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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

2-Furanmethanol,5-ethenyltetrahydro-a,a,5-trimethyl-

Cas:60047-17-8

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2-(tetrahydro-5-methyl-5-vinyl-2-furyl)propan-2-ol

Cas:60047-17-8

Min.Order:1

Negotiable

Type:Other

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Natural Extract 98% Linalool oxide 60047-17-8 HACCP Manufacturer

Cas:60047-17-8

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Shanghai Seasonsgreen Chemical Co.,Ltd

Shanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu

lower price High quality Linalool oxide

Cas:60047-17-8

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Manufacturers

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

Linalool oxide

Cas:60047-17-8

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 60047-17-8 with best quality

Cas:60047-17-8

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

2-Furanmethanol,5-ethenyltetrahydro-a,a,5-trimethyl-

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung, LG, Merck, Thermo Fisher Scientific and so o

60047-17-8

Cas:60047-17-8

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

60047-17-8

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec 2-(2-Hydroxy-2-Propyl)-5-Methyl-5-Vinyltetrahydrofuran H90710 100mg

Cas:60047-17-8

Min.Order:1 bottle

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

Linalool oxide

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Linalool Oxide (Mixture of isoMers)

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

BOC Sciences

We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white to yellow powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as

2-(2-Hydroxy-2-propyl)-5-methyl-5-vinyltetrahydrofuran

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Fandachem Co.,Ltd

2-Furanmethanol,5-ethenyltetrahydro-a,a,5-trimethyl- cas 60047-17-8Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

2-Furanmethanol,5-ethenyltetrahydro-a,a,5-trimethyl- cas 60047-17-8

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Other

inquiry

Shanghai Yuanye Bio-Technology Co., Ltd.

good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:5ml Application:Pharma;Industry;Agricultural;chemical reaserch Transportation:by express or by sea Port:Any port

2-(2-Hydroxy-2-Propyl)-5-Methyl-5-Vinyltetrahydrofuran

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chemlyte Solutions

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

2-(2-Hydroxy-2-Propyl)-5-Methyl-5-Vinyltetrahydrofuran

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Other

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

Linalool oxide

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

HENAN SUNLAKE ENTERPRISE CORPORATION

Linalool oxide Basic information Product Name: Linalool oxide Synonyms: LINALYL OXIDE;FEMA 3746;FEMA 2635 OXIDE;ACETIC ACID LINALYL ESTER;5-ETHENYLTETRAHYDRO-ALPHA,ALPHA,5-TRIMETHYL-2-FURANMETHANOL;3,7-DI

Linalool oxide

Cas:60047-17-8

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right

Linalool oxide CAS NO.60047-17-8

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Nanjing Chemlin Chemical Co., Ltd.

please contact us to confirm the required quantity and quote, we will provide you with COA,NMR,HPLC and other relevant information Storage:Store in a cool place. Keep container tightly closed in a dry and well-ventilated place Package:as your needs A

2-Furanmethanol,5-ethenyltetrahydro-a,a,5-trimethyl-

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

SHANGHAI ZZBIO CO., LTD.

High pure standard, Quick shippment COA with HPLC, MS and NMR spectra. Package:100mg Application:pharmaceutical industry, food industry, research

Linalool oxide

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

NovaChemistry

high purity Application:Drug intermediates Materials intermediates and active molecules

2-(2-Hydroxy-2-Propyl)-5-Methyl-5-Vinyltetrahydrofuran

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Sigma-Aldrich Chemie GmbH

Linalool oxide is a monoterpenoid compound, commonly found in some species of the aromatic plants. It can be obtained from linalool either by oxidation or via biotransfomation using the fungus Aspergillus niger. It is always present as a mixture of b

Linalool oxide

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

PFALTZ-BAUER

more information,pls contact with us!

2-Furanmethanol,5-ethenyltetrahydro-a,a,5-trimethyl-

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

NATURAL ADVANTAGE

LINALOOL OXIDE

2-Furanmethanol,5-ethenyltetrahydro-a,a,5-trimethyl-

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Millennium Specialty Chemicals Inc.

