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Cas:6005-99-8
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryDayang Chem (Hangzhou) Co.,Ltd.
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine chemicals, ph
Shanghai Upbio Tech Co.,Ltd
1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:6005-99-8
Min.Order:1 Gram
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inquiryQingdao Beluga Import and Export Co., LTD
N-TRIDECANOPHENONE CAS:6005-99-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interm
Cas:6005-99-8
Min.Order:1 Gram
Negotiable
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inquiryShandong Hanjiang Chemical Co., Ltd.
Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:6005-99-8
Min.Order:1 Kilogram
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inquiryHenan Wentao Chemical Product Co., Ltd.
Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou J&H Chemical Co., Ltd.
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryGIHI CHEMICALS CO.,LIMITED
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Henan Allgreen Chemical Co.,Ltd
high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Henan Tianfu Chemical Co., Ltd.
1.Our services：A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.
Antimex Chemical Limied
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Henan Kanbei Chemical Co.,LTD
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Hebei Quanhe Biotechnology Co. LTD
1. Timely and efficient service to ensure communication with customers2. Produce products of different specifications and sizes according to your requirements.3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures sta
Shanghai Chinqesen Biotechnology Co., Ltd.
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ZHEJIANG JIUZHOU CHEM CO.,LTD
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Shanghai united Scientific Co.,Ltd.
United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat
Nanjing Raymon Biotech Co., Ltd.
1-Tridecanone,1-phenyl- Storage:keep in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/pharma intermediate Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen
Hebei Ruishun Trade Co.,Ltd
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Chemical Co.Ltd
Manufacturer,strong R&D,professional team Storage:Store in a cool, dry place. Store in a tightly closed container. Package:according to your requirement Application:ZhiShang Chemical is owned by ZhiShang Group, is a professional new-type chemicals en
Synthetic route
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| With iron(III) trifluoromethanesulfonate; trifluorormethanesulfonic acid In tetrahydrofuran at 100℃; for 12h; Schlenk technique; Inert atmosphere; | 98% |
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| With iron(III) trifluoromethanesulfonate; trifluorormethanesulfonic acid In tetrahydrofuran at 100℃; for 12h; Reagent/catalyst; Schlenk technique; Inert atmosphere; | 96% |
-
-
22986-80-7
2-hydroxy-2-phenyltetradecanoic acid
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| With (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)); oxygen; pivalaldehyde In acetonitrile for 2h; Ambient temperature; | 95% |
| With (NMe4)Co(III)Me2opba*2H2O*CH3CN; oxygen; pivalaldehyde In acetonitrile for 2h; | 95% |
| With oxygen; pivalaldehyde; Co(III) ortho-phenylene-bis(N'-methyloxamidate) In acetonitrile at 20℃; | 95% |
| Conditions | Yield |
|---|---|
