices. 2. Fast and safe delivery 1) The package c
Cas:647-42-7
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:647-42-7
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inquiryProduct Name: 3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluoro-1-octanol Synonyms: 1,1,2,2-Tetrahydroperfluoro-1-octanol;3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-1-octano;3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluoro-octan
Appearance:Colorless liquid Storage:R.T Package:25kg/Barrel Application:Intermediate of perfluorohexyl ethyl acrylate Transportation:Express/Sea/Air Port:Any port in China
Cas:647-42-7
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry1H,1H,2H,2H-PERFLUORO-1-OCTANOL CAS:647-42-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality org
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:647-42-7
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiry1. Well-equipped, stable and high-quality raw material supply chain, to provide customers with the best quality products. 2.Strict quality inspection process and professional certificate testing to ensure the quality level of the final product. 3.E
Cas:647-42-7
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:647-42-7
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:647-42-7
Min.Order:4 Kilogram
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:647-42-7
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:647-42-7
Min.Order:10 Gram
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inquirySuperior quality, moderate price & quick delivery. Appearance:Colorless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:1H,1H, 2H, 2H-T
Cas:647-42-7
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inquiryProduct name: Perfluorohexyl Ethanol CAS No.: 647-42-7 Molecule Formula:C8H5F13O Molecule Weight:364.10 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:647-42-7
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inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Product Name:1H,1H,2H,2H-PERFLUORO-1-OCTANOL CAS No
Cas:647-42-7
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inquiry1H,1H,2H,2H-PERFLUORO-1-OCTANOL Chemical Properties Boiling point 88-95 °C28 mm Hg(lit.) density 1.651 g/mL at 25 °C(lit.) refractive index n20/D 1.313(lit.) RTECS RH1460000 Fp 197 °F form liquid pka 14.26&plusm
Cas:647-42-7
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:647-42-7
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FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:647-42-7
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:647-42-7
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inquiry1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
With hydrogenchloride; formic acid; oxygen; copper; zinc In water at 80℃; for 2h; Product distribution; various solvents, water concentration; | 100% |
With water In N,N-dimethyl-formamide at 125 - 130℃; under 2625.26 Torr; for 32h; Large scale; Green chemistry; | 88% |
Yield given. Multistep reaction; |
potassium 8,8,8,7,7,6,6,5,5,4,4,3,3-tridecafluorooctyl sulfate
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; water at 20℃; for 0.166667h; | 96% |
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
With dihydrogen peroxide; sodium hydroxide In water at 45℃; for 2h; Temperature; | 91% |
3,4-Dihydro-5-<(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro)octyloxy>-2H-pyrrole
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
Conditions | Yield |
---|---|
With 2-pyrrolidinon at 140℃; for 3h; | A 90% B 1% |
3-(2-fluoro-phenyl)-3-hydroxy-propionic acid 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl ester
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3-hydroxy-3-(2'-fluorophenyl)propanol
Conditions | Yield |
---|---|
With lithium triethylborohydride In tetrahydrofuran at 20℃; for 2h; | A n/a B 88% |
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
(C6F13C2H4O)2SO2
Conditions | Yield |
---|---|
Stage #1: 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane With sulfuric acid; sulfur trioxide In water at 30℃; for 1.66h; Stage #2: With sodium sulfite; water at 0 - 80℃; for 2h; Product distribution / selectivity; | A 82.3% B n/a |
