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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 2,--Nitroacetophenone supplier in China

Cas:577-59-3

Min.Order:0 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Henan Allgreen Chemical Co.,Ltd

The company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:White or off-white Solid Storage:Sealed, dry, m

2'-Nitroacetophenone, 97%

Cas:577-59-3

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

2-Nitroacetophenone

Cas:577-59-3

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem’s R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. Near 20 years DayangChem has provided dif

High purity 2-Nitroacetophenone 98% TOP1 supplier in China

Cas:577-59-3

Min.Order:1 Gram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

2'-Nitroacetophenone

Cas:577-59-3

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

o-Nitroacetophenone

Cas:577-59-3

Min.Order:1 Kilogram

FOB Price: $100.0 / 150.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Top Purity CAS 577-59-3 with fast shipping

Cas:577-59-3

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

2-Nitroacetophenone CAS577-59-3

Cas:577-59-3

Min.Order:1 Kilogram

FOB Price: $7.0 / 9.0

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

Product name: 2'-Nitroacetophenone CAS No.: 577-59-3 Molecular formula C8H7NO3 Appearance: Colorless to light yellow solid or liquid Assay: ≥98

2'-Nitroacetophenone

Cas:577-59-3

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

2-Nitroacetophenone 577-59-3

Cas:577-59-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

2-Nitroacetophenone 99%

Cas:577-59-3

Min.Order:1 Kilogram

FOB Price: $89.0 / 100.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

2-Nitroacetophenone CAS:577-59-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme

2-Nitroacetophenone CAS:577-59-3

Cas:577-59-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Hot Sell Factory Supply Raw Material CAS 577-59-3 2'-Nitroacetophne

Cas:577-59-3

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

2-Nitroacetophenone

Cas:577-59-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

2'-Nitroacetophenone

Cas:577-59-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

2'-Nitroacetophne

Cas:577-59-3

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

2-Nitroacetophenone

Cas:577-59-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply o-Nitroacetophenone

Cas:577-59-3

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and als

2-Nitroacetophenone

Cas:577-59-3

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

2-Nitroacetophenone CAS NO.577-59-3

Cas:577-59-3

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Kemi-Works Chemical Co., Ltd

2-Nitroacetophenone CAS No.577-59-3 MF: C8H7NO3 Appearance: colorless to light yellow solid or liquid Density: 1.23g/cm3 MP: 28-30℃ Assay:98% … ISO9001 Appearance:Colorless to yellowish solid or liquid Storage:Store in dry and

2-Nitroacetophenone

Cas:577-59-3

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

2'-Nitroacetophne

Cas:577-59-3

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:yellow-green liquid or crystals Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:as per your request Application:Used as Pharmaceutical Intermed

2-Nitroacetophenone

Cas:577-59-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

Tianfu Chemical, built in 2009, is a professional supplier for API materials in China. With 10 years development, we have bulit our own factory and lab to produce a certain of products. And we have established stable business relationship

577-59-3 2-Nitroacetophenone

Cas:577-59-3

Min.Order:1 Kilogram

FOB Price: $200.0

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

2-Nitroacetophenone Chemical Properties Melting point 76-78 °C(lit.) Boiling point 202 °C(lit.) density 1.23 refractive index n20/D 1.55(lit.) Fp >230 °F storage temp. Refrigerator Water Solubility Insoluble

2'-Nitroacetophenone

Cas:577-59-3

Min.Order:1 Gram

FOB Price: $66.0

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

2-Nitroacetophenone

Cas:577-59-3

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

2-Nitroacetophenone

Cas:577-59-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

2-Nitroacetophenone

Cas:577-59-3

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Hangzhou ZeErRui Chemical Co., Ltd.

ProductName:2-Nitroacetophenone CAS:577-59-3 Synonyms:1-(2-nitrophenyl)ethanone;1-(2-nitrophenyl)ethan-1-one;2-nitrophenylacetoaldehyde;2`-Nitroacetophenone;O-NITROACETOPHENONE;2-acetylnitrobenzene; 2'-METHYLBIPHENYL-2-CARBOXYLICACID;Etha

2-Nitroacetophenone

Cas:577-59-3

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Zhongqi chem Co.,Ltd.