| Stage #1: 1-dodecene; 3-phenyl-propenal With 3-methylpyridin-2-ylamine; Wilkinson's catalyst; 4-trifluoromethylbenzoic acid; cyclohexylamine In toluene at 130℃; for 12h; Stage #2: With hydrogenchloride; water In tetrahydrofuran | A 92% B 91% |
| Conditions | Yield |
|---|---|
| With dipotassium peroxodisulfate; methylene blue; potassium carbonate In water at 25℃; for 12h; Irradiation; Green chemistry; | 82% |
| Conditions | Yield |
|---|---|
| With Mg-Al hydrotalcite; chloro[N-[4-(dimethylamino)phenyl]-2-pyridinecarboxamidato](pentamethylcyclopentadienyl)iridium In 5,5-dimethyl-1,3-cyclohexadiene at 160℃; for 8h; Schlenk technique; | 80% |
| Conditions | Yield |
|---|---|
| With iron(III) trifluoromethanesulfonate; trifluorormethanesulfonic acid In tetrahydrofuran at 60 - 100℃; for 13h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Schlenk technique; Inert atmosphere; Sealed tube; | 78% |
| Conditions | Yield |
|---|---|
| With tert.-butylnitrite; N-hydroxyphthalimide In acetonitrile at 80℃; for 24h; Schlenk technique; | 70% |
| Conditions | Yield |
|---|---|
| With manganese; ethylene dibromide In tetrahydrofuran Product distribution; 1.) 0 deg C to rt, 1 h; 2.) 0 deg C, 20 min; 3.) rt, 30 min; coupling of benzoyl chloride with organomanganese bromides; | 68% |
| With manganese; ethylene dibromide In tetrahydrofuran 1.) 0 deg C to rt, 1 h; 2.) 0 deg C, 20 min; 3.) rt, 30 min; | 68% |
-
-
1851-92-9, 132362-82-4
1-hydroxytridecylbenzene
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| With thio-xanthene-9-one In dimethyl sulfoxide for 18h; Irradiation; Green chemistry; chemoselective reaction; | 66% |
| at 30℃; for 48h; by Corynebacterium equi IFO 3730; | 91 % Chromat. |
-
-
112-41-4
1-dodecene
-
-
15174-47-7
α-methyl-trans-cinnamaldehyde
-
A
-
18787-66-1
pentadecan-3-one
-
B
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| Stage #1: 1-dodecene; α-methyl-trans-cinnamaldehyde With 3-methylpyridin-2-ylamine; Wilkinson's catalyst; 4-trifluoromethylbenzoic acid; cyclohexylamine In toluene at 130℃; for 12h; Stage #2: With hydrogenchloride; water In tetrahydrofuran | A 60% B 60% |
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| at 630℃; under 1.50012 Torr; | 43% |
| Conditions | Yield |
|---|---|
| With potassium phosphate In neat (no solvent) at 175℃; for 24h; Sealed tube; | 16% |
| Conditions | Yield |
|---|---|
| With aluminium trichloride | |
| With aluminum (III) chloride for 3h; Friedel Crafts acylation; Reflux; Cooling with ice; | |
| Friedel-Crafts Acylation; |
-
-
77815-56-6
Trimethyl-(1-phenyl-1-phenylsulfanyl-tridecyloxy)-silane
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| With aqueous acid Yield given; |
| Conditions | Yield |
|---|---|
| With dichloroaluminum hydride; triethyl borane 1) 1,2-dichloroethane, RT, 1 h, 2) -25 deg C, 2 h; Yield given. Multistep reaction; |
| Conditions | Yield |
|---|---|
| With copper; zinc; tetrakis(triphenylphosphine) palladium(0) 1.) benzene, DMF, RT, 1h, 60 C, 3-4h; 2.) benzene, RT; Yield given. Multistep reaction; |
-
-
611-71-2, 611-72-3, 17199-29-0, 90-64-2
MANDELIC ACID
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| Multi-step reaction with 4 steps 1.1: 65 percent / H2SO4 / toluene / 24 h / 20 °C 2.1: n-BuLi; iPr2NH / hexane; tetrahydrofuran / 0.5 h / -78 °C 2.2: 65 percent / HMPA / hexane; tetrahydrofuran / 4 h / -78 - 20 °C 3.1: 100 percent / KOH / ethanol / 2 h / 20 °C 4.1: 95 percent / pivalaldehyde; O2 / Co(III)-Me2opba / acetonitrile / 20 °C View Scheme |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1.1: n-BuLi; iPr2NH / hexane; tetrahydrofuran / 0.5 h / -78 °C 1.2: 65 percent / HMPA / hexane; tetrahydrofuran / 4 h / -78 - 20 °C 2.1: 100 percent / KOH / ethanol / 2 h / 20 °C 3.1: 95 percent / pivalaldehyde; O2 / Co(III)-Me2opba / acetonitrile / 20 °C View Scheme |