Stage #1: 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane With sulfuric acid; sulfur trioxide at 20℃; for 1.66h; Stage #2: With sodium sulfite; water at 20 - 80℃; for 2h; Product distribution / selectivity; | A 81.1% B n/a |
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
(C6F13C2H4O)2SO2
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
Stage #1: 1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane; (C6F13C2H4O)2SO2 With sulfuric acid; sulfur trioxide at 20 - 80℃; for 1.66h; Stage #2: With sodium sulfite; water at 20 - 80℃; for 2h; Product distribution / selectivity; | 75.9% |
Conditions | Yield |
---|---|
Stage #1: (C6F13C2H4O)2SO2 With sulfuric acid; sulfur trioxide at 20 - 80℃; for 1.33h; Stage #2: With water at 20 - 80℃; for 1.5 - 2h; Product distribution / selectivity; | 70.3% |
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
N,N-dimethyl-formamide
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
dimethylamine hydriodide
Conditions | Yield |
---|---|
With water Product distribution; | A 33% B n/a C 66% |
3-hydroxy-3-phenyl-propionic acid 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl ester
A
1-phenyl-1,3-propanediol
B
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
With lithium triethylborohydride In tetrahydrofuran at 20℃; for 2h; | A 61% B n/a |
3-hydroxy-3-o-tolyl-propionic acid 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyl ester
A
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
With lithium triethylborohydride In tetrahydrofuran at 20℃; for 2h; | A n/a B 55% |
N-(2-formylaminoethyl)formamide
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 150℃; for 24h; | A 31.4% B 16.7% C 51% |
In N,N-dimethyl-formamide at 150℃; for 24h; | A 31.4% B 16.7% C 51% |
piperidin-2-one
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
Conditions | Yield |
---|---|
at 140℃; for 7.25h; Yields of byproduct given; | A n/a B n/a C 18.3% |
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
With sodium azide In N,N-dimethyl-formamide for 12h; Reflux; | A n/a B 15% |
N-Methylformamide
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
With sodium hydroxide; water 1.) 140 degC, 6 h; 2.)62-85 degC, 22 h; Yield given. Multistep reaction; |
N-Methylformamide
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
Conditions | Yield |
---|---|
at 140℃; for 1h; Product distribution; Rate constant; var. temp., time, substrate (DMF) investigated; |
N-Methylformamide
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
Yield given. Yields of byproduct given; |
N-isopropylformamide
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
Conditions | Yield |
---|---|
With water at 140℃; for 1h; Product distribution; Rate constant; var. temp., time, substrate (DMF, 1,2-ethanyl-bis-formamide) investigated; |
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 30℃; Product distribution; variation of condition; also with NaOMe; | |
With radical initiator; water In N,N-dimethyl-formamide Heating; | |
With water; lithium chloride In N,N-dimethyl-formamide for 69h; electrolysis at carbon fibre cathode; | A 68 % Spectr. B 32 % Spectr. |
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
Conditions | Yield |
---|---|
With water; formamide at 150℃; for 6h; | A 5.2 % Chromat. B 1.4 % Chromat. C n/a D 7.2 % Chromat. |
With water; formamide at 140℃; for 4.5h; | A 3.9 % Chromat. B 3.9 % Chromat. C n/a D 10.0 % Chromat. |
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
C
(perfluoro-n-hexyl)ethane
Conditions | Yield |
---|---|
With water; lithium chloride In N,N-dimethyl-formamide Product distribution; effect of quantity of water and current on electroreduction; | A 80 % Spectr. B 5 % Spectr. C 15 % Spectr. |
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
With N-Methylformamide Yield given. Yields of byproduct given; |
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
formamide
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
Conditions | Yield |
---|---|
With water at 140℃; for 4.5h; | A 3.9 % Chromat. B 3.9 % Chromat. C n/a D 10.0 % Chromat. |
formamide
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
Conditions | Yield |
---|---|
With 2-(F-hexyl)-1-iodoethane; water at 140℃; for 4.5h; | A 3.9 % Chromat. B 3.9 % Chromat. C n/a D 10.0 % Chromat. |
