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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryHigh quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white to yellow powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as
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inquiry2-Furanmethanol,5-ethenyltetrahydro-a,a,5-trimethyl- cas 60047-17-8Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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Linalool oxide Basic information Product Name: Linalool oxide Synonyms: LINALYL OXIDE;FEMA 3746;FEMA 2635 OXIDE;ACETIC ACID LINALYL ESTER;5-ETHENYLTETRAHYDRO-ALPHA,ALPHA,5-TRIMETHYL-2-FURANMETHANOL;3,7-DI
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please contact us to confirm the required quantity and quote, we will provide you with COA,NMR,HPLC and other relevant information Storage:Store in a cool place. Keep container tightly closed in a dry and well-ventilated place Package:as your needs A
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inquiryHigh pure standard, Quick shippment COA with HPLC, MS and NMR spectra. Package:100mg Application:pharmaceutical industry, food industry, research
high purity Application:Drug intermediates Materials intermediates and active molecules
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inquiryLinalool oxide is a monoterpenoid compound, commonly found in some species of the aromatic plants. It can be obtained from linalool either by oxidation or via biotransfomation using the fungus Aspergillus niger. It is always present as a mixture of b
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inquiryLINALOOL OXIDE
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inquiryLINALOOL OXIDE
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inquirymore information,please contact us
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inquiry1-(5-ethynyl-5-methyl-2-tetrahydrofuranyl)-1-methylethanol
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
With quinoline; hydrogen; Pd-BaSO4 In methanol Ambient temperature; | 92% |
3,7-dimethylocta-1,6-dien-3-ol
A
6,7-epoxylinalool
B
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
With pyridine; pyridine-3-carbonitrile; dihydrogen peroxide; methyltrioxorhenium(VII) In dichloromethane; water at -0.15℃; for 1.7h; Yields of byproduct given; | A 82% B n/a |
5,6-epoxy-6-methyl-2-heptanone
vinyl magnesium bromide
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
In tetrahydrofuran for 12h; Ambient temperature; | 75% |
3,7-dimethylocta-1,6-dien-3-ol
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
With maleic anhydride; urea-hydrogen peroxide complex In dichloromethane at 0℃; for 5h; | 75% |
With 3-chloro-benzenecarboperoxoic acid In chloroform at 0℃; for 8h; | 72% |
With Beauveria sulfurescens ATCC7159 In various solvent(s) for 16h; |
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
With potassium tert-butylate; tert-butyl alcohol at 70 - 80℃; for 6h; | 72.91% |
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
With potassium tert-butylate In N,N-dimethyl-formamide at 25℃; | 70% |
(2E)-3-methyl-5-{(4R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl}-2-pentene-1-ol
trifluoromethylsulfonic anhydride
A
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
at -78℃; | A n/a B 43% |
trifluoromethylsulfonic anhydride
(4'S,2E)-3-methyl-5-(2',2',5',5'-tetramethyl-1',3'-dioxolan-4'-yl)-2-penten-1-ol
A
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
at -78℃; | A n/a B 43% |
peracetic acid
linalool
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
monoperoxyphthalic acid
linalool
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
With potassium tert-butylate; hydroxide 1) DMF, 25 deg C; Yield given. Multistep reaction; |
3,7-dimethylocta-1,6-dien-3-ol
A
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
B
3-hydroxy-2,2,6-trimethyl-6-vinyltetrahydropyran
Conditions | Yield |
---|---|
With cetylpyridinium peroxotungstophosphate; dihydrogen peroxide In chloroform; water for 1h; Ambient temperature; | A 48 % Chromat. B 22 % Chromat. |
