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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

3-dimethylamino-1-phenyl-propan-1-ol

Cas:5554-64-3

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Benzenemethanol,α-[2-(dimethylamino)ethyl]-

Cas:5554-64-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Benzenemethanol,α-[2-(dimethylamino)ethyl]-

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Benzenemethanol,α-[2-(dimethylamino)ethyl]-

Cas:5554-64-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

N,N-Dimethyl-3-phenyl-3-hydroxypropylamine

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

3-dimethylamino-1-phenyl-propan-1-ol

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

hight degree of purity Application:Fine chemical intermediates, used as the main raw material for he synthesis of various pesticides, medicines, surfactants, polymer monomers, Ond Ontifungal agents

Benzenemethanol,α-[2-(dimethylamino)ethyl]-

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

DB BIOTECH CO., LTD

best seller Application:API

3-dimethylamino-1-phenyl-propan-1-ol

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

3-dimethylamino-1-phenyl-propan-1-ol

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SAGECHEM LIMITED

5554-64-3 Application:intermediate

Benzenemethanol, a-[2-(dimethylamino)ethyl]-

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hunan Longxianng Runhui Trading Co.,Ltd

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

3-Dimethylamino-1-phenyl-propan-1-ol

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Terui OP New Material Technology Co., Ltd.

The factory supplies Application:manufacturing supplies

Benzenemethanol,α-[2-(dimethylamino)ethyl]-

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

5554-64-3

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Muhuang Technology Co., Ltd

best seller Application:API

3-dimethylamino-1-phenyl-propan-1-ol

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

3-dimethylamino-1-phenyl-propan-1-ol

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Bide Pharmatech Ltd

Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical

3-(Dimethylamino)-1-phenylpropan-1-ol

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Other

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

Benzenemethanol, a-[2-(dimethylamino)ethyl]-

Cas:5554-64-3

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Changzhou Extraordinary Pharmatech co.,LTD

Changzhou Extraordinary Pharmatech co., LTD. As a leading chemical manufacturer and supplier in China.DAS authentication is passed.We can provide the popular precursor chemicals, we have our own strong R & D team, have our own laboratories and fa

3-Dimethylamino-1-phenyl-1-propanol

Cas:5554-64-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Toda Biotechnology Co., Limited.

Todachem specialize in exporting chemicals for 10 years, we manufacture and distribute high quality pharmaceutical APIs, intermediates, special chemicals, active molecule and other fine chemicals. We have our research laboratory and more than 100 n

Factory direct supply 3-dimethylamino-1-phenyl-propan-1-ol with best quality

Cas:5554-64-3

Min.Order:1 Kilogram

FOB Price: $90.0 / 100.0

Type:Trading Company

inquiry

Shanghai Hanhong Scientific Co.,Ltd.

factory,reasonable price Appearance:detailed see specifications Storage:Store in dry, dark and ventilated place. Package:according to the clients requirement Application:pharmaceutical intermediates Transportation:by courier,air or sea Port:S

3-(Dimethylamino)-1-phenylpropan-1-ol5554-64-3

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Nanjing Norris Pharm Technology Co., Ltd.

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

3-Dimethylamino-1-phenyl-propan-1-ol

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Chemical Technology Co.,LTD

1. Production capacity: we have three production base with high-tech production equipment and instruments, equipped with professional production personnel, meet your requirements.2. Quality assurance: we have a first-class testing equipment and testi

3-dimethylamino-1-phenyl-propan-1-ol

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Other

inquiry

Simson Pharma Limited

The system can just identify the products information in first sheet, it is not be permitted to add or edit new sheet by userself.Our products are required in MG to Gram only. · Pharmaceutical Reference Standards· Traceable workin

3-Dimethylamino-1-phenyl-1-propanol

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Shanghai PotentPharm Science and Technology Co.,Ltd

1 good quality, better price and bettter service;2 Timely delivery;3 100% refunded if parcel is not delivered or poor quality.We will try to satisfy you upon receipt of your reply. I hope that we can become a long-term cooperative partner. Applicatio