-
-
830341-88-3
5-dodecyl-2,2-dimethyl-5-phenyl-1,3-dioxolan-4-one
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: 100 percent / KOH / ethanol / 2 h / 20 °C 2: 95 percent / pivalaldehyde; O2 / Co(III)-Me2opba / acetonitrile / 20 °C View Scheme |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: LDA / tetrahydrofuran / -78 - 20 °C 2: KOH / ethanol / 20 °C 3: 95 percent / (NMe4)Co(III)Me2opba*2H2O*CH3CN; pivalaldehyde; O2 / acetonitrile / 2 h View Scheme |
-
-
334927-76-3
methyl 2-hydroxy-2-phenyltetradecanoate
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: KOH / ethanol / 20 °C 2: 95 percent / (NMe4)Co(III)Me2opba*2H2O*CH3CN; pivalaldehyde; O2 / acetonitrile / 2 h View Scheme | |
| Multi-step reaction with 2 steps 1: NaOH 2: 95 percent / O2, pivalaldehyde, (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)) / acetonitrile / 2 h / Ambient temperature View Scheme |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: LDA 2: NaOH 3: 95 percent / O2, pivalaldehyde, (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)) / acetonitrile / 2 h / Ambient temperature View Scheme |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: LDA 2: NaOH 3: 95 percent / O2, pivalaldehyde, (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)) / acetonitrile / 2 h / Ambient temperature View Scheme | |
| Multi-step reaction with 3 steps 1: LDA 2: NaOH 3: 95 percent / O2, pivalaldehyde, (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)) / acetonitrile / 2 h / Ambient temperature View Scheme |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: LDA 2: NaOH 3: 95 percent / O2, pivalaldehyde, (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)) / acetonitrile / 2 h / Ambient temperature View Scheme |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 5 steps 1: 1) n-butyllithium - N,N,N'N'-tetramethylethylenediamine / 1) THF, -78 deg C 2: n-butyllithium - N,N,N'N'-tetramethylethylenediamine complex / hexane, 0 deg C 3: m-chloroperbenzoic acid / CH2Cl2 4: benzene / Heating 5: aqueous acid View Scheme |
-
-
67274-35-5, 321038-62-4
trimethylsilane
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| Multi-step reaction with 4 steps 1: n-butyllithium - N,N,N'N'-tetramethylethylenediamine complex / hexane, 0 deg C 2: m-chloroperbenzoic acid / CH2Cl2 3: benzene / Heating 4: aqueous acid View Scheme |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 6 steps 1: 95 percent / ethanol 2: 1) n-butyllithium - N,N,N'N'-tetramethylethylenediamine / 1) THF, -78 deg C 3: n-butyllithium - N,N,N'N'-tetramethylethylenediamine complex / hexane, 0 deg C 4: m-chloroperbenzoic acid / CH2Cl2 5: benzene / Heating 6: aqueous acid View Scheme |
-
-
77815-49-7
1-phenyl-1-phenylthio-1-trimethylsilyltridecane
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: m-chloroperbenzoic acid / CH2Cl2 2: benzene / Heating 3: aqueous acid View Scheme |
-
-
6005-99-8
1-phenyltridecan-1-one
-
-
132362-82-4
(S)-1-phenyl-1-tridecanol
| Conditions | Yield |
|---|---|
| Stage #1: 1-phenyltridecan-1-one With dimethylsulfide borane complex; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole In tetrahydrofuran; toluene at 0 - 20℃; for 1.66667h; Inert atmosphere; Stage #2: With hydrogenchloride In tetrahydrofuran; water; toluene Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 96% |
-
-
