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Cas:112-53-8
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Dodecyl alcohol Basic information Product Name: Dodecyl alcohol Synonyms: RARECHEM AL BD 0157;TIMTEC-BB SBB008734;N-DODECYL ALCOHOL;1-Hydroxydodecane;Alfol 12;alfol
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inquiryName: 1-Dodecanol CAS: 112-53-8 Appearance: Colorless Clear liquid Application: Used in the manufacture of high-efficiency detergents, surfactants, foaming agents, hair creams, lotions, textile oils, fungicides, cosmetics, plas
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inquiryProduct Name: 1-Dodecanol CAS: 112-53-8 MF: C12H26O MW: 186.33 EINECS: 203-982-0 Mol File: 112-53-8.mol 1-Dodecanol Structure 1-Dodecanol Chemical Properties Melting point 22-26 °C(lit.) Boiling point 260-262 °C(li
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2-(dodecyloxy)tetrahydro-2H-pyran
1-dodecyl alcohol
Conditions | Yield |
---|---|
With aniline-terephthalaldehyde resin p-toluenesulfonic acid salt In methanol at 20℃; for 3.5h; Reagent/catalyst; | 100% |
With tris-(4-bromophenyl)aminium hexachloroantimonate In methanol at 20℃; for 2h; | 99% |
bis(trimethylsilyl)sulphate In methanol; 1,2-dichloro-ethane for 1.5h; Ambient temperature; | 98% |
Dodecanol triethylsilyl ether
1-dodecyl alcohol
Conditions | Yield |
---|---|
With 7,7',8,8'-tetracyanoquinodimethane In water; acetonitrile for 5h; Ambient temperature; | 100% |
With MCM-41 In methanol for 2h; Ambient temperature; | 99% |
With mesoporous silica MCM-41 In methanol at 20℃; for 2h; | 99% |
tert-butyldimethylsilyl ether of dodecan-1-ol
1-dodecyl alcohol
Conditions | Yield |
---|---|
With polymer-supported dicyanoketene acetal; water In acetonitrile at 20℃; for 24h; Hydrolysis; | 100% |
With aniline-terephthalaldehyde resin p-toluenesulfonic acid salt In methanol at 20℃; for 1h; Reagent/catalyst; | 100% |
With high p-toluenesulfonate content diphenylamine and terephthalaldehyde resin In methanol at 20℃; for 1h; Reagent/catalyst; | 100% |
1-dodecanyl formate
1-dodecyl alcohol
Conditions | Yield |
---|---|
With hydrogenchloride In acetone at 20℃; for 0.25h; | 100% |
Conditions | Yield |
---|---|
With MCM-41 In methanol for 2h; Ambient temperature; | 100% |
With mesoporous silica MCM-41 In methanol at 20℃; for 2h; | 100% |
With polymer-supported dicyanoketene acetal; water In acetonitrile at 20℃; for 1h; Hydrolysis; | 98% |
Conditions | Yield |
---|---|
With hydrogen; copper-palladium; silica gel In ethanol at 25℃; under 760 Torr; Kinetics; | A n/a B 100% |
bis-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-thiocarbamic acid O-dodecyl ester
B
1-dodecyl alcohol
Conditions | Yield |
---|---|
With 3-chloro-benzenecarboperoxoic acid In dichloromethane at -78℃; for 1h; | A n/a B 100% |
1-dodecyl alcohol
Conditions | Yield |
---|---|
With (triphenylphosphine)gold(I) chloride; silver trifluoromethanesulfonate In ethanol; benzene at 20℃; for 1h; | 100% |
Conditions | Yield |
---|---|
With C32H36ClNO2P2Ru; potassium tert-butylate; hydrogen In neat (no solvent) at 120℃; under 38002.6 Torr; for 20h; Autoclave; Green chemistry; | 99% |
With hydrogen In hexane at 200℃; under 15001.5 Torr; for 8h; Reagent/catalyst; | 99.8% |
Stage #1: methyl n-dodecanoate With phenylsilane; fac-[Mn-(xantphos)(CO)3Br] at 120℃; for 12h; Inert atmosphere; Stage #2: With water; sodium hydroxide In methanol at 20℃; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With methanol; Na/SiO2 In tetrahydrofuran at 0 - 25℃; Bouveault-Blanc reduction; Inert atmosphere; | 99.5% |
With potassium borohydride; hafnium tetrachloride In tetrahydrofuran at 40℃; for 9.6h; Inert atmosphere; Cooling with ice; | 95% |
