Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:577-59-3
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inquiryThe company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:White or off-white Solid Storage:Sealed, dry, m
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Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. Near 20 years DayangChem has provided dif
Cas:577-59-3
Min.Order:1 Gram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:577-59-3
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:577-59-3
Min.Order:1 Kilogram
FOB Price: $100.0 / 150.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:577-59-3
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Type:Trading Company
inquiry1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W
Cas:577-59-3
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inquiryProduct name: 2'-Nitroacetophenone CAS No.: 577-59-3 Molecular formula C8H7NO3 Appearance: Colorless to light yellow solid or liquid Assay: ≥98
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:577-59-3
Min.Order:1 Kilogram
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:577-59-3
Min.Order:1 Kilogram
FOB Price: $89.0 / 100.0
Type:Trading Company
inquiry2-Nitroacetophenone CAS:577-59-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
Cas:577-59-3
Min.Order:1 Gram
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:577-59-3
Min.Order:10 Kilogram
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:577-59-3
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:577-59-3
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and als
Cas:577-59-3
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:577-59-3
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiry2-Nitroacetophenone CAS No.577-59-3 MF: C8H7NO3 Appearance: colorless to light yellow solid or liquid Density: 1.23g/cm3 MP: 28-30℃ Assay:98% … ISO9001 Appearance:Colorless to yellowish solid or liquid Storage:Store in dry and
We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:577-59-3
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:yellow-green liquid or crystals Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:as per your request Application:Used as Pharmaceutical Intermed
Tianfu Chemical, built in 2009, is a professional supplier for API materials in China. With 10 years development, we have bulit our own factory and lab to produce a certain of products. And we have established stable business relationship
Cas:577-59-3
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry2-Nitroacetophenone Chemical Properties Melting point 76-78 °C(lit.) Boiling point 202 °C(lit.) density 1.23 refractive index n20/D 1.55(lit.) Fp >230 °F storage temp. Refrigerator Water Solubility Insoluble
Cas:577-59-3
Min.Order:1 Gram
FOB Price: $66.0
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:577-59-3
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:577-59-3
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryProductName:2-Nitroacetophenone CAS:577-59-3 Synonyms:1-(2-nitrophenyl)ethanone;1-(2-nitrophenyl)ethan-1-one;2-nitrophenylacetoaldehyde;2`-Nitroacetophenone;O-NITROACETOPHENONE;2-acetylnitrobenzene; 2'-METHYLBIPHENYL-2-CARBOXYLICACID;Etha
Cas:577-59-3
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
C11H17NO3Si
2-acetylnitrobenzene
Conditions | Yield |
---|---|