With tert.-butylhydroperoxide; Ti-MCM-41 zeolite In acetonitrile at 79.9℃; for 24h; Product distribution; var. of catalyst, time; | A 37.8 % Turnov. B 42.3 % Turnov. |
With cetylpyridinium peroxotungstophosphate; dihydrogen peroxide In chloroform; water for 1h; Mechanism; Ambient temperature; | A 48 % Chromat. B 22 % Chromat. |
oct-1-ene
A
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
B
1,2-Epoxyoctane
Conditions | Yield |
---|---|
With cetylpyridinium peroxotungstophosphate; dihydrogen peroxide In chloroform; tert-butyl alcohol at 60℃; for 8h; | A 48 % Chromat. B 76 % Chromat. |
3,7-dimethylocta-1,6-dien-3-ol
A
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
B
3-hydroxy-2,2,6-trimethyl-6-vinyltetrahydropyran
C
Nerol
Conditions | Yield |
---|---|
With titanium silicate; dihydrogen peroxide In methanol; water at 59.84℃; for 24h; |
3,7-dimethylocta-1,6-dien-3-ol
A
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
B
Nerol
Conditions | Yield |
---|---|
With dihydrogen peroxide; aluminium In methanol; water at 59.84℃; for 31h; |
3,7-dimethyloct-6-en-1-yn-3-ol
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: NaBr / acetonitrile; H2O / 9 h / Ambient temperature; electrolysis 2: NaOH / acetonitrile; H2O / 1 h / Ambient temperature 3: 92 percent / H2(g), quinoline / 5percent Pd/BaSO4 / methanol / Ambient temperature View Scheme |
5-(3,3-Dimethyl-oxiranyl)-3-methyl-pent-1-yn-3-ol
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaOH / acetonitrile; H2O / 1 h / Ambient temperature 2: 92 percent / H2(g), quinoline / 5percent Pd/BaSO4 / methanol / Ambient temperature View Scheme |
2,3-Dihydroxy-2,6-dimethyl-octen-(6)
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: I2, NaHCO3 / acetonitrile / 0 °C 2: 70 percent / KO-t-Bu / dimethylformamide / 25 °C View Scheme |
Acetic acid (E)-2-benzyloxy-1,1,5-trimethyl-hept-5-enyl ester
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: I2 / acetonitrile / 0 °C 2: 1.) KO-t-Bu, 2.) OH(1-) / 1) DMF, 25 deg C View Scheme |
3,7-dimethylocta-1,6-dien-3-ol
A
6,7-epoxylinalool
B
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
C
3-hydroxy-2,2,6-trimethyl-6-vinyltetrahydropyran
Conditions | Yield |
---|---|
With [(n-C6H13)4N]3[PO4[WO(O2)2]4]; dihydrogen peroxide In water; acetonitrile at 80℃; for 5h; Catalytic behavior; |
3,7-dimethylocta-1,6-dien-3-ol
A
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
B
3-hydroxy-2,2,6-trimethyl-6-vinyltetrahydropyran
C
epoxy-linalooloxide
Conditions | Yield |
---|---|
With 4C19H34N(1+)*HBW4O24(4-); dihydrogen peroxide In water; acetonitrile at 80℃; for 5h; Catalytic behavior; | |
With 7C16H36N(1+)*3H(1+)*2H2O*(Co2PW9O34)2(10-); dihydrogen peroxide In water; acetonitrile at 80℃; for 5h; Catalytic behavior; Reagent/catalyst; Temperature; |
Essigsaeure-<(6S,2E)-6,7-dihydroxy-3,7-dimethyl-2-octen-1-yl>ester
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C 2: potassium carbonate / methanol / 24 h / 20 °C 3: -78 °C View Scheme | |
Multi-step reaction with 4 steps 1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C 2: potassium carbonate / methanol / 24 h / 20 °C 3: -78 °C 4: Irradiation View Scheme | |
Multi-step reaction with 4 steps 1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C 2: potassium carbonate / methanol / 24 h / 20 °C 3: phosphorus tribromide / diethyl ether / 0.33 h / -7 °C 4: Irradiation View Scheme |
Essigsaeure-<(6S,2E)-6,7-isopropylidendioxy-3,7-dimethyl-2-octen-1-yl>ester
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate / methanol / 24 h / 20 °C 2: -78 °C View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / methanol / 24 h / 20 °C 2: -78 °C 3: Irradiation View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / methanol / 24 h / 20 °C 2: phosphorus tribromide / diethyl ether / 0.33 h / -7 °C 3: Irradiation View Scheme |
(2E)-3-methyl-5-{(4R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl}-2-pentene-1-ol
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: phosphorus tribromide / diethyl ether / 0.33 h / -7 °C 2: Irradiation View Scheme | |