With ethandithiol; sodium tetrahydroborate In tetrahydrofuran for 24h; Heating; | 94% |
Conditions | Yield |
---|---|
With aluminium trichloride; diphenylstibane In tetrahydrofuran for 3h; Ambient temperature; | 99% |
Stage #1: Dodecanal With phenylsilane; potassium tert-butylate In toluene at 20℃; for 0.5h; Inert atmosphere; Stage #2: With water; sodium hydroxide In toluene at 0 - 20℃; | 99% |
With LaNi5 hydride In tetrahydrofuran; methanol 1) 0 deg C, 4 h, 2) r.t., 14 h; | 98% |
Conditions | Yield |
---|---|
With water; dichloro bis(acetonitrile) palladium(II) at 40℃; for 1h; | 99% |
With water; dichloro bis(acetonitrile) palladium(II) In tetrahydrofuran at 40℃; for 1h; | 98% |
dodecyl allyl carbonate
2-propanethiol
A
1-dodecyl alcohol
B
allylisopropyl sulfide
C
carbon dioxide
Conditions | Yield |
---|---|
With Roussin's red salt ester; tetrabutylammomium bromide; potassium hydride In tetrahydrofuran; ethanol at 40℃; | A 99% B n/a C n/a |
Conditions | Yield |
---|---|
Stage #1: 1-dodecene With PyBH2I In dichloromethane at 20℃; Stage #2: With sodium hydroxide; dihydrogen peroxide In methanol; dichloromethane at 0 - 20℃; | 98% |
Stage #1: 1-dodecene With sodium tetrahydroborate; ethyl iodide In 1,2-dimethoxyethane at 25℃; for 20h; Stage #2: With dihydrogen peroxide; sodium hydroxide In water at 0 - 25℃; for 0.333333h; Solvent; Reagent/catalyst; | 96% |
Stage #1: 1-dodecene With borane-THF In tetrahydrofuran; water at 0 - 20℃; for 7h; Inert atmosphere; Stage #2: With dihydrogen peroxide; sodium hydroxide In tetrahydrofuran; water at 0 - 20℃; for 6.5h; Inert atmosphere; | 95% |
Acetic acid dodecyloxymethyl ester
1-dodecyl alcohol
Conditions | Yield |
---|---|
With potassium carbonate In methanol; water | 98% |
1-dodecyl alcohol
Conditions | Yield |
---|---|
With tetra-N-butylammonium tribromide In methanol for 0.41h; | 98% |
N-Dodecyloxy-selenobenzimidic acid phenyl ester
1-dodecyl alcohol
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride In benzene for 2h; Heating; | 97% |
1-dodecyl alcohol
Conditions | Yield |
---|---|
With 2,5-bis(perfluorobutyl)-1,4-benzoquinone In water; acetonitrile at 50℃; for 6h; Reagent/catalyst; | 97% |
With low-loading and alkylated polystyrene-supported-SO3H In water at 100℃; for 12h; | 94% |
Conditions | Yield |
---|---|
With C24H38Cl2N3PRu; hydrogen; sodium methylate In isopropyl alcohol at 100℃; under 38002.6 Torr; for 2h; Autoclave; | 97% |
With 5 wt% Re/TiO2; hydrogen In neat (no solvent) at 230℃; under 37503.8 Torr; for 30h; Autoclave; | 81% |
Conditions | Yield |
---|---|
With potassium borohydride; hafnium tetrachloride In tetrahydrofuran at 40℃; for 15.3h; Inert atmosphere; Cooling with ice; | 96% |
With indium(III) bromide; 1,1,3,3-Tetramethyldisiloxane In chloroform at 60℃; for 1h; Inert atmosphere; | 95% |
With 1,1,3,3-Tetramethyldisiloxane; copper(II) bis(trifluoromethanesulfonate) In toluene at 80℃; for 16h; sealed tube; | 95% |
dodecyl methoxymethyl ether
1-dodecyl alcohol
Conditions | Yield |
---|---|
With low-loading and alkylated polystyrene-supported-SO3H In water at 100℃; for 24h; | 96% |
With dimethylboron bromide; triethylamine 1) CH2Cl2, 1,2-dichloroethane, -78 deg C, 1h, 2) RT, 1h; Yield given. Multistep reaction; |
1-dodecyl alcohol
Conditions | Yield |
---|---|
With low-loading and alkylated polystyrene-supported-SO3H In water at 100℃; for 24h; | 96% |
With acetyl chloride In methanol at 20℃; for 4h; | 95% |
With tetra-N-butylammonium tribromide In methanol; dichloromethane for 6h; Heating; | 94% |
With acetonyltriphenylphosphonium bromide In methanol; dichloromethane for 5h; | 88% |