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl trifluoromethanesulfonate
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
C
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro-octyloxy)-octane
Conditions | Yield |
---|---|
With solution aqueuse de soude 10 N for 0.25h; Heating; | A 33 % Spectr. B 31 % Spectr. C 35 % Spectr. |
2-pyrrolidinon
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
Conditions | Yield |
---|---|
at 140℃; for 1h; Product distribution; Mechanism; Rate constant; other times, temperatures; also with ε-caprolactam; |
2-pyrrolidinon
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
1-(1-pyrrolidin-2-yl)-2-pyrrolidone
Conditions | Yield |
---|---|
With potassium carbonate 1.) 140 deg C, 6.00 h, 2.) EtOH, CHCl3, 68 deg C, 5 h; Yield given. Multistep reaction. Yields of byproduct given; |
2-pyrrolidinon
3,4-Dihydro-5-<(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro)octyloxy>-2H-pyrrole
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
1-(1-pyrrolidin-2-yl)-2-pyrrolidone
Conditions | Yield |
---|---|
In toluene at 140℃; Rate constant; also without solvent at other temperatures; |
2-pyrrolidinon
3,4,5,6-Tetrahydro-7-<2-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro)octyloxy>-2H-azepine
A
caprolactam
B
1H,1H,2H,2H-tridecafluoro-n-octanol
C
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
D
1-(4,5,6,7-tetrahydro-3H-azepin-2-yl)-2-pyrrolidinone
Conditions | Yield |
---|---|
In toluene at 140℃; for 24h; Yields of byproduct given. Title compound not separated from byproducts; | A n/a B n/a C n/a D 47.4 % Chromat. |
In toluene at 140℃; Rate constant; |
piperidin-2-one
1,1,1,2,2,3,3,4,4,5,5,6,6-Tridecafluoro-8-iodooctane
A
1H,1H,2H,2H-tridecafluoro-n-octanol
B
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooct-1-ene
Conditions | Yield |
---|---|
at 140℃; for 1h; Rate constant; Mechanism; other times; also with ε-caprolactam; |
phosgene
1H,1H,2H,2H-tridecafluoro-n-octanol
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl chloroformate
Conditions | Yield |
---|---|
In diethyl ether for 24h; Heating; | 100% |
Conditions | Yield |
---|---|
With bismuth(lll) trifluoromethanesulfonate In 1,2-dichloro-ethane at 80℃; for 24h; Inert atmosphere; Schlenk technique; chemoselective reaction; | 100% |
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; palladium diacetate at 45℃; for 96h; Time; Temperature; | 98.2% |
1H,1H,2H,2H-tridecafluoro-n-octanol
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctanoic acid
Conditions | Yield |
---|---|
With chromium(VI) oxide; sulfuric acid In diethyl ether; acetone for 0.0833333h; | 98% |
Stage #1: 1H,1H,2H,2H-tridecafluoro-n-octanol With Jones reagent In acetone Stage #2: With isopropyl alcohol In acetone | 84% |
With chromium(VI) oxide; sulfuric acid In diethyl ether; water; acetone for 0.5h; Jones oxidation; | 76% |
1H,1H,2H,2H-tridecafluoro-n-octanol
β,β,β-trichloroethoxysulfonyl isocyanate
Conditions | Yield |
---|---|
at 20℃; for 0.0166667h; Addition; | 98% |
1H,1H,2H,2H-tridecafluoro-n-octanol
<(4-nitrophenyl)oxy>sulfonyl isocyanate
Conditions | Yield |
---|---|
at 20℃; for 0.0166667h; Addition; | 98% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 140℃; for 6h; | 98% |
1H,1H,2H,2H-tridecafluoro-n-octanol
acrylic acid methyl ester
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-propenoate
Conditions | Yield |
---|---|
With C32H16F52O4Ti; hydroquinone In toluene at 80℃; for 3.5h; Reagent/catalyst; Large scale; | 97.2% |
With titanium(III) sulphate; hydroquinone In cyclohexane at 120℃; for 8h; Reagent/catalyst; |
ethyl bromide
1H,1H,2H,2H-tridecafluoro-n-octanol
1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluoro-9-oxaundecane
Conditions | Yield |
---|---|
With potassium hydroxide In 1-methyl-pyrrolidin-2-one; water at 50 - 70℃; for 7h; | 97% |
succinic acid anhydride
1H,1H,2H,2H-tridecafluoro-n-octanol
1H,2H,2H-perfluoro-1-octyl succinic acid monoester
Conditions | Yield |
---|---|
With dmap In tetrahydrofuran at 100℃; for 2h; | 97% |
With triethylamine In tetrahydrofuran at 100℃; for 1h; | 94% |
In tetrahydrofuran at 100℃; for 1h; | 94% |
With triethylamine; N-ethyl-N,N-diisopropylamine | |
With pyridine In 1,2-dimethoxyethane at 65 - 75℃; for 36h; Inert atmosphere; |