With nitrogen dioxide at 20℃; for 1h; | 100% |
Conditions | Yield |
---|---|
With calcium silicate; sulfuric acid; nitric acid at -15℃; | 97% |
With sulfuric acid; nitric acid at -15℃; | 80% |
With nitric acid | |
Multi-step reaction with 3 steps 1: pyridine / methanol / Reflux 2: silver(I) nitrite; dipotassium peroxodisulfate; palladium diacetate / 1,2-dichloro-ethane / 48 h / 130 °C / sealed tube 3: hydrogenchloride; water / diethyl ether / 24 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
With potassium permanganate; sulfuric acid; acetic acid In water at 30 - 50℃; for 8h; Temperature; Reagent/catalyst; Cooling; Large scale; | 96% |
With nickel-doped graphene carbon nitride nanoparticles; air In ethanol at 25℃; for 8h; Irradiation; Green chemistry; | 93% |
With oxygen In water for 4h; Reflux; | 87% |
1-(2-nitrophenyl)ethan-1-ol
2-acetylnitrobenzene
Conditions | Yield |
---|---|
With 2,2,6,6-tetramethyl-piperidine-N-oxyl; iron(III) chloride In water; ethyl acetate at 20℃; for 10h; | 96% |
With Montmorillonite K10; ferric nitrate In hexane at 60℃; for 7h; | 93% |
With caesium carbonate In toluene at 110℃; for 18h; | 83% |
2-ethynyl-1-nitrobenzene
2-acetylnitrobenzene
Conditions | Yield |
---|---|
With C22H20AuN3O2P(1+)*CF3O3S(1-); water; silver trifluoromethanesulfonate; acetic acid at 100℃; for 10h; | 94% |
With potassium tetrachloroaurate(III); (S)-2-(2-(1H-benzo[d][1,2,3]triazol-1-yl)acetamido)propanoic acid; water; silver trifluoromethanesulfonate; acetic acid Schlenk technique; Inert atmosphere; | 88% |
With methanol; [Co((dimethylglyoximate)BF2)2•2H2O] at 65℃; for 60h; Sealed tube; Neutral conditions; regioselective reaction; | 60% |
carbon monoxide
tetramethylstannane
2-nitrobenzenediazonium tetrafluoroborate
2-acetylnitrobenzene
Conditions | Yield |
---|---|
With palladium diacetate In acetonitrile for 0.5h; Ambient temperature; | 93% |
Conditions | Yield |
---|---|
With palladium diacetate; triethylamine; triphenylphosphine In dimethyl sulfoxide; N,N-dimethyl-formamide at 20 - 100℃; for 2h; Heck Reaction; Microwave irradiation; regioselective reaction; | 91% |
2-acetylnitrobenzene
Conditions | Yield |
---|---|
With hydrogenchloride; water for 0.0833333h; microwave irradiation; | 90% |
With hydrogenchloride for 4h; Heating; Yield given; |
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol at 20℃; | A 8% B 87% |
Conditions | Yield |
---|---|
With cobalt(II) stearate; sodium carbonate; sodium hydroxide at 140 - 165℃; under 6000.6 Torr; for 19.5h; pH=7 - 8.5; Pressure; Temperature; | 85.5% |
1-(2-nitro-phenyl)-ethanone oxime
2-acetylnitrobenzene
Conditions | Yield |
---|---|
With perchloric acid; dihydrogen peroxide; potassium bromide; ammonium molybdate tetrahydrate In water at 20℃; for 3h; | 85% |
With sulfuric acid |
(E)-1-(2-nitrophenyl)ethanone O-methyl oxime
2-acetylnitrobenzene
Conditions | Yield |
---|---|
With hydrogenchloride; water In dichloromethane at 100℃; for 24h; Sealed tube; | 85% |
With hydrogenchloride; water In diethyl ether at 20℃; for 24h; | 84% |
2-acetylnitrobenzene
Conditions | Yield |
---|---|
With sulfuric acid; acetic acid In water Reflux; | 80.5% |
Conditions | Yield |
---|---|
With trifluoromethylsulfonic anhydride; ethylammonium nitrate at 0 - 20℃; for 2h; Inert atmosphere; | A n/a B 77% |
With aluminium trinitrate; acetic anhydride; scandium tris(trifluoromethanesulfonate) In acetonitrile at 20℃; for 24h; | A 6% B 12% |