Located in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an

2-Nitroacetophenone

Cas:577-59-3

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Synthetic route

C11H17NO3Si
1352706-75-2

C11H17NO3Si

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With nitrogen dioxide at 20℃; for 1h;100%
acetophenone
98-86-2

acetophenone

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With calcium silicate; sulfuric acid; nitric acid at -15℃;97%
With sulfuric acid; nitric acid at -15℃;80%
With nitric acid
Multi-step reaction with 3 steps
1: pyridine / methanol / Reflux
2: silver(I) nitrite; dipotassium peroxodisulfate; palladium diacetate / 1,2-dichloro-ethane / 48 h / 130 °C / sealed tube
3: hydrogenchloride; water / diethyl ether / 24 h / 20 °C
View Scheme
2-nitro(ethylbenzene)
612-22-6

2-nitro(ethylbenzene)

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With potassium permanganate; sulfuric acid; acetic acid In water at 30 - 50℃; for 8h; Temperature; Reagent/catalyst; Cooling; Large scale;96%
With nickel-doped graphene carbon nitride nanoparticles; air In ethanol at 25℃; for 8h; Irradiation; Green chemistry;93%
With oxygen In water for 4h; Reflux;87%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With 2,2,6,6-tetramethyl-piperidine-N-oxyl; iron(III) chloride In water; ethyl acetate at 20℃; for 10h;96%
With Montmorillonite K10; ferric nitrate In hexane at 60℃; for 7h;93%
With caesium carbonate In toluene at 110℃; for 18h;83%
2-ethynyl-1-nitrobenzene
16433-96-8

2-ethynyl-1-nitrobenzene

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With C22H20AuN3O2P(1+)*CF3O3S(1-); water; silver trifluoromethanesulfonate; acetic acid at 100℃; for 10h;94%
With potassium tetrachloroaurate(III); (S)-2-(2-(1H-benzo[d][1,2,3]triazol-1-yl)acetamido)propanoic acid; water; silver trifluoromethanesulfonate; acetic acid Schlenk technique; Inert atmosphere;88%
With methanol; [Co((dimethylglyoximate)BF2)2•2H2O] at 65℃; for 60h; Sealed tube; Neutral conditions; regioselective reaction;60%
carbon monoxide
201230-82-2

carbon monoxide

tetramethylstannane
594-27-4

tetramethylstannane

2-nitrobenzenediazonium tetrafluoroborate
365-33-3

2-nitrobenzenediazonium tetrafluoroborate

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With palladium diacetate In acetonitrile for 0.5h; Ambient temperature;93%
trimethylsiloxyethene
6213-94-1

trimethylsiloxyethene

o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With palladium diacetate; triethylamine; triphenylphosphine In dimethyl sulfoxide; N,N-dimethyl-formamide at 20 - 100℃; for 2h; Heck Reaction; Microwave irradiation; regioselective reaction;91%
2,2-Dimethyl-5-(2-nitro-benzoyl)-[1,3]dioxane-4,6-dione

2,2-Dimethyl-5-(2-nitro-benzoyl)-[1,3]dioxane-4,6-dione

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With hydrogenchloride; water for 0.0833333h; microwave irradiation;90%
With hydrogenchloride for 4h; Heating; Yield given;
2-Nitrobenzoylessigsaeure

2-Nitrobenzoylessigsaeure

A

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

B

2-Nitrobenzoylessigsaeureethylester

2-Nitrobenzoylessigsaeureethylester

Conditions
ConditionsYield
With hydrogenchloride In ethanol at 20℃;A 8%
B 87%
ethylbenzene
100-41-4

ethylbenzene

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With cobalt(II) stearate; sodium carbonate; sodium hydroxide at 140 - 165℃; under 6000.6 Torr; for 19.5h; pH=7 - 8.5; Pressure; Temperature;85.5%
1-(2-nitro-phenyl)-ethanone oxime
10342-62-8

1-(2-nitro-phenyl)-ethanone oxime

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With perchloric acid; dihydrogen peroxide; potassium bromide; ammonium molybdate tetrahydrate In water at 20℃; for 3h;85%
With sulfuric acid
(E)-1-(2-nitrophenyl)ethanone O-methyl oxime
1262802-04-9

(E)-1-(2-nitrophenyl)ethanone O-methyl oxime

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With hydrogenchloride; water In dichloromethane at 100℃; for 24h; Sealed tube;85%
With hydrogenchloride; water In diethyl ether at 20℃; for 24h;84%
C18H23NO7

