Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:619-24-9
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:619-24-9
Min.Order:1 Metric Ton
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Type:Manufacturers
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new ap
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:619-24-9
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryFactory price CAS 619-24-9 3-Nitrobenzonitrile in stock Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediates (Fluor
Cas:619-24-9
Min.Order:1 Gram
FOB Price: $2000.0
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:619-24-9
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:619-24-9
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquirym-Nitrobenzonitrile Molecular formula: C7H4N2O2 CAS NO.: 619-24-9 Appearance: light yellow crystalline powder Content: 99% min Appearance:light yellow crystalline powder Storage:Store in cool and
Appearance:Yellowish powder Storage:R.T Package:25kg/drum Application:pharmaceutical and pesticide intermediates Transportation:Express/Sea/Air Port:Any port in China
Cas:619-24-9
Min.Order:25 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:619-24-9
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:619-24-9
Min.Order:1 Kilogram
FOB Price: $76.0 / 85.0
Type:Trading Company
inquiry3-Nitrobenzonitrile CAS:619-24-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
Cas:619-24-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:619-24-9
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists
Cas:619-24-9
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. We have several production line,So we can control the lowest price. We also have several
Cas:619-24-9
Min.Order:25 Gram
FOB Price: $90.0 / 100.0
Type:Trading Company
inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s
Cas:619-24-9
Min.Order:1 Kilogram
FOB Price: $40.0 / 50.0
Type:Lab/Research institutions
inquiryHangzhou Fanda Chemical Co.,Ltd (FandaChem) , a China-based chemical company, specialize in exporting 3-Nitrobenzonitrile CAS:619-24-9, Please contact us by email freely. We are leading exporter in China. If you really need this cargo
Cas:619-24-9
Min.Order:0 Metric Ton
Negotiable
Type:Other
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:619-24-9
Min.Order:1 Gram
FOB Price: $58.0
Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:619-24-9
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:619-24-9
Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:619-24-9
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:YELLOWISH CRYSTALLINE POWDER OR NEEDLES Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:as per your request Application:Used as Pharmaceutical Inte
Established in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:619-24-9
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryProduct name: 3-Nitrobenzonitrile CAS No.:619-24-9 Molecule Formula:C7H4N2O2 Molecule Weight:148.12 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:619-24-9
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Name: 3-Nitrobenzonitrile CAS: 619-24-9 MF: C7H4N2O2 MW: 148.12 EINECS: 210-587-7 Mol File: 619-24-9.mol 3-Nitrobenzonitrile Structure 3-Nitrobenzonitrile Chemical Properties Melting point 114-117 °C(lit.) Boiling
Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
Conditions | Yield |
---|---|
With dmap; thionyl chloride In dichloromethane for 0.5h; Ambient temperature; | 100% |
With 2-chloro-1,3-dimethylimidazolinium chloride; triethylamine In dichloromethane at 20℃; for 24h; Dehydration; | 99% |
With chlorosulfonic acid In toluene at 90℃; for 0.5h; | 99% |
Conditions | Yield |
---|---|
With ammonia; iodine In water; acetonitrile at 20℃; for 0.666667h; | 99% |