With 2,5-bis(perfluorohexyl)-3,6-dichloro-1,4-benzoquinone In water; acetonitrile at 50℃; for 6h; | 84% |
dodecyl 4-methylbenzenesulphonate
1-dodecyl alcohol
Conditions | Yield |
---|---|
With tetraethylammonium perchlorate; triethylamine In dimethyl sulfoxide at 20℃; for 6h; Electrolysis; Green chemistry; | 96% |
1-Methylsulfanylmethoxy-dodecane
1-dodecyl alcohol
Conditions | Yield |
---|---|
With dimethylboron bromide In dichloromethane; 1,2-dichloro-ethane 1.) -78 deg C, 1 h 2.) warming up to 0 deg C, 1 h; | 95% |
With dimethylboron bromide; triethylamine 1) CH2Cl2, 1,2-dichloroethane, -78 deg C, 1h, 2) 0 deg C, 1h; Yield given. Multistep reaction; | |
Multi-step reaction with 2 steps 1: 1) Me2BBr, 2) Et3N / 1) CH2Cl2, 1,2-dichloroethane, -78 deg C, 1h, 2) RT, 1h 2: 1) Me2BBr, 2) Et3N / 1) CH2Cl2, 1,2-dichloroethane, -78 deg C, 1h, 2) RT, 1h View Scheme |
Conditions | Yield |
---|---|
In N,N,N,N,N,N-hexamethylphosphoric triamide; water at 100℃; for 2.5h; | 94% |
Conditions | Yield |
---|---|
In N,N,N,N,N,N-hexamethylphosphoric triamide; water at 100℃; for 5.5h; | 94% |
With oxygen; triethylamine; sodium iodide In acetonitrile at 32℃; for 24h; Schlenk technique; UV-irradiation; | 50% |
1-((dodecyloxy)methyl)-4-methoxybenzene
1-dodecyl alcohol
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate; sodium cyanoborohydride In tetrahydrofuran for 10h; Heating; | 94% |
With t-butyl bromide In acetonitrile for 1h; Solvent; Temperature; Reflux; chemoselective reaction; | 92% |
With N,N,N,N-tetraethylammonium tetrafluoroborate In methanol Electrochemical reaction; | 90% |
Conditions | Yield |
---|---|
With n-butyllithium; ammonia borane In tetrahydrofuran; hexane at 23℃; for 1.3h; | 94% |
((dodecyloxy)methyl)benzene
1-dodecyl alcohol
Conditions | Yield |
---|---|
With Ti-HMS; hydrogen; 5% Pd on active carbon In methanol under 760 Torr; for 6h; Ambient temperature; | 94% |
Stage #1: ((dodecyloxy)methyl)benzene With Bromotrichloromethane; (4,4'-di-tert-butyl-2,2'-dipyridyl)-bis-(2-phenylpyridine(-1H))-iridium(III) hexafluorophosphate In dichloromethane at 20℃; for 12h; Inert atmosphere; Irradiation; Stage #2: With methanol In dichloromethane Inert atmosphere; | 66% |
Conditions | Yield |
---|---|
toluene-4-sulfonic acid at 85℃; for 4h; Esterification; | 100% |
With 2-methyl-1-butylimidazolium trifluoroacetate In neat (no solvent) at 70℃; for 1h; | 96% |
Stage #1: formic acid With acetic anhydride at 40℃; for 2h; Stage #2: 1-dodecyl alcohol at 0 - 20℃; for 15.25h; | 94% |
With hydrogenchloride |
Conditions | Yield |
---|---|
With air; sodium nitrite In trifluoroacetic acid at 0 - 20℃; for 5h; | 100% |
With Iron(III) nitrate nonahydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium chloride; oxygen In 1,2-dichloro-ethane at 25℃; for 12h; | 100% |
With Iron(III) nitrate nonahydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; potassium chloride; oxygen In 1,2-dichloro-ethane at 20℃; for 12h; Reagent/catalyst; Schlenk technique; | 100% |
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical at 20℃; for 0.5h; electrolysis; | 100% |
Stage #1: 1-dodecyl alcohol With oxalyl dichloride; dimethyl sulfoxide In dichloromethane at -78℃; for 0.25h; Oxidation; Stage #2: With triethylamine at -78 - 20℃; for 0.166667h; | 100% |
With iodosylbenzene; Cl-CH2-PS supported 5-amino-1,10-phenanthroline-Ru In acetonitrile at 60℃; for 6h; | 100% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0℃; for 0.25h; | 100% |
With triethylamine In dichloromethane at 0℃; for 3h; Inert atmosphere; | 99% |
With triethylamine In dichloromethane at 0℃; for 12h; | 93% |
L-N-Boc-Ala
1-dodecyl alcohol
N-tert-butoxycarbonyl-L-alanine dodecyl ester