1851-92-9, 132362-82-4
1-hydroxytridecylbenzene
| Conditions | Yield |
|---|---|
| With thio-xanthene-9-one In dimethyl sulfoxide for 18h; Irradiation; Green chemistry; chemoselective reaction; | 66% |
| at 30℃; for 48h; by Corynebacterium equi IFO 3730; | 91 % Chromat. |
-
-
6005-99-8
1-phenyltridecan-1-one
-
-
1851-92-9, 132362-82-4
1-hydroxytridecylbenzene
| Conditions | Yield |
|---|---|
| With lithium aluminium tetrahydride; diethyl ether | |
| With sodium tetrahydroborate In tetrahydrofuran; methanol at 0 - 5℃; |
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| With zinc |
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| With iron(III) trifluoromethanesulfonate; trifluorormethanesulfonic acid In tetrahydrofuran at 100℃; for 12h; Schlenk technique; Inert atmosphere; | 98% |
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| With iron(III) trifluoromethanesulfonate; trifluorormethanesulfonic acid In tetrahydrofuran at 100℃; for 12h; Reagent/catalyst; Schlenk technique; Inert atmosphere; | 96% |
-
-
22986-80-7
2-hydroxy-2-phenyltetradecanoic acid
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| With (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)); oxygen; pivalaldehyde In acetonitrile for 2h; Ambient temperature; | 95% |
| With (NMe4)Co(III)Me2opba*2H2O*CH3CN; oxygen; pivalaldehyde In acetonitrile for 2h; | 95% |
| With oxygen; pivalaldehyde; Co(III) ortho-phenylene-bis(N'-methyloxamidate) In acetonitrile at 20℃; | 95% |
-
-
112-41-4
1-dodecene
-
-
104-55-2
3-phenyl-propenal
-
A
-
2345-27-9
tetradecan-2-one
-
B
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| Stage #1: 1-dodecene; 3-phenyl-propenal With 3-methylpyridin-2-ylamine; Wilkinson's catalyst; 4-trifluoromethylbenzoic acid; cyclohexylamine In toluene at 130℃; for 12h; Stage #2: With hydrogenchloride; water In tetrahydrofuran | A 92% B 91% |
| Conditions | Yield |
|---|---|
| With dipotassium peroxodisulfate; methylene blue; potassium carbonate In water at 25℃; for 12h; Irradiation; Green chemistry; | 82% |
| Conditions | Yield |
|---|---|
| With Mg-Al hydrotalcite; chloro[N-[4-(dimethylamino)phenyl]-2-pyridinecarboxamidato](pentamethylcyclopentadienyl)iridium In 5,5-dimethyl-1,3-cyclohexadiene at 160℃; for 8h; Schlenk technique; | 80% |
| Conditions | Yield |
|---|---|
| With iron(III) trifluoromethanesulfonate; trifluorormethanesulfonic acid In tetrahydrofuran at 60 - 100℃; for 13h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Schlenk technique; Inert atmosphere; Sealed tube; | 78% |
| Conditions | Yield |
|---|---|
| With tert.-butylnitrite; N-hydroxyphthalimide In acetonitrile at 80℃; for 24h; Schlenk technique; | 70% |
| Conditions | Yield |
|---|---|
| With manganese; ethylene dibromide In tetrahydrofuran Product distribution; 1.) 0 deg C to rt, 1 h; 2.) 0 deg C, 20 min; 3.) rt, 30 min; coupling of benzoyl chloride with organomanganese bromides; | 68% |
| With manganese; ethylene dibromide In tetrahydrofuran 1.) 0 deg C to rt, 1 h; 2.) 0 deg C, 20 min; 3.) rt, 30 min; | 68% |
-
-
1851-92-9, 132362-82-4
1-hydroxytridecylbenzene
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| With thio-xanthene-9-one In dimethyl sulfoxide for 18h; Irradiation; Green chemistry; chemoselective reaction; | 66% |
| at 30℃; for 48h; by Corynebacterium equi IFO 3730; | 91 % Chromat. |
-
-
112-41-4
1-dodecene
-
-
15174-47-7
α-methyl-trans-cinnamaldehyde
-
A
-
18787-66-1
pentadecan-3-one
-
B