LINALOOL OXIDE

2-Furanmethanol,5-ethenyltetrahydro-a,a,5-trimethyl-

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

J.H. Calo Company, Inc.

more information,please contact us

2-Furanmethanol,5-ethenyltetrahydro-a,a,5-trimethyl-

Cas:60047-17-8

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

1-(5-ethynyl-5-methyl-2-tetrahydrofuranyl)-1-methylethanol
97277-67-3

1-(5-ethynyl-5-methyl-2-tetrahydrofuranyl)-1-methylethanol

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
With quinoline; hydrogen; Pd-BaSO4 In methanol Ambient temperature;92%
3,7-dimethylocta-1,6-dien-3-ol
78-70-6

3,7-dimethylocta-1,6-dien-3-ol

A

6,7-epoxylinalool
15249-35-1

6,7-epoxylinalool

B

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
With pyridine; pyridine-3-carbonitrile; dihydrogen peroxide; methyltrioxorhenium(VII) In dichloromethane; water at -0.15℃; for 1.7h; Yields of byproduct given;A 82%
B n/a
5,6-epoxy-6-methyl-2-heptanone
16262-93-4

5,6-epoxy-6-methyl-2-heptanone

vinyl magnesium bromide
1826-67-1

vinyl magnesium bromide

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
In tetrahydrofuran for 12h; Ambient temperature;75%
3,7-dimethylocta-1,6-dien-3-ol
78-70-6

3,7-dimethylocta-1,6-dien-3-ol

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
With maleic anhydride; urea-hydrogen peroxide complex In dichloromethane at 0℃; for 5h;75%
With 3-chloro-benzenecarboperoxoic acid In chloroform at 0℃; for 8h;72%
With Beauveria sulfurescens ATCC7159 In various solvent(s) for 16h;
C17H26O5S

C17H26O5S

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
With potassium tert-butylate; tert-butyl alcohol at 70 - 80℃; for 6h;72.91%
2-[5-(1-Iodo-ethyl)-5-methyl-tetrahydro-furan-2-yl]-propan-2-ol

2-[5-(1-Iodo-ethyl)-5-methyl-tetrahydro-furan-2-yl]-propan-2-ol

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
With potassium tert-butylate In N,N-dimethyl-formamide at 25℃;70%
(2E)-3-methyl-5-{(4R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl}-2-pentene-1-ol
119906-63-7

(2E)-3-methyl-5-{(4R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl}-2-pentene-1-ol

trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

A

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

B

C14H23F3O5S

C14H23F3O5S

Conditions
ConditionsYield
at -78℃;A n/a
B 43%
trifluoromethylsulfonic anhydride
358-23-6

trifluoromethylsulfonic anhydride

(4'S,2E)-3-methyl-5-(2',2',5',5'-tetramethyl-1',3'-dioxolan-4'-yl)-2-penten-1-ol
61262-97-3

(4'S,2E)-3-methyl-5-(2',2',5',5'-tetramethyl-1',3'-dioxolan-4'-yl)-2-penten-1-ol

A

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

B

C14H23F3O5S

C14H23F3O5S

Conditions
ConditionsYield
at -78℃;A n/a
B 43%
peracetic acid
79-21-0

peracetic acid

linalool
126-91-0

linalool

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

monoperoxyphthalic acid
2311-91-3

monoperoxyphthalic acid

linalool
126-91-0

linalool

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Acetic acid 1-[5-(1-iodo-ethyl)-5-methyl-tetrahydro-furan-2-yl]-1-methyl-ethyl ester

Acetic acid 1-[5-(1-iodo-ethyl)-5-methyl-tetrahydro-furan-2-yl]-1-methyl-ethyl ester

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
With potassium tert-butylate; hydroxide 1) DMF, 25 deg C; Yield given. Multistep reaction;
3,7-dimethylocta-1,6-dien-3-ol
78-70-6

3,7-dimethylocta-1,6-dien-3-ol

A

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

B

3-hydroxy-2,2,6-trimethyl-6-vinyltetrahydropyran
14049-11-7

3-hydroxy-2,2,6-trimethyl-6-vinyltetrahydropyran

Conditions
ConditionsYield
With cetylpyridinium peroxotungstophosphate; dihydrogen peroxide In chloroform; water for 1h; Ambient temperature;A 48 % Chromat.
B 22 % Chromat.
With tert.-butylhydroperoxide; Ti-MCM-41 zeolite In acetonitrile at 79.9℃; for 24h; Product distribution; var. of catalyst, time;A 37.8 % Turnov.
B 42.3 % Turnov.
With cetylpyridinium peroxotungstophosphate; dihydrogen peroxide In chloroform; water for 1h; Mechanism; Ambient temperature;A 48 % Chromat.
B 22 % Chromat.
oct-1-ene
111-66-0

oct-1-ene

A

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

B

1,2-Epoxyoctane
2984-50-1

1,2-Epoxyoctane

Conditions
ConditionsYield
With cetylpyridinium peroxotungstophosphate; dihydrogen peroxide In chloroform; tert-butyl alcohol at 60℃; for 8h;A 48 % Chromat.
B 76 % Chromat.
3,7-dimethylocta-1,6-dien-3-ol
78-70-6