3-(DiMethylaMino)-1-phenylpropan-1-ol

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Snap Intermediates

Benzenemethanol,α-[2-(dimethylamino)ethyl]-

Cas:5554-64-3

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

3-(dimethylamino)propiophenone hydrochloride
879-72-1

3-(dimethylamino)propiophenone hydrochloride

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

Conditions
ConditionsYield
With methanol; sodium tetrahydroborate; sodium hydroxide at 20℃; for 1h; pH=12 - 13; Cooling with ice;96%
Stage #1: 3-(dimethylamino)propiophenone hydrochloride With potassium hydroxide In water
Stage #2: With methanol; sodium tetrahydroborate; potassium hydroxide at 0 - 22℃; for 1.5h;
95%
With diisobutylaluminium hydride In tetrahydrofuran; dichloromethane for 2h; Ambient temperature;92%
3-dimethylaminopropiophenone
3506-36-3

3-dimethylaminopropiophenone

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

Conditions
ConditionsYield
With sodium tetrahydroborate In water at 0 - 20℃;91%
With lithium aluminium tetrahydride
With aluminium trichloride; aluminum isopropoxide; isopropyl alcohol
N,N-Dimethyl-α-chlorobenzoylacetamide
87968-05-6

N,N-Dimethyl-α-chlorobenzoylacetamide

A

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

(+/-)-N-methylephedrine
1201-56-5

(+/-)-N-methylephedrine

Conditions
ConditionsYield
With lithium aluminium tetrahydride In diethyl ether for 20h; Heating;A n/a
B 24%
3-chloro-1-phenyl-propan-1-ol
18776-12-0

3-chloro-1-phenyl-propan-1-ol

dimethyl amine
124-40-3

dimethyl amine

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

styrene
292638-84-7

styrene

N-(chloromethyl)dimethylamine
30438-74-5

N-(chloromethyl)dimethylamine

A

2-benzyl-2-propenal
30457-88-6

2-benzyl-2-propenal

B

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

C

methyl-(3-phenyl-propyl)-amine
23580-89-4

methyl-(3-phenyl-propyl)-amine

D

bis-(3-phenyl-propyl)-amine
93948-20-0

bis-(3-phenyl-propyl)-amine

Conditions
ConditionsYield
In acetonitrile for 12h; Heating; Yield given. Further byproducts given. Yields of byproduct given;
diethyl ether
60-29-7

diethyl ether

water
7732-18-5

water

3-dimethylaminopropiophenone
3506-36-3

3-dimethylaminopropiophenone

activated aluminium

activated aluminium

A

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

B

1.6-bis-dimethylamino-3.4-diphenyl-hexanediol-(3.4)

1.6-bis-dimethylamino-3.4-diphenyl-hexanediol-(3.4)

β-dimethylamino-propiophenone hydrochloride

β-dimethylamino-propiophenone hydrochloride

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

Conditions
ConditionsYield
With water; palladium Hydrogenation;
3-dimethylamino-1-phenyl-propanone-(1)-hydrochloride

3-dimethylamino-1-phenyl-propanone-(1)-hydrochloride

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

Conditions
ConditionsYield
With water; nickel Hydrogenation;
3-(dimethylamino)propiophenone hydrochloride
879-72-1

3-(dimethylamino)propiophenone hydrochloride

water
7732-18-5

water

palladium/charcoal

palladium/charcoal

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

Conditions
ConditionsYield
Hydrogenation;
acetophenone
98-86-2

acetophenone

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 83 percent / aq. HCl / ethanol / 2 h / Heating
2: 91 percent / NaBH4 / H2O / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: hydrogenchloride / ethanol; water / 3 h / Heating / reflux
2: sodium tetrahydroborate / ethanol / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1.1: hydrogenchloride / ethanol / 2 h / Reflux
2.1: potassium hydroxide / water
2.2: 1.5 h / 0 - 22 °C
View Scheme
acetophenone
98-86-2

acetophenone

butadiynediyl-bis magnesium bromide

butadiynediyl-bis magnesium bromide

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 84 percent / conc. aq. HCl / ethanol / 2 h / Heating
2: 92 percent / DIBAL-H / tetrahydrofuran; CH2Cl2 / 2 h / Ambient temperature
View Scheme
N,N-dimethyl 3-oxo-3-phenyl-propanamide
18871-71-1