C18H23NO7

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With sulfuric acid; acetic acid In water Reflux;80.5%
acetophenone
98-86-2

acetophenone

A

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

B

3-Nitroacetophenone
121-89-1

3-Nitroacetophenone

Conditions
ConditionsYield
With trifluoromethylsulfonic anhydride; ethylammonium nitrate at 0 - 20℃; for 2h; Inert atmosphere;A n/a
B 77%
With aluminium trinitrate; acetic anhydride; scandium tris(trifluoromethanesulfonate) In acetonitrile at 20℃; for 24h;A 6%
B 12%
With Nitrogen dioxide; ozone In dichloromethane at -10℃; Mechanism; Product distribution; var. time; other ketones and benzaldehyde;
2-nitrobenzenesulfonyl hydrazide
5906-99-0

2-nitrobenzenesulfonyl hydrazide

acetonitrile
75-05-8

acetonitrile

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With 1,10-Phenanthroline; water; palladium diacetate at 100℃; under 760.051 Torr; for 6h;74%
o-nitroiodobenzene
609-73-4

o-nitroiodobenzene

triethylamine
121-44-8

triethylamine

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With water; oxygen; zinc(II) oxide In acetonitrile at 20℃; Irradiation;64%
2-nitro-benzaldehyde
552-89-6

2-nitro-benzaldehyde

A

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

B

(+/-)-2-(2-nitrophenyl)oxirane
39830-70-1

(+/-)-2-(2-nitrophenyl)oxirane

Conditions
ConditionsYield
In diethyl ether 1.) 0 deg C 1 h: 2.) 3 h room temperature;A 14%
B 61%
Z-2-<1-Hydroxy-1-(2-nitrophenyl)methylen>acetessigsaeureethylester
104765-26-6

Z-2-<1-Hydroxy-1-(2-nitrophenyl)methylen>acetessigsaeureethylester

A

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

B

4-hydroxy-4-(2-nitrophenyl)but-3-en-2-one
60143-82-0

4-hydroxy-4-(2-nitrophenyl)but-3-en-2-one

Conditions
ConditionsYield
With sulfuric acid In water for 5h; Heating;A 61%
B 25%
2-nitro-benzaldehyde
552-89-6

2-nitro-benzaldehyde

diazomethyl-trimethyl-silane
18107-18-1

diazomethyl-trimethyl-silane

A

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

B

(+/-)-2-(2-nitrophenyl)oxirane
39830-70-1

(+/-)-2-(2-nitrophenyl)oxirane

Trimethyl-[(2R,3R)-3-(2-nitro-phenyl)-oxiranyl]-silane

Trimethyl-[(2R,3R)-3-(2-nitro-phenyl)-oxiranyl]-silane

Conditions
ConditionsYield
With triethylamine In methanol; diethyl ether for 26h; Ambient temperature;A 8%
B 52%
C 14%
C11H13NO2S2

C11H13NO2S2

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With water In 1,4-dioxane at 110℃; for 2h; Inert atmosphere; Microwave irradiation;52%
2-nitrophenyl bromide
577-19-5

2-nitrophenyl bromide

triethylamine
121-44-8

triethylamine

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With water; oxygen; zinc(II) oxide In acetonitrile at 20℃; Irradiation;49%
2-aminoacetophenone
551-93-9

2-aminoacetophenone

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With 3-chloro-benzenecarboperoxoic acid In chloroform for 2h; Reflux;43%
2-nitro-benzaldehyde
552-89-6

2-nitro-benzaldehyde

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With diethyl ether at -10℃;
Acetaldehyde oxime
107-29-9

Acetaldehyde oxime

2-Nitrophenyldiazonium
25910-37-6

2-Nitrophenyldiazonium

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With sodium acetate; copper(II) sulfate; sodium sulfite in wss. Loesung und anschl. mit wss. HCl;
o-nitrocumene
6526-72-3

o-nitrocumene

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
Erhitzen mit Luft;
ethyl (2-nitrobenzoyl)acetate
52119-39-8

ethyl (2-nitrobenzoyl)acetate

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With sulfuric acid; water
2-Nitrobenzoylessigsaeure
22751-16-2

2-Nitrobenzoylessigsaeure

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
durch Vakuumdestillation;
2-Nitrobenzoylessigsaeure
22751-16-2

2-Nitrobenzoylessigsaeure

A

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

B

methylammonium carbonate
15719-64-9, 15719-76-3, 97762-63-5

methylammonium carbonate

Conditions
ConditionsYield
bei der Destillation im Vakuum;
diethyl 2-(2-nitro-benzoyl)malonate
106718-56-3

diethyl 2-(2-nitro-benzoyl)malonate

2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With sulfuric acid; acetic acid
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With methanol; sodium tetrahydroborate In 1,4-dioxane at 20℃; for 0.5h;100%
With C40H37ClN2PRuS(1+)*C24H20B(1-); isopropyl alcohol; potassium hydroxide at 82℃; for 2h; Catalytic behavior;100%
With sodium tetrahydroborate In 1,4-dioxane; methanol at 0 - 20℃; for 1h;99%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