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; | 100% |
papain on XAD-7 In dichloromethane at 37℃; for 18h; | 55% |
1-dodecyl alcohol
3-tert-butoxycarbonyl-2-chloro-1,3,2-oxazaphospholidine
3-tert-butoxycarbonyl-2-dodecyloxy-1,3,2-oxazaphospholidine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane -60 deg C to r.t., 1 h; | 100% |
1-dodecyl alcohol
2-chloro-3-methyl-1,3,2-oxazaphospholidine
2-Dodecyloxy-3-methyl-1,3,2-oxazaphosphacyclopentane
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 1h; -30 - -40 deg C to RT; | 100% |
1-dodecyl alcohol
3-tert-2-chloro-1,3,2-oxazaphosphacyclopentane
3-tert-butyl-2-dodecyloxy-1,3,2-oxazaphosphacyclopentane
Conditions | Yield |
---|---|
With triethylamine In dichloromethane for 1h; -60 deg C to rt; | 100% |
Conditions | Yield |
---|---|
cerium (IV) sulfate; silica gel for 1h; Heating; | 100% |
1-dodecyl alcohol
bis(trichloromethyl) carbonate
n-dodecyl chloroformate
Conditions | Yield |
---|---|
With pyridine In tetrachloromethane at -15 - 20℃; | 100% |
With pyridine In tetrahydrofuran for 2h; | |
With pyridine In chloroform for 2h; ice cooling; |
Conditions | Yield |
---|---|
With 2,6-di-tert-butyl-4-methyl-phenol; toluene-4-sulfonic acid In toluene for 7h; Reflux; | 100% |
With toluene-4-sulfonic acid; 1-octyl-3-methylimidazolium tetrafluoroborate at 80℃; for 1h; | 98% |
With toluene-4-sulfonic acid In 5,5-dimethyl-1,3-cyclohexadiene | 95% |
1-dodecyl alcohol
perbenzyl fucosyl bromide
Conditions | Yield |
---|---|
With 4 A molecular sieve; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine for 4h; Substitution; | 100% |
1-dodecyl alcohol
(2S,3S,4R,5R,6S)-3,4,5-Tris-benzyloxy-2-iodo-6-methyl-tetrahydro-pyran
Conditions | Yield |
---|---|
With 4 A molecular sieve; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine for 4h; Substitution; | 100% |
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In pyridine at 0 - 20℃; for 48h; | 100% |
1-dodecyl alcohol
4-(4-bromophenyl)-4-oxo-butyric acid
dodecyl 4-(4-bromophenyl)-4-oxobutanoate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; | 100% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; | 99% |
1-dodecyl alcohol
N-t-butoxycarbonyl-N-methyl-β-alanine
Boc-MeβAla-O-n-dodecyl
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; | 100% |
1-dodecyl alcohol
1-hexadecylcarboxylic acid
dodecyl hexadecanoic acid ester
Conditions | Yield |
---|---|
With zirconium(IV) oxychloride In 1,3,5-trimethyl-benzene at 162℃; for 24h; | 100% |
With toluene-4-sulfonic acid In benzene for 30h; Reflux; | 100% |
iron(III) chloride In 1,3,5-trimethyl-benzene at 162℃; for 24h; | 99% |
C15H12ClF18NS
1-dodecyl alcohol
bis-(4,4,5,5,6,6,7,7,7-nonafluoro-heptyl)-thiocarbamic acid O-dodecyl ester
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 12h; | 100% |
C19H12ClF26NS
1-dodecyl alcohol
bis-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-thiocarbamic acid O-dodecyl ester
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran at 20℃; for 12h; | 100% |
1-dodecyl alcohol
3-(tert-butyldimethylsilyloxy)glutaric anhydride
3-(tert-butyldimethylsilyloxy)-5-oxo-5-(dodecyloxy)pentanoic acid
Conditions | Yield |
---|---|
In toluene Heating; | 100% |
In toluene for 24h; Reflux; | 95% |
1-dodecyl alcohol
Pyroglutamic acid
ethyl 2-oxopyrrolidine-5-carboxylate
2-pyrrolidone-5-carboxylic acid n-dodecyl ester
Conditions | Yield |
---|---|
Novozym 435 at 60℃; under 15.0015 Torr; for 24h; Enzymatic reaction; | 100% |
Conditions | Yield |
---|---|
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran at 20℃; Mitsunobu reaction; | 100% |
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