With Nitrogen dioxide; ozone In dichloromethane at -10℃; Mechanism; Product distribution; var. time; other ketones and benzaldehyde; |
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; water; palladium diacetate at 100℃; under 760.051 Torr; for 6h; | 74% |
Conditions | Yield |
---|---|
With water; oxygen; zinc(II) oxide In acetonitrile at 20℃; Irradiation; | 64% |
diazomethane
2-nitro-benzaldehyde
A
2-acetylnitrobenzene
B
(+/-)-2-(2-nitrophenyl)oxirane
Conditions | Yield |
---|---|
In diethyl ether 1.) 0 deg C 1 h: 2.) 3 h room temperature; | A 14% B 61% |
Z-2-<1-Hydroxy-1-(2-nitrophenyl)methylen>acetessigsaeureethylester
A
2-acetylnitrobenzene
B
4-hydroxy-4-(2-nitrophenyl)but-3-en-2-one
Conditions | Yield |
---|---|
With sulfuric acid In water for 5h; Heating; | A 61% B 25% |
2-nitro-benzaldehyde
diazomethyl-trimethyl-silane
A
2-acetylnitrobenzene
B
(+/-)-2-(2-nitrophenyl)oxirane
Conditions | Yield |
---|---|
With triethylamine In methanol; diethyl ether for 26h; Ambient temperature; | A 8% B 52% C 14% |
2-acetylnitrobenzene
Conditions | Yield |
---|---|
With water In 1,4-dioxane at 110℃; for 2h; Inert atmosphere; Microwave irradiation; | 52% |
Conditions | Yield |
---|---|
With water; oxygen; zinc(II) oxide In acetonitrile at 20℃; Irradiation; | 49% |
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In chloroform for 2h; Reflux; | 43% |
Conditions | Yield |
---|---|
With diethyl ether at -10℃; |
Conditions | Yield |
---|---|
With sodium acetate; copper(II) sulfate; sodium sulfite in wss. Loesung und anschl. mit wss. HCl; |
Conditions | Yield |
---|---|
Erhitzen mit Luft; |
ethyl (2-nitrobenzoyl)acetate
2-acetylnitrobenzene
Conditions | Yield |
---|---|
With sulfuric acid; water |
2-Nitrobenzoylessigsaeure
2-acetylnitrobenzene
Conditions | Yield |
---|---|
durch Vakuumdestillation; |
2-Nitrobenzoylessigsaeure
A
2-acetylnitrobenzene
B
methylammonium carbonate
Conditions | Yield |
---|---|
bei der Destillation im Vakuum; |
diethyl 2-(2-nitro-benzoyl)malonate
2-acetylnitrobenzene
Conditions | Yield |
---|---|
With sulfuric acid; acetic acid |
2-acetylnitrobenzene
1-(2-nitrophenyl)ethan-1-ol
Conditions | Yield |
---|---|
With methanol; sodium tetrahydroborate In 1,4-dioxane at 20℃; for 0.5h; | 100% |
With C40H37ClN2PRuS(1+)*C24H20B(1-); isopropyl alcohol; potassium hydroxide at 82℃; for 2h; Catalytic behavior; | 100% |
With sodium tetrahydroborate In 1,4-dioxane; methanol at 0 - 20℃; for 1h; | 99% |
2-acetylnitrobenzene
N,N-dimethyl-formamide dimethyl acetal
3-(dimethylamino)-1-(2-nitrophenyl)prop-2-en-1-one
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 100 - 110℃; for 2h; | 100% |
In N,N-dimethyl-formamide at 100℃; for 0.833333h; | 95% |
In N,N-dimethyl-formamide at 100℃; for 2h; Inert atmosphere; | 90% |
2-acetylnitrobenzene
oxalic acid diethyl ester
4-(2-nitrophenyl)-2,4-dioxobutanoic acid ethyl ester
Conditions | Yield |
---|---|
With sodium ethanolate In tetrahydrofuran at 0℃; for 2h; | 99% |
Stage #1: oxalic acid diethyl ester With sodium methylate In diethyl ether at 20℃; Inert atmosphere; Stage #2: 2-acetylnitrobenzene In diethyl ether at 20℃; for 12h; | 86% |
With sodium ethanolate In tetrahydrofuran at 0℃; for 2h; Inert atmosphere; | 78% |
2-acetylnitrobenzene
(S)-1-(2-nitrophenyl)ethanol
Conditions | Yield |