N,N-dimethyl 3-oxo-3-phenyl-propanamide

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 81 percent / N-chlorosuccinimide / CCl4 / 4 h / Heating
2: LiAlH4 / diethyl ether / 20 h / Heating
View Scheme
3-(N,N-dimethylamino)propiophenone

3-(N,N-dimethylamino)propiophenone

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

Conditions
ConditionsYield
With sodium borohydrid In methanol; water; isopropyl alcohol15.2 g (97%)
N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

3-(dimethylamino)-1-phenylpropyl chloride hydrochloride
1011-59-2

3-(dimethylamino)-1-phenylpropyl chloride hydrochloride

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-3-hydroxy-3-phenylpropylamine With hydrogenchloride In diethyl ether
Stage #2: With thionyl chloride Reflux;
96%
With hydrogenchloride; thionyl chloride In dichloromethane
With thionyl chloride In dichloromethane
5-bromo-2-chloropyridine
53939-30-3

5-bromo-2-chloropyridine

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

3-((5-bromopyridin-2-yl)oxy)-N,N-dimethyl-3-phenylpropan-1-amine
1584114-08-8

3-((5-bromopyridin-2-yl)oxy)-N,N-dimethyl-3-phenylpropan-1-amine

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-3-hydroxy-3-phenylpropylamine With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 1h;
Stage #2: 5-bromo-2-chloropyridine In N,N-dimethyl-formamide; mineral oil at 75℃; for 12h;
91%
4-nitro-1H-pyrazole
2075-46-9

4-nitro-1H-pyrazole

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

N,N-dimethyl-3-(4-nitro-1H-pyrazol-1-yl)-3-phenylpropan-1-amine
1557241-82-3

N,N-dimethyl-3-(4-nitro-1H-pyrazol-1-yl)-3-phenylpropan-1-amine

Conditions
ConditionsYield
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃;80%
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 0 - 20℃; Mitsunobu Displacement;
4-nitro-phenol
100-02-7

4-nitro-phenol

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

N,N-dimethyl-3-(4-nitrophenoxy)-3-phenylpropan-1-amine
72084-00-5

N,N-dimethyl-3-(4-nitrophenoxy)-3-phenylpropan-1-amine

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 16h; Mitsunobu Displacement;80%
With di-isopropyl azodicarboxylate; triphenylphosphine In dichloromethane at 20℃; for 48h; Mitsunobu Displacement;
N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

6-[1-(tetrahydropyran-2-yl)-1H-pyrazol-4-yl]-1-(2-trimethylsilanylethoxymethyl)-1H-indazole-3-carboxylic acid (1H-pyrazol-4-yl)amide
1422982-35-1

6-[1-(tetrahydropyran-2-yl)-1H-pyrazol-4-yl]-1-(2-trimethylsilanylethoxymethyl)-1H-indazole-3-carboxylic acid (1H-pyrazol-4-yl)amide

C36H48N8O3Si

C36H48N8O3Si

Conditions
ConditionsYield
With tributylphosphine; diethylazodicarboxylate In tetrahydrofuran at 70℃; for 1h;75%
1-indoline
496-15-1

1-indoline

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

N-[3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropyl]-N,N-dimethylamine
915953-59-2

N-[3-(2,3-dihydro-1H-indol-1-yl)-3-phenylpropyl]-N,N-dimethylamine

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-3-hydroxy-3-phenylpropylamine With methanesulfonyl chloride; triethylamine In acetonitrile at 20℃; for 3h;
Stage #2: 1-indoline With potassium carbonate at 20℃; for 14h; Further stages.;
72%
N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

phenol
108-95-2

phenol

N,N-dimethyl-3-phenoxy-3-phenyl-1-propanamine

N,N-dimethyl-3-phenoxy-3-phenyl-1-propanamine

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-3-hydroxy-3-phenylpropylamine With methanesulfonyl chloride; triethylamine In acetonitrile
Stage #2: phenol With potassium carbonate In acetonitrile for 65h; Heating;
69%
3,4-dimethoxyphenol
2033-89-8