N,N-dimethyl-formamide dimethyl acetal
4637-24-5

N,N-dimethyl-formamide dimethyl acetal

3-(dimethylamino)-1-(2-nitrophenyl)prop-2-en-1-one
87488-61-7

3-(dimethylamino)-1-(2-nitrophenyl)prop-2-en-1-one

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 100 - 110℃; for 2h;100%
In N,N-dimethyl-formamide at 100℃; for 0.833333h;95%
In N,N-dimethyl-formamide at 100℃; for 2h; Inert atmosphere;90%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

oxalic acid diethyl ester
95-92-1

oxalic acid diethyl ester

4-(2-nitrophenyl)-2,4-dioxobutanoic acid ethyl ester
178114-28-8

4-(2-nitrophenyl)-2,4-dioxobutanoic acid ethyl ester

Conditions
ConditionsYield
With sodium ethanolate In tetrahydrofuran at 0℃; for 2h;99%
Stage #1: oxalic acid diethyl ester With sodium methylate In diethyl ether at 20℃; Inert atmosphere;
Stage #2: 2-acetylnitrobenzene In diethyl ether at 20℃; for 12h;
86%
With sodium ethanolate In tetrahydrofuran at 0℃; for 2h; Inert atmosphere;78%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

Conditions
ConditionsYield
With D-glucose In aq. phosphate buffer at 25℃; for 24h; pH=7.0; stereoselective reaction;99%
With Debaryomyces hansenii P1 at 30℃; for 48h; pH=5.5; Microbiological reaction; enantioselective reaction;87%
With (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole In dichloromethane at -78℃; for 24h; Inert atmosphere;74%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

benzaldehyde
100-52-7

benzaldehyde

4-methyl-2-phenylquinazoline
1806-66-2

4-methyl-2-phenylquinazoline

Conditions
ConditionsYield
With ammonium formate In 1,4-dioxane; water at 60℃; for 6h; Catalytic behavior; Temperature; Time; Reagent/catalyst; Sealed tube; Green chemistry;99%
Stage #1: 2-acetylnitrobenzene; benzaldehyde In water at 60℃; for 0.0833333h;
Stage #2: With borane-ammonia complex In water at 60℃; for 8h; Catalytic behavior; Temperature; Time; Reagent/catalyst;
99%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

4-cyanobenzaldehyde
105-07-7

4-cyanobenzaldehyde

4-(4-methylquinazolin-2-yl)benzonitrile

4-(4-methylquinazolin-2-yl)benzonitrile

Conditions
ConditionsYield
With ammonium formate In 1,4-dioxane; water at 60℃; for 6h; Sealed tube; Green chemistry;99%
Stage #1: 2-acetylnitrobenzene; 4-cyanobenzaldehyde In water at 60℃; for 0.0833333h;
Stage #2: With borane-ammonia complex In water at 60℃; for 8h;
97%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

diethyl cyanophosphonate
2942-58-7

diethyl cyanophosphonate

lithium cyanide
2408-36-8

lithium cyanide

1-cyano-1-(2-nitrophenyl)ethyl diethylphosphate

1-cyano-1-(2-nitrophenyl)ethyl diethylphosphate

Conditions
ConditionsYield
In tetrahydrofuran at 20℃; for 0.0833333h;99%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

2-aminoacetophenone
551-93-9

2-aminoacetophenone

Conditions
ConditionsYield
With potassium hydroxide In isopropyl alcohol at 100℃; Microwave irradiation;98%
With formic acid; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; triethylamine; potassium iodide In dimethyl sulfoxide at 100℃; for 20h; Inert atmosphere; chemoselective reaction;97%
With 1-methylcyclohex-1-ene; palladium on activated charcoal In methanol at 80℃; for 0.166667h; microwave irradiation;95%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

4-chlorobenzaldehyde
104-88-1

4-chlorobenzaldehyde

trans-3-(4-chlorophenyl)-1-(2-nitrophenyl)prop-2-en-1-one
69511-65-5

trans-3-(4-chlorophenyl)-1-(2-nitrophenyl)prop-2-en-1-one

Conditions
ConditionsYield
With acetic acid In ethanol Aldol Condensation;98%
With sodium hydroxide In ethanol; water at 20℃; for 12h;98%
With potassium hydroxide In methanol; water91%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