3,7-dimethylocta-1,6-dien-3-ol

A

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

B

3-hydroxy-2,2,6-trimethyl-6-vinyltetrahydropyran
14049-11-7

3-hydroxy-2,2,6-trimethyl-6-vinyltetrahydropyran

C

Nerol
106-25-2

Nerol

Conditions
ConditionsYield
With titanium silicate; dihydrogen peroxide In methanol; water at 59.84℃; for 24h;
3,7-dimethylocta-1,6-dien-3-ol
78-70-6

3,7-dimethylocta-1,6-dien-3-ol

A

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

B

Nerol
106-25-2

Nerol

Conditions
ConditionsYield
With dihydrogen peroxide; aluminium In methanol; water at 59.84℃; for 31h;
3,7-dimethyloct-6-en-1-yn-3-ol
29171-20-8

3,7-dimethyloct-6-en-1-yn-3-ol

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: NaBr / acetonitrile; H2O / 9 h / Ambient temperature; electrolysis
2: NaOH / acetonitrile; H2O / 1 h / Ambient temperature
3: 92 percent / H2(g), quinoline / 5percent Pd/BaSO4 / methanol / Ambient temperature
View Scheme
5-(3,3-Dimethyl-oxiranyl)-3-methyl-pent-1-yn-3-ol
74026-67-8

5-(3,3-Dimethyl-oxiranyl)-3-methyl-pent-1-yn-3-ol

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NaOH / acetonitrile; H2O / 1 h / Ambient temperature
2: 92 percent / H2(g), quinoline / 5percent Pd/BaSO4 / methanol / Ambient temperature
View Scheme
2,3-Dihydroxy-2,6-dimethyl-octen-(6)
78631-57-9

2,3-Dihydroxy-2,6-dimethyl-octen-(6)

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: I2, NaHCO3 / acetonitrile / 0 °C
2: 70 percent / KO-t-Bu / dimethylformamide / 25 °C
View Scheme
Acetic acid (E)-2-benzyloxy-1,1,5-trimethyl-hept-5-enyl ester
78631-58-0

Acetic acid (E)-2-benzyloxy-1,1,5-trimethyl-hept-5-enyl ester

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: I2 / acetonitrile / 0 °C
2: 1.) KO-t-Bu, 2.) OH(1-) / 1) DMF, 25 deg C
View Scheme
3,7-dimethylocta-1,6-dien-3-ol
78-70-6

3,7-dimethylocta-1,6-dien-3-ol

A

6,7-epoxylinalool
15249-35-1

6,7-epoxylinalool

B

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

C

3-hydroxy-2,2,6-trimethyl-6-vinyltetrahydropyran
14049-11-7

3-hydroxy-2,2,6-trimethyl-6-vinyltetrahydropyran

Conditions
ConditionsYield
With [(n-C6H13)4N]3[PO4[WO(O2)2]4]; dihydrogen peroxide In water; acetonitrile at 80℃; for 5h; Catalytic behavior;
3,7-dimethylocta-1,6-dien-3-ol
78-70-6

3,7-dimethylocta-1,6-dien-3-ol

A

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

B

3-hydroxy-2,2,6-trimethyl-6-vinyltetrahydropyran
14049-11-7

3-hydroxy-2,2,6-trimethyl-6-vinyltetrahydropyran

C

epoxy-linalooloxide
861071-75-2

epoxy-linalooloxide

Conditions
ConditionsYield
With 4C19H34N(1+)*HBW4O24(4-); dihydrogen peroxide In water; acetonitrile at 80℃; for 5h; Catalytic behavior;
With 7C16H36N(1+)*3H(1+)*2H2O*(Co2PW9O34)2(10-); dihydrogen peroxide In water; acetonitrile at 80℃; for 5h; Catalytic behavior; Reagent/catalyst; Temperature;
Essigsaeure-<(6S,2E)-6,7-dihydroxy-3,7-dimethyl-2-octen-1-yl>ester
61302-43-0