3,4-dimethoxyphenol

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

[3-(3,4-dimethoxy-phenoxy)-3-phenyl-propyl]-dimethyl-amine

[3-(3,4-dimethoxy-phenoxy)-3-phenyl-propyl]-dimethyl-amine

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-3-hydroxy-3-phenylpropylamine With methanesulfonyl chloride; triethylamine In acetonitrile at 20℃; for 3h;
Stage #2: 3,4-dimethoxyphenol With potassium carbonate In acetonitrile for 16h; Heating;
67%
6-fluoroindoline
2343-23-9

6-fluoroindoline

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

C19H23N2F
915953-62-7

C19H23N2F

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-3-hydroxy-3-phenylpropylamine With methanesulfonyl chloride; triethylamine In acetonitrile at 20℃; for 3h;
Stage #2: 6-fluoroindoline With potassium carbonate at 20℃; for 14h; Further stages.;
64%
N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

3-chloro-N,N-dimethyl-3-phenylpropan-1-amine
79130-51-1

3-chloro-N,N-dimethyl-3-phenylpropan-1-amine

Conditions
ConditionsYield
With methanesulfonyl chloride; triethylamine In dichloromethane at 20℃;64%
N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

2-fluoro-1,4-dimethoxybenzene
82830-49-7

2-fluoro-1,4-dimethoxybenzene

[3-(2,5-dimethoxy-phenoxy)-3-phenylpropyl]dimethylamine
1342798-05-3

[3-(2,5-dimethoxy-phenoxy)-3-phenylpropyl]dimethylamine

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-3-hydroxy-3-phenylpropylamine With sodium hydride In dimethyl sulfoxide at 20℃; for 0.5h;
Stage #2: 2-fluoro-1,4-dimethoxybenzene In dimethyl sulfoxide at 135 - 140℃; for 4h;
63%
6-chloropyridine-3-ol
41288-96-4

6-chloropyridine-3-ol

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

3-((6-chloropyridin-3-yl)oxy)-N,N-dimethyl-3-phenylpropan-1-amine
1584114-00-0

3-((6-chloropyridin-3-yl)oxy)-N,N-dimethyl-3-phenylpropan-1-amine

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; Mitsunobu Displacement; Inert atmosphere;60%
N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

2,3-dihydro-4-fluoro-1H-indole
552866-98-5

2,3-dihydro-4-fluoro-1H-indole

C19H23N2F
915953-60-5

C19H23N2F

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-3-hydroxy-3-phenylpropylamine With methanesulfonyl chloride; triethylamine In acetonitrile at 20℃; for 3h;
Stage #2: 2,3-dihydro-4-fluoro-1H-indole With potassium carbonate at 20℃; for 14h; Further stages.;
51%
5-fluoroindoline
2343-22-8

5-fluoroindoline

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

C19H23N2F
915953-61-6

C19H23N2F

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-3-hydroxy-3-phenylpropylamine With methanesulfonyl chloride; triethylamine In acetonitrile at 20℃; for 3h;
Stage #2: 5-fluoroindoline With potassium carbonate at 20℃; for 14h; Further stages.;
49%
2,3-dihydro-7-fluoro-1H-indole
769966-04-3

2,3-dihydro-7-fluoro-1H-indole

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

C19H23N2F
915953-63-8

C19H23N2F

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-3-hydroxy-3-phenylpropylamine With methanesulfonyl chloride; triethylamine In acetonitrile at 20℃; for 3h;
Stage #2: 2,3-dihydro-7-fluoro-1H-indole With potassium carbonate at 20℃; for 14h; Further stages.;
47%
O-methylresorcine
150-19-6

O-methylresorcine

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

[3-(3-methoxy-phenoxy)-3-phenyl-propyl]-dimethyl-amine
57226-14-9

[3-(3-methoxy-phenoxy)-3-phenyl-propyl]-dimethyl-amine

Conditions
ConditionsYield
With PS-PPh3; dibenzyl azodicarboxylate In dichloromethane at 20℃; for 20h; Mitsunobu reaction;47%
4-fluorobenzo[1,3]dioxolane
943830-74-8