4-methyl-benzaldehyde
104-87-0

4-methyl-benzaldehyde

(2E)-3-(4-methylphenyl)-1-(2-nitrophenyl)-2-propen-1-one
244610-62-6

(2E)-3-(4-methylphenyl)-1-(2-nitrophenyl)-2-propen-1-one

Conditions
ConditionsYield
With sodium hydroxide In ethanol at 0℃; for 3h; Aldol condensation; Inert atmosphere;97%
With acetic acid In ethanol Aldol Condensation;97%
With sodium hydroxide In ethanol; water at 20℃; for 12h;97%
With potassium hydroxide In methanol; water93%
With magnesium oxide In o-xylene at 90℃; for 8h; Claisen-Schmidt Condensation; Inert atmosphere;80 %Chromat.
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

benzaldehyde
100-52-7

benzaldehyde

aniline
62-53-3

aniline

1-(2-nitrophenyl)-3-phenyl-3-(phenylamino)propan-1-one

1-(2-nitrophenyl)-3-phenyl-3-(phenylamino)propan-1-one

Conditions
ConditionsYield
With C11H18N3O2(1+)*C2F3O2(1-) In neat (no solvent) at 20℃; for 2h; Mannich Aminomethylation;97%
With graphene oxide In ethanol at 20℃; for 5h; Mannich Aminomethylation; Green chemistry;90%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

2-Chloroanisole
766-51-8

2-Chloroanisole

C15H13NO4

C15H13NO4

Conditions
ConditionsYield
With C34H36ClN3Pd; sodium t-butanolate In 1,4-dioxane at 100℃; for 4h; Reagent/catalyst;97%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

1-chloro-3-methoxy-benzene
2845-89-8

1-chloro-3-methoxy-benzene

C15H13NO4

C15H13NO4

Conditions
ConditionsYield
With C48H64ClN3Pd; sodium t-butanolate In 1,4-dioxane at 100℃; for 4h; Reagent/catalyst;97%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

benzaldehyde
100-52-7

benzaldehyde

2'-nitro-chalcone
16619-38-8

2'-nitro-chalcone

Conditions
ConditionsYield
With sodium hydroxide In ethanol at 0℃; for 3h;96%
With sodium methylate In ethanol for 3h; Ambient temperature;88%
With sodium hydroxide; ethanol
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

benzaldehyde
100-52-7

benzaldehyde

(2E)-1-(2-nitrophenyl)-3-phenyl-2-propen-1-one
53744-32-4

(2E)-1-(2-nitrophenyl)-3-phenyl-2-propen-1-one

Conditions
ConditionsYield
With acetic acid In ethanol Aldol Condensation;96%
With sodium hydroxide In ethanol at 0℃; for 3h; Aldol condensation; Inert atmosphere;95%
Stage #1: 2-acetylnitrobenzene With potassium hydroxide In ethanol; water at 0 - 20℃; for 0.5h;
Stage #2: benzaldehyde In ethanol; water at 20℃; for 3h;
83%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

2-phenyl-1H-indol-3-carboxaldehyde
25365-71-3

2-phenyl-1H-indol-3-carboxaldehyde

(E)-1-(2-Nitro-phenyl)-3-(2-phenyl-1H-indol-3-yl)-propenone
151390-85-1

(E)-1-(2-Nitro-phenyl)-3-(2-phenyl-1H-indol-3-yl)-propenone

Conditions
ConditionsYield
With piperidine In ethanol for 2h; Heating;96%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

4-methyl-benzaldehyde
104-87-0

4-methyl-benzaldehyde

4-methyl-2-(4-methylphenyl)quinazoline
1400697-35-9

4-methyl-2-(4-methylphenyl)quinazoline

Conditions
ConditionsYield
With ammonium formate In 1,4-dioxane; water at 60℃; for 6h; Sealed tube; Green chemistry;96%
Stage #1: 2-acetylnitrobenzene; 4-methyl-benzaldehyde In water at 60℃; for 0.0833333h;
Stage #2: With borane-ammonia complex In water at 60℃; for 8h;
95%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