Essigsaeure-<(6S,2E)-6,7-dihydroxy-3,7-dimethyl-2-octen-1-yl>ester

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C
2: potassium carbonate / methanol / 24 h / 20 °C
3: -78 °C
View Scheme
Multi-step reaction with 4 steps
1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C
2: potassium carbonate / methanol / 24 h / 20 °C
3: -78 °C
4: Irradiation
View Scheme
Multi-step reaction with 4 steps
1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C
2: potassium carbonate / methanol / 24 h / 20 °C
3: phosphorus tribromide / diethyl ether / 0.33 h / -7 °C
4: Irradiation
View Scheme
Essigsaeure-<(6S,2E)-6,7-isopropylidendioxy-3,7-dimethyl-2-octen-1-yl>ester
61262-98-4

Essigsaeure-<(6S,2E)-6,7-isopropylidendioxy-3,7-dimethyl-2-octen-1-yl>ester

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium carbonate / methanol / 24 h / 20 °C
2: -78 °C
View Scheme
Multi-step reaction with 3 steps
1: potassium carbonate / methanol / 24 h / 20 °C
2: -78 °C
3: Irradiation
View Scheme
Multi-step reaction with 3 steps
1: potassium carbonate / methanol / 24 h / 20 °C
2: phosphorus tribromide / diethyl ether / 0.33 h / -7 °C
3: Irradiation
View Scheme
(2E)-3-methyl-5-{(4R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl}-2-pentene-1-ol
119906-63-7

(2E)-3-methyl-5-{(4R)-2,2,5,5-tetramethyl-[1,3]dioxolan-4-yl}-2-pentene-1-ol

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: phosphorus tribromide / diethyl ether / 0.33 h / -7 °C
2: Irradiation
View Scheme
Multi-step reaction with 2 steps
1: -78 °C
2: Irradiation
View Scheme
(4'S,2E)-3-methyl-5-(2',2',5',5'-tetramethyl-1',3'-dioxolan-4'-yl)-2-penten-1-ol
61262-97-3

(4'S,2E)-3-methyl-5-(2',2',5',5'-tetramethyl-1',3'-dioxolan-4'-yl)-2-penten-1-ol

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: phosphorus tribromide / diethyl ether / 0.33 h / -7 °C
2: Irradiation
View Scheme
Multi-step reaction with 2 steps
1: -78 °C
2: Irradiation
View Scheme
(4'S,2E)-1-brom-3-methyl-5-(2',2',5',5'-tetramethyl-1',3'-dioxolan-4'-yl)-2-penten
116660-94-7

(4'S,2E)-1-brom-3-methyl-5-(2',2',5',5'-tetramethyl-1',3'-dioxolan-4'-yl)-2-penten

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
Irradiation;
C14H23F3O5S

C14H23F3O5S

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
Irradiation;
C14H23F3O5S

C14H23F3O5S

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
Irradiation;
essigsaeure-<(E,R)-6,7-dihydroxy-3,7-dimethyl-2-octenyl>ester
86561-84-4

essigsaeure-<(E,R)-6,7-dihydroxy-3,7-dimethyl-2-octenyl>ester

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C
2: potassium carbonate / methanol / 24 h / 20 °C
3: -78 °C
View Scheme
Multi-step reaction with 4 steps
1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C
2: potassium carbonate / methanol / 24 h / 20 °C
3: -78 °C
4: Irradiation
View Scheme
Multi-step reaction with 4 steps
1: toluene-4-sulfonic acid / methanol / 3 h / 20 °C
2: potassium carbonate / methanol / 24 h / 20 °C
3: phosphorus tribromide / diethyl ether / 0.33 h / -7 °C
4: Irradiation
View Scheme
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

methyl-2 ethyl-2 (methyl-1 hydroxy-1 ethyl)-5 tetrahydrofuranne

methyl-2 ethyl-2 (methyl-1 hydroxy-1 ethyl)-5 tetrahydrofuranne

Conditions
ConditionsYield
With triethylsilane; 1% Pd on activated carbon In water at 20℃; for 12h; Reagent/catalyst; Green chemistry; chemoselective reaction;99%
With hydrogen; palladium 10% on activated carbon In methanol at 30℃;88%
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