1H,1H,2H,2H-tridecafluoro-n-octanol
3,3,4,4,5,5,6,6,7,7,8,8,8-Tridecafluoro-octyl phosphorodichloridate
Conditions | Yield |
---|---|
With triethylamine; trichlorophosphate In diethyl ether for 1h; Ambient temperature; | 96% |
With triethylamine; trichlorophosphate In diethyl ether at 0℃; |
Conditions | Yield |
---|---|
Pd-C In hydrogen | 96% |
1H,1H,2H,2H-tridecafluoro-n-octanol
toluene-4-sulfonic acid
glycine
glycine 2-perfluorohexylethyl ester p-toluenesulphonate
Conditions | Yield |
---|---|
In toluene for 4h; Heating; | 96% |
In cyclohexane for 17h; Reflux; | 78% |
Conditions | Yield |
---|---|
With saccharin sodium salt at 80 - 90℃; for 2h; | 95.5% |
1H,1H,2H,2H-tridecafluoro-n-octanol
3-chloroprop-1-ene
8-(allyloxyl)-1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorooctane
Conditions | Yield |
---|---|
With sodium hydroxide; tetra(n-butyl)ammonium hydroxide at 40℃; for 6h; | 95% |
With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate at 45℃; for 6h; | 94% |
With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate at 30℃; for 8h; Yield given; |
1H,1H,2H,2H-tridecafluoro-n-octanol
isocyanate de chloro-4 phenoxysulfonyle
Conditions | Yield |
---|---|
at 20℃; for 0.0166667h; Addition; | 95% |
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
Pd-C In hydrogen | 95% |
With hydrogen; palladium on activated charcoal at 160℃; for 10h; atmospheric pressure; | 92% |
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
With tetraphosphorus decasulfide In toluene for 12h; Heating; | 95% |
p-(chloromethyl)benzoyl chloride
1H,1H,2H,2H-tridecafluoro-n-octanol
C16H10ClF13O2
Conditions | Yield |
---|---|
With triethylamine In acetone at 10 - 20℃; for 2h; Inert atmosphere; | 95% |
With triethylamine In acetone at 10 - 20℃; for 2h; Inert atmosphere; | 95% |
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
With phosphorus pentoxide; phosphoric acid In water at 50 - 60℃; for 48h; Temperature; | 94.7% |
poly(methacrylic acid)
1H,1H,2H,2H-tridecafluoro-n-octanol
3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl 2-methylpropenoate
Conditions | Yield |
---|---|
With hydroquinone; toluene-4-sulfonic acid In toluene at 115℃; for 5h; | 94% |
With sulfuric acid; hydroquinone In benzene Heating; | |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; |
1H,1H,2H,2H-tridecafluoro-n-octanol
p-toluenesulfonyl chloride
toluene-4-sulfonic acid 3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluorooctyl ester
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; | 94% |
With triethylamine In dichloromethane | 92% |
With triethylamine In dichloromethane at 0 - 20℃; Tosylation; | 91% |
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); triethylamine; 1,4-di(diphenylphosphino)-butane In dichloromethane at 60℃; for 48h; Inert atmosphere; Schlenk technique; stereoselective reaction; | 94% |
O-methylcaprolactim
1H,1H,2H,2H-tridecafluoro-n-octanol
3,4,5,6-Tetrahydro-7-<2-(3,3,4,4,5,5,6,6,7,7,8,8,8-tridecafluoro)octyloxy>-2H-azepine
Conditions | Yield |
---|---|
Heating; | 93.4% |
1H,1H,2H,2H-tridecafluoro-n-octanol
allyl bromide
8-(allyloxyl)-1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorooctane
Conditions | Yield |
---|---|
With sodium hydroxide at 60℃; under 75.0075 Torr; for 1h; Temperature; Inert atmosphere; Large scale; | 93% |
With sodium hydroxide at 60 - 80℃; for 4h; Inert atmosphere; | 88% |
With sodium hydroxide at 60 - 80℃; for 4h; Inert atmosphere; | 88% |
1H,1H,2H,2H-tridecafluoro-n-octanol
2-Bromoacetyl bromide
Bromure d'acetate de 2-F-hexylethyle
Conditions | Yield |
---|---|
In diethyl ether at 0 - 20℃; for 12h; | 93% |
In diethyl ether at 60℃; for 12h; | 68% |
at 60℃; |
1H,1H,2H,2H-tridecafluoro-n-octanol
Conditions | Yield |
---|---|
Stage #1: 1H,1H,2H,2H-tridecafluoro-n-octanol With pyridine; di(succinimido) carbonate In N,N-dimethyl-formamide at 40℃; for 15h; Stage #2: Nα-(tert-butyloxycarbonyl)-(R)-lysine tert-butyl ester In N,N-dimethyl-formamide at 20 - 30℃; | 93% |
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal at 105℃; for 8h; | 92% |
With hydrogen; palladium on activated charcoal at 105℃; for 8h; atmospheric pressure; | 92% |
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