1-(2-aminophenyl)ethanol
941706-81-6

1-(2-aminophenyl)ethanol

Conditions
ConditionsYield
With sodium tetrahydroborate In ethanol; water at 45℃; for 2h; Green chemistry;95%
With sodium tetrahydroborate; water at 0 - 20℃; for 5h;95%
With sodium tetrahydroborate; pyrographite In tetrahydrofuran; water at 50 - 60℃; for 3h;90%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

3-methylbenzo[c]isoxazole
4127-53-1

3-methylbenzo[c]isoxazole

Conditions
ConditionsYield
With 2-bromo-2-nitropropane; indium In methanol; water at 50℃; for 0.333333h; Reduction; cyclisation;95%
With hydrogen In toluene at 30℃; under 6750.68 Torr; for 1h; Catalytic behavior; Reagent/catalyst; Autoclave; chemoselective reaction;94%
With tin(II) chloride dihdyrate In methanol; ethyl acetate at 20℃; Inert atmosphere;93%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

2-bromo-1-(2-nitrophenyl)ethanone
6851-99-6

2-bromo-1-(2-nitrophenyl)ethanone

Conditions
ConditionsYield
With aluminium trichloride; bromine In diethyl ether95%
With bromine; copper(ll) bromide In chloroform; ethyl acetate at 80℃;91.8%
With aluminum (III) chloride; bromine In diethyl ether at 0 - 20℃; for 4h; Inert atmosphere;88%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

hydrazone of 2-nitroacetophenone
116271-34-2

hydrazone of 2-nitroacetophenone

Conditions
ConditionsYield
With hydrazine hydrate; acetic acid In ethanol; water for 3h; Heating;95%
With hydrazine hydrate; acetic acid In ethanol at 80℃; for 1h; Reflux;95%
With hydrazine hydrate; acetic acid In ethanol for 3h; Reflux;81%
With hydrazine hydrate; acetic acid In ethanol for 4h; Reflux;49.3%
With hydrazine hydrate In ethanol Reflux;
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

N,N-dimethyl-formamide dimethyl acetal
4637-24-5

N,N-dimethyl-formamide dimethyl acetal

(E)-3-(N,N-dimethylamino)-1-(2-nitrophenyl)-2-propen-1-one
153813-81-1

(E)-3-(N,N-dimethylamino)-1-(2-nitrophenyl)-2-propen-1-one

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 100℃; for 0.75h; Inert atmosphere;95%
In toluene at 110℃; Inert atmosphere;95%
In N,N-dimethyl-formamide at 100℃; for 8h;88%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

4-bromo-benzaldehyde
1122-91-4

4-bromo-benzaldehyde

(E)-1-(2-nitrophenyl)-3-(4-bromophenyl)-2-propen-1-one

(E)-1-(2-nitrophenyl)-3-(4-bromophenyl)-2-propen-1-one

Conditions
ConditionsYield
With acetic acid In ethanol Aldol Condensation;95%
With sodium hydroxide; ethanol
With sodium hydroxide In ethanol; water at 20℃;
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

N-methoxylamine hydrochloride
593-56-6

N-methoxylamine hydrochloride

o-nitroacetophenone O-methyl oxime
288591-69-5

o-nitroacetophenone O-methyl oxime

Conditions
ConditionsYield
In pyridine; ethanol for 8h; Condensation; Heating;95%
With pyridine In ethanol for 3h; Molecular sieve; Heating / reflux;87%
With pyridine In ethanol at 60℃; for 6h;
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

1,2-diamino-benzene
95-54-5

1,2-diamino-benzene

C22H18N4O4
1235974-13-6

C22H18N4O4

Conditions
ConditionsYield
With silica gel-supported sulfuric acid In methanol at 20℃; for 0.833333h;95%
2-acetylnitrobenzene
577-59-3

2-acetylnitrobenzene

3,4-dimethoxy-benzaldehyde
120-14-9

3,4-dimethoxy-benzaldehyde

(2E)-3-(3,4-dimethoxyphenyl)-1-(2-nitrophenyl)-2-propen-1-one

(2E)-3-(3,4-dimethoxyphenyl)-1-(2-nitrophenyl)-2-propen-1-one

Conditions
ConditionsYield
With sodium hydroxide In ethanol at 0℃; for 3h; Aldol condensation; Inert atmosphere;95%
With sodium hydroxide In ethanol; water at 20℃; for 12h;91%
With potassium hydroxide In ethanol; water at 0 - 25℃; Claisen-Schmidt Condensation; Inert atmosphere;83%
With sodium hydroxide In ethanol; water at 20℃;75%
With sodium hydroxide In ethanol; water at 20℃;
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