5-methyl-5-vinyl-dihydro-furan-2-one
1073-11-6

5-methyl-5-vinyl-dihydro-furan-2-one

Conditions
ConditionsYield
With 3 A molecular sieve; pyridinium chlorochromate In dichloromethane for 3h; Heating;73%
With 3 A molecular sieve; pyridinium chlorochromate In dichloromethane for 4h; Heating;73%
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

acetyl chloride
75-36-5

acetyl chloride

acetic acid 1-methyl-1-(5-methyl-5-vinyl-tetrahydro-furan-2-yl)-ethyl ester

acetic acid 1-methyl-1-(5-methyl-5-vinyl-tetrahydro-furan-2-yl)-ethyl ester

Conditions
ConditionsYield
With pyridine; dmap In dichloromethane at 0 - 20℃; Acetylation;53%
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

ethyl vinyl ether
109-92-2

ethyl vinyl ether

5-(2-(1-ethoxyethoxy)propan-2-yl)-2-methyl-2-vinyltetrahydrofuran

5-(2-(1-ethoxyethoxy)propan-2-yl)-2-methyl-2-vinyltetrahydrofuran

Conditions
ConditionsYield
With toluene-4-sulfonic acid In diethyl ether at 5 - 20℃; for 12.5h;37%
monomethyl oxalyl chloride
5781-53-3

monomethyl oxalyl chloride

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

C13H20O5

C13H20O5

C13H20O5

C13H20O5

Conditions
ConditionsYield
With pyridine In diethyl ether at 22℃; for 16h; Inert atmosphere;A 30%
B 32%
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

2,6-dimethyl-octa-4,6-dien-3-one
91056-18-7

2,6-dimethyl-octa-4,6-dien-3-one

Conditions
ConditionsYield
With hydrogen cation
carbon disulfide
75-15-0

carbon disulfide

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

C11H17O2S2(1-)*Na(1+)

C11H17O2S2(1-)*Na(1+)

Conditions
ConditionsYield
With sodium hydride 1.) THF, RT, 1 h, 2.) THF, 20 min; Multistep reaction;
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

A

2,2,5-trimethylcyclohept-4-en-1-one
19822-67-4

2,2,5-trimethylcyclohept-4-en-1-one

B

(4E,6E)-2,6-Dimethyl-octa-4,6-dien-3-one
91056-18-7

(4E,6E)-2,6-Dimethyl-octa-4,6-dien-3-one

Conditions
ConditionsYield
With potassium hydrogensulfate at 200℃; for 0.5h;A 0.7 % Chromat.
B 41 % Chromat.
carbon disulfide
75-15-0

carbon disulfide

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

xanthate of 1-(5-ethenyl-5-methyl-2-tetrahydrofuranyl)-1-methylethanol
97277-68-4

xanthate of 1-(5-ethenyl-5-methyl-2-tetrahydrofuranyl)-1-methylethanol

Conditions
ConditionsYield
With sodium hydride 1.) THF; Multistep reaction;
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

2,2,5-trimethylcyclohept-4-en-1-one
19822-67-4

2,2,5-trimethylcyclohept-4-en-1-one

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, 20 min
2: tetrahydrofuran / 0.33 h
3: 200 °C
View Scheme
Multi-step reaction with 4 steps
1: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, 20 min
2: tetrahydrofuran / 0.33 h
3: 200 °C
4: 44 percent / RhCl3*3H2O, Na2CO3 / 10 h / 200 °C
View Scheme
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

2-methyl-5-(prop-1-en-2-yl)-2-vinyltetrahydrofuran
13679-86-2

2-methyl-5-(prop-1-en-2-yl)-2-vinyltetrahydrofuran

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, 20 min
2: tetrahydrofuran / 0.33 h
3: 200 °C
View Scheme
2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran
60047-17-8

2-methyl-5-(2'-propyl-2'-hydroxy)-2-vinyltetrahydrofuran

xanthate of 1-(5-ethenyl-5-methyl-2-tetrahydrofuranyl)-1-methylethanol
97277-68-4

xanthate of 1-(5-ethenyl-5-methyl-2-tetrahydrofuranyl)-1-methylethanol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) NaH / 1.) THF, RT, 1 h, 2.) THF, 20 min
2: tetrahydrofuran / 0.33 h
View Scheme

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