---|---|
With D-glucose In aq. phosphate buffer at 25℃; for 24h; pH=7.0; stereoselective reaction; | 99% |
With Debaryomyces hansenii P1 at 30℃; for 48h; pH=5.5; Microbiological reaction; enantioselective reaction; | 87% |
With (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole In dichloromethane at -78℃; for 24h; Inert atmosphere; | 74% |
Conditions | Yield |
---|---|
With ammonium formate In 1,4-dioxane; water at 60℃; for 6h; Catalytic behavior; Temperature; Time; Reagent/catalyst; Sealed tube; Green chemistry; | 99% |
Stage #1: 2-acetylnitrobenzene; benzaldehyde In water at 60℃; for 0.0833333h; Stage #2: With borane-ammonia complex In water at 60℃; for 8h; Catalytic behavior; Temperature; Time; Reagent/catalyst; | 99% |
Conditions | Yield |
---|---|
With ammonium formate In 1,4-dioxane; water at 60℃; for 6h; Sealed tube; Green chemistry; | 99% |
Stage #1: 2-acetylnitrobenzene; 4-cyanobenzaldehyde In water at 60℃; for 0.0833333h; Stage #2: With borane-ammonia complex In water at 60℃; for 8h; | 97% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.0833333h; | 99% |
Conditions | Yield |
---|---|
With potassium hydroxide In isopropyl alcohol at 100℃; Microwave irradiation; | 98% |
With formic acid; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; triethylamine; potassium iodide In dimethyl sulfoxide at 100℃; for 20h; Inert atmosphere; chemoselective reaction; | 97% |
With 1-methylcyclohex-1-ene; palladium on activated charcoal In methanol at 80℃; for 0.166667h; microwave irradiation; | 95% |
2-acetylnitrobenzene
4-chlorobenzaldehyde
trans-3-(4-chlorophenyl)-1-(2-nitrophenyl)prop-2-en-1-one
Conditions | Yield |
---|---|
With acetic acid In ethanol Aldol Condensation; | 98% |
With sodium hydroxide In ethanol; water at 20℃; for 12h; | 98% |
With potassium hydroxide In methanol; water | 91% |
2-acetylnitrobenzene
4-methyl-benzaldehyde
(2E)-3-(4-methylphenyl)-1-(2-nitrophenyl)-2-propen-1-one
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 0℃; for 3h; Aldol condensation; Inert atmosphere; | 97% |
With acetic acid In ethanol Aldol Condensation; | 97% |
With sodium hydroxide In ethanol; water at 20℃; for 12h; | 97% |
With potassium hydroxide In methanol; water | 93% |
With magnesium oxide In o-xylene at 90℃; for 8h; Claisen-Schmidt Condensation; Inert atmosphere; | 80 %Chromat. |
Conditions | Yield |
---|---|
With C11H18N3O2(1+)*C2F3O2(1-) In neat (no solvent) at 20℃; for 2h; Mannich Aminomethylation; | 97% |
With graphene oxide In ethanol at 20℃; for 5h; Mannich Aminomethylation; Green chemistry; | 90% |
Conditions | Yield |
---|---|
With C34H36ClN3Pd; sodium t-butanolate In 1,4-dioxane at 100℃; for 4h; Reagent/catalyst; | 97% |
Conditions | Yield |
---|---|
With C48H64ClN3Pd; sodium t-butanolate In 1,4-dioxane at 100℃; for 4h; Reagent/catalyst; | 97% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 0℃; for 3h; | 96% |
With sodium methylate In ethanol for 3h; Ambient temperature; | 88% |
With sodium hydroxide; ethanol |
2-acetylnitrobenzene
benzaldehyde
(2E)-1-(2-nitrophenyl)-3-phenyl-2-propen-1-one
Conditions | Yield |
---|---|
With acetic acid In ethanol Aldol Condensation; | 96% |
With sodium hydroxide In ethanol at 0℃; for 3h; Aldol condensation; Inert atmosphere; | 95% |
Stage #1: 2-acetylnitrobenzene With potassium hydroxide In ethanol; water at 0 - 20℃; for 0.5h; Stage #2: benzaldehyde In ethanol; water at 20℃; for 3h; | 83% |