4-fluorobenzo[1,3]dioxolane

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

oxalic acid
144-62-7

oxalic acid

3-[(benzo[d][1,3]dioxolan-4-yl)oxy]-N,N-dimethyl-3-phenylpropylamine oxalate

3-[(benzo[d][1,3]dioxolan-4-yl)oxy]-N,N-dimethyl-3-phenylpropylamine oxalate

Conditions
ConditionsYield
Stage #1: 4-fluorobenzo[1,3]dioxolane; N,N-dimethyl-3-hydroxy-3-phenylpropylamine With potassium hydroxide In dimethyl sulfoxide at 85℃; for 4h;
Stage #2: oxalic acid
47%
N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

4-methoxy-phenol
150-76-5

4-methoxy-phenol

N,N-dimethyl-3-(4-methoxy-phenyloxy)-3-phenyl-propanamine

N,N-dimethyl-3-(4-methoxy-phenyloxy)-3-phenyl-propanamine

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-3-hydroxy-3-phenylpropylamine With methanesulfonyl chloride; triethylamine In acetonitrile at 20℃; for 3h;
Stage #2: 4-methoxy-phenol With potassium carbonate In acetonitrile for 16h; Heating;
46%
4-hydroxybenzotrifluoride
402-45-9

4-hydroxybenzotrifluoride

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

N,N-dimethyl-3-phenyl-3-(4-(trifluoromethyl)phenoxy)-1-propylamine
56225-81-1

N,N-dimethyl-3-phenyl-3-(4-(trifluoromethyl)phenoxy)-1-propylamine

Conditions
ConditionsYield
Stage #1: N,N-dimethyl-3-hydroxy-3-phenylpropylamine With methanesulfonyl chloride; triethylamine In acetonitrile at 20℃; for 3h;
Stage #2: 4-hydroxybenzotrifluoride With potassium carbonate In acetonitrile for 16h; Heating;
35%
4-(3-piperidin-1-yl-propoxy)-phenol
81878-15-1

4-(3-piperidin-1-yl-propoxy)-phenol

N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

dimethyl-{3-phenyl-3-[4-(3-piperidin-1-yl-propoxy)-phenoxy]-propyl}-amine

dimethyl-{3-phenyl-3-[4-(3-piperidin-1-yl-propoxy)-phenoxy]-propyl}-amine

Conditions
ConditionsYield
With PS-PPh3; dibenzyl azodicarboxylate In dichloromethane at 20℃; for 20h; Mitsunobu reaction;10%
N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

2-chloro-2,2-diphenylacetyl chloride
2902-98-9

2-chloro-2,2-diphenylacetyl chloride

benzilic acid-(3-dimethylamino-1-phenyl-propyl ester)
801171-59-5

benzilic acid-(3-dimethylamino-1-phenyl-propyl ester)

Conditions
ConditionsYield
With diethyl ether Erhitzen des Reaktionsprodukts mit Wasser;
N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

benzoic acid-(3-dimethylamino-1-phenyl-propyl ester)
25314-81-2

benzoic acid-(3-dimethylamino-1-phenyl-propyl ester)

Conditions
ConditionsYield
With benzoyl chloride In 1,4-dioxane at 25 - 50℃; Kinetics;
N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

benzoyl chloride
98-88-4

benzoyl chloride

benzoic acid-(3-dimethylamino-1-phenyl-propyl ester)
25314-81-2

benzoic acid-(3-dimethylamino-1-phenyl-propyl ester)

Conditions
ConditionsYield
In benzene
N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

methyl iodide
74-88-4

methyl iodide

3-Hydroxy-3-phenylpropyltrimethylammoniumiodid
24221-52-1

3-Hydroxy-3-phenylpropyltrimethylammoniumiodid

Conditions
ConditionsYield
In ethanol for 0.666667h; Heating; Yield given;
N,N-dimethyl-3-hydroxy-3-phenylpropylamine
5554-64-3

N,N-dimethyl-3-hydroxy-3-phenylpropylamine

(R)-Mandelic Acid
611-71-2

(R)-Mandelic Acid

(R)-3-Dimethylamino-1-phenyl-propan-1-ol; compound with (R)-hydroxy-phenyl-acetic acid

(R)-3-Dimethylamino-1-phenyl-propan-1-ol; compound with (R)-hydroxy-phenyl-acetic acid

Conditions
ConditionsYield
In ethyl acetate 77 deg C, 1 h and -15 deg C, 1 h; Yield given;

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