Multi-step reaction with 2 steps 1: -78 °C 2: Irradiation View Scheme |
(4'S,2E)-3-methyl-5-(2',2',5',5'-tetramethyl-1',3'-dioxolan-4'-yl)-2-penten-1-ol
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: phosphorus tribromide / diethyl ether / 0.33 h / -7 °C 2: Irradiation View Scheme | |
Multi-step reaction with 2 steps 1: -78 °C 2: Irradiation View Scheme |
(4'S,2E)-1-brom-3-methyl-5-(2',2',5',5'-tetramethyl-1',3'-dioxolan-4'-yl)-2-penten
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
Irradiation; |
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
Irradiation; |
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
Irradiation; |
essigsaeure-<(E,R)-6,7-dihydroxy-3,7-dimethyl-2-octenyl>ester
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C 2: potassium carbonate / methanol / 24 h / 20 °C 3: -78 °C View Scheme | |
Multi-step reaction with 4 steps 1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C 2: potassium carbonate / methanol / 24 h / 20 °C 3: -78 °C 4: Irradiation View Scheme | |
Multi-step reaction with 4 steps 1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C 2: potassium carbonate / methanol / 24 h / 20 °C 3: phosphorus tribromide / diethyl ether / 0.33 h / -7 °C 4: Irradiation View Scheme |
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
With triethylsilane; 1% Pd on activated carbon In water at 20℃; for 12h; Reagent/catalyst; Green chemistry; chemoselective reaction; | 99% |
With hydrogen; palladium 10% on activated carbon In methanol at 30℃; | 88% |
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
5-methyl-5-vinyl-dihydro-furan-2-one
Conditions | Yield |
---|---|
With 3 A molecular sieve; pyridinium chlorochromate In dichloromethane for 3h; Heating; | 73% |
With 3 A molecular sieve; pyridinium chlorochromate In dichloromethane for 4h; Heating; | 73% |
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
acetyl chloride
Conditions | Yield |
---|---|
With pyridine; dmap In dichloromethane at 0 - 20℃; Acetylation; | 53% |
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
ethyl vinyl ether
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In diethyl ether at 5 - 20℃; for 12.5h; | 37% |
monomethyl oxalyl chloride
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
With pyridine In diethyl ether at 22℃; for 16h; Inert atmosphere; | A 30% B 32% |
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
2,6-dimethyl-octa-4,6-dien-3-one
Conditions | Yield |
---|---|
With hydrogen cation |
carbon disulfide
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
With sodium hydride 1.) THF, RT, 1 h, 2.) THF, 20 min; Multistep reaction; |
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
A
2,2,5-trimethylcyclohept-4-en-1-one
B
(4E,6E)-2,6-Dimethyl-octa-4,6-dien-3-one
Conditions | Yield |
---|---|
With potassium hydrogensulfate at 200℃; for 0.5h; | A 0.7 % Chromat. B 41 % Chromat. |
carbon disulfide
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
xanthate of 1-(5-ethenyl-5-methyl-2-tetrahydrofuranyl)-1-methylethanol
Conditions | Yield |
---|---|
With sodium hydride 1.) THF; Multistep reaction; |
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
2,2,5-trimethylcyclohept-4-en-1-one
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, 20 min 2: tetrahydrofuran / 0.33 h 3: 200 °C View Scheme | |
Multi-step reaction with 4 steps 1: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, 20 min 2: tetrahydrofuran / 0.33 h 3: 200 °C 4: 44 percent / RhCl3*3H2O, Na2CO3 / 10 h / 200 °C View Scheme |
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
2-methyl-5-(prop-1-en-2-yl)-2-vinyltetrahydrofuran
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, 20 min 2: tetrahydrofuran / 0.33 h 3: 200 °C View Scheme |
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
xanthate of 1-(5-ethenyl-5-methyl-2-tetrahydrofuranyl)-1-methylethanol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, 20 min 2: tetrahydrofuran / 0.33 h View Scheme |
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