2-acetylnitrobenzene
2-phenyl-1H-indol-3-carboxaldehyde
(E)-1-(2-Nitro-phenyl)-3-(2-phenyl-1H-indol-3-yl)-propenone
Conditions | Yield |
---|---|
With piperidine In ethanol for 2h; Heating; | 96% |
2-acetylnitrobenzene
4-methyl-benzaldehyde
4-methyl-2-(4-methylphenyl)quinazoline
Conditions | Yield |
---|---|
With ammonium formate In 1,4-dioxane; water at 60℃; for 6h; Sealed tube; Green chemistry; | 96% |
Stage #1: 2-acetylnitrobenzene; 4-methyl-benzaldehyde In water at 60℃; for 0.0833333h; Stage #2: With borane-ammonia complex In water at 60℃; for 8h; | 95% |
2-acetylnitrobenzene
1-(2-aminophenyl)ethanol
Conditions | Yield |
---|---|
With sodium tetrahydroborate In ethanol; water at 45℃; for 2h; Green chemistry; | 95% |
With sodium tetrahydroborate; water at 0 - 20℃; for 5h; | 95% |
With sodium tetrahydroborate; pyrographite In tetrahydrofuran; water at 50 - 60℃; for 3h; | 90% |
Conditions | Yield |
---|---|
With 2-bromo-2-nitropropane; indium In methanol; water at 50℃; for 0.333333h; Reduction; cyclisation; | 95% |
With hydrogen In toluene at 30℃; under 6750.68 Torr; for 1h; Catalytic behavior; Reagent/catalyst; Autoclave; chemoselective reaction; | 94% |
With tin(II) chloride dihdyrate In methanol; ethyl acetate at 20℃; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With aluminium trichloride; bromine In diethyl ether | 95% |
With bromine; copper(ll) bromide In chloroform; ethyl acetate at 80℃; | 91.8% |
With aluminum (III) chloride; bromine In diethyl ether at 0 - 20℃; for 4h; Inert atmosphere; | 88% |
2-acetylnitrobenzene
hydrazone of 2-nitroacetophenone
Conditions | Yield |
---|---|
With hydrazine hydrate; acetic acid In ethanol; water for 3h; Heating; | 95% |
With hydrazine hydrate; acetic acid In ethanol at 80℃; for 1h; Reflux; | 95% |
With hydrazine hydrate; acetic acid In ethanol for 3h; Reflux; | 81% |
With hydrazine hydrate; acetic acid In ethanol for 4h; Reflux; | 49.3% |
With hydrazine hydrate In ethanol Reflux; |
2-acetylnitrobenzene
N,N-dimethyl-formamide dimethyl acetal
(E)-3-(N,N-dimethylamino)-1-(2-nitrophenyl)-2-propen-1-one
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 100℃; for 0.75h; Inert atmosphere; | 95% |
In toluene at 110℃; Inert atmosphere; | 95% |
In N,N-dimethyl-formamide at 100℃; for 8h; | 88% |
Conditions | Yield |
---|---|
With acetic acid In ethanol Aldol Condensation; | 95% |
With sodium hydroxide; ethanol | |
With sodium hydroxide In ethanol; water at 20℃; |
2-acetylnitrobenzene
N-methoxylamine hydrochloride
o-nitroacetophenone O-methyl oxime
Conditions | Yield |
---|---|
In pyridine; ethanol for 8h; Condensation; Heating; | 95% |
With pyridine In ethanol for 3h; Molecular sieve; Heating / reflux; | 87% |
With pyridine In ethanol at 60℃; for 6h; |
Conditions | Yield |
---|---|
With silica gel-supported sulfuric acid In methanol at 20℃; for 0.833333h; | 95% |
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol at 0℃; for 3h; Aldol condensation; Inert atmosphere; | 95% |
With sodium hydroxide In ethanol; water at 20℃; for 12h; | 91% |
With potassium hydroxide In ethanol; water at 0 - 25℃; Claisen-Schmidt Condensation; Inert atmosphere; | 83% |
With sodium hydroxide In ethanol; water at 20℃; | 75% |
With sodium hydroxide In ethanol; water at 20℃; |
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