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| Stage #1: 1-dodecene; α-methyl-trans-cinnamaldehyde With 3-methylpyridin-2-ylamine; Wilkinson's catalyst; 4-trifluoromethylbenzoic acid; cyclohexylamine In toluene at 130℃; for 12h; Stage #2: With hydrogenchloride; water In tetrahydrofuran | A 60% B 60% |
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| at 630℃; under 1.50012 Torr; | 43% |
| Conditions | Yield |
|---|---|
| With potassium phosphate In neat (no solvent) at 175℃; for 24h; Sealed tube; | 16% |
| Conditions | Yield |
|---|---|
| With aluminium trichloride | |
| With aluminum (III) chloride for 3h; Friedel Crafts acylation; Reflux; Cooling with ice; | |
| Friedel-Crafts Acylation; |
-
-
77815-56-6
Trimethyl-(1-phenyl-1-phenylsulfanyl-tridecyloxy)-silane
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| With aqueous acid Yield given; |
| Conditions | Yield |
|---|---|
| With dichloroaluminum hydride; triethyl borane 1) 1,2-dichloroethane, RT, 1 h, 2) -25 deg C, 2 h; Yield given. Multistep reaction; |
| Conditions | Yield |
|---|---|
| With copper; zinc; tetrakis(triphenylphosphine) palladium(0) 1.) benzene, DMF, RT, 1h, 60 C, 3-4h; 2.) benzene, RT; Yield given. Multistep reaction; |
-
-
611-71-2, 611-72-3, 17199-29-0, 90-64-2
MANDELIC ACID
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| Multi-step reaction with 4 steps 1.1: 65 percent / H2SO4 / toluene / 24 h / 20 °C 2.1: n-BuLi; iPr2NH / hexane; tetrahydrofuran / 0.5 h / -78 °C 2.2: 65 percent / HMPA / hexane; tetrahydrofuran / 4 h / -78 - 20 °C 3.1: 100 percent / KOH / ethanol / 2 h / 20 °C 4.1: 95 percent / pivalaldehyde; O2 / Co(III)-Me2opba / acetonitrile / 20 °C View Scheme |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1.1: n-BuLi; iPr2NH / hexane; tetrahydrofuran / 0.5 h / -78 °C 1.2: 65 percent / HMPA / hexane; tetrahydrofuran / 4 h / -78 - 20 °C 2.1: 100 percent / KOH / ethanol / 2 h / 20 °C 3.1: 95 percent / pivalaldehyde; O2 / Co(III)-Me2opba / acetonitrile / 20 °C View Scheme |
-
-
830341-88-3
5-dodecyl-2,2-dimethyl-5-phenyl-1,3-dioxolan-4-one
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: 100 percent / KOH / ethanol / 2 h / 20 °C 2: 95 percent / pivalaldehyde; O2 / Co(III)-Me2opba / acetonitrile / 20 °C View Scheme |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: LDA / tetrahydrofuran / -78 - 20 °C 2: KOH / ethanol / 20 °C 3: 95 percent / (NMe4)Co(III)Me2opba*2H2O*CH3CN; pivalaldehyde; O2 / acetonitrile / 2 h View Scheme |
-
-
334927-76-3
methyl 2-hydroxy-2-phenyltetradecanoate
-
-
6005-99-8
1-phenyltridecan-1-one
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: KOH / ethanol / 20 °C 2: 95 percent / (NMe4)Co(III)Me2opba*2H2O*CH3CN; pivalaldehyde; O2 / acetonitrile / 2 h View Scheme | |
| Multi-step reaction with 2 steps 1: NaOH 2: 95 percent / O2, pivalaldehyde, (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)) / acetonitrile / 2 h / Ambient temperature View Scheme |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: LDA 2: NaOH 3: 95 percent / O2, pivalaldehyde, (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)) / acetonitrile / 2 h / Ambient temperature View Scheme |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: LDA 2: NaOH 3: 95 percent / O2, pivalaldehyde, (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)) / acetonitrile / 2 h / Ambient temperature View Scheme | |
| Multi-step reaction with 3 steps 1: LDA 2: NaOH 3: 95 percent / O2, pivalaldehyde, (NMe4)*2H2O*CH3CN (L = ortho-phenylenebis(N'-methyloxamidate)) / acetonitrile / 2 h / Ambient temperature View Scheme |
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