With hydroxylamine hydrochloride In 1-methyl-pyrrolidin-2-one for 0.25h; Heating; | 98% |
With 1-methyl-pyrrolidin-2-one; hydroxylamine hydrochloride at 100℃; for 0.5h; Condensation; microwave irradiation; | 97% |
Conditions | Yield |
---|---|
Stage #1: 3-Nitrobenzyl alcohol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tert-butylhypochlorite In dichloromethane at 20℃; for 1h; Inert atmosphere; Stage #2: With ammonia; iodine In dichloromethane; water at 20℃; for 2h; Inert atmosphere; | 99% |
With ammonium hydroxide; iodine at 60℃; for 3h; | 92% |
With ammonium hydroxide; iodine at 60℃; for 3h; | 92% |
Conditions | Yield |
---|---|
With N-iodo-succinimide; 1,10-Phenanthroline; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; 1,1,1,2,2,2-hexamethyldisilane; oxygen; copper diacetate; diisopropylamine at 20 - 150℃; Schlenk technique; | 99% |
1,1-dimethyl-2-[(3-nitrophenyl)methylidene]hydrazine
3-nitrobenzonitrile
Conditions | Yield |
---|---|
With 3,3-dimethyldioxirane In acetone at 0℃; for 0.05h; | 97% |
Conditions | Yield |
---|---|
With aluminum oxide; methanesulfonyl chloride at 100℃; for 0.0666667h; | 97% |
Stage #1: E-3-nitrobenzaldoxime With 2-chloro-1-methyl-pyridinium iodide In dichloromethane at 20℃; for 0.166667h; Stage #2: With triethylamine In dichloromethane at 20℃; for 1h; | 91% |
With palladium diacetate; triphenylphosphine In acetonitrile for 3h; Reflux; | 81% |
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 3h; Schlenk technique; | 97% |
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 3h; Schlenk technique; | 97% |
With mesoporous silica SBA-15 supported Cu2O nanoparticles In N,N-dimethyl-formamide at 120℃; for 8h; Green chemistry; | 94% |
With CuO-supported Pd(0) nanoparticles In N,N-dimethyl-formamide at 120℃; for 13h; | 60% |
With 3% Pd/CeO2; sodium hydroxide In ethanol; N,N-dimethyl-formamide at 55℃; for 10h; Irradiation; | 40% |
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 4h; Green chemistry; | 97% |
Conditions | Yield |
---|---|
With thionyl chloride; N,N-dimethyl-formamide at 55 - 60℃; for 2h; | 96% |
With hydroxyammonium sulfate; zinc for 0.45h; Microwave irradiation; | 87% |
With aluminum oxide; aminosulfonic acid; urea for 0.1h; Irradiation; | 81% |
With ammonium hydroxide; thionyl chloride 2.) dioxane, 3.) reflux; Multistep reaction; |
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 3h; Schlenk technique; | 96% |
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 3h; Schlenk technique; | 96% |
With 3% Pd/ZrO2; sodium acetate In N,N-dimethyl-formamide; isopropyl alcohol at 55℃; for 12h; Irradiation; | 60% |
With 1-methyl-pyrrolidin-2-one; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; sodium carbonate at 120℃; for 12h; Schlenk technique; Inert atmosphere; |
3-Bromonitrobenzene
N-cyano-N-phenyl-p-toluenesulfonamide
3-nitrobenzonitrile
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; bis(1,5-cyclooctadiene)iridium(I) tetrafluoroborate; ammonium cerium (IV) nitrate; lanthanum(lll) triflate; XPhos at 100℃; for 8h; | 95.1% |
trimethylsilyl cyanide
m-nitrobenzene boronic acid
3-nitrobenzonitrile
Conditions | Yield |
---|---|
With copper(I) oxide; oxygen; N,N`-dimethylethylenediamine In acetonitrile at 25℃; for 12h; Schlenk technique; | 95% |
With potassium phosphate; copper(l) iodide In 1-methyl-pyrrolidin-2-one at 60℃; for 2h; | 67% |
3-nitrobenzonitrile
Conditions | Yield |
---|---|
With iron(III) chloride; 2,6-di-tert-butyl-4-methyl-phenol In toluene at 20℃; for 0.116667h; Schlenk technique; | 94% |
3,6,6-Trimethyl-4-{[1-(3-nitro-phenyl)-meth-(E)-ylidene]-amino}-4,6-dihydro-1H-cyclopenta[1,2,4]triazine-5,7-dicarboxylic acid dimethyl ester
A
3-nitro-benzaldehyde
B
3-nitrobenzonitrile
Conditions | Yield |
---|---|
With sodium methylate In ethanol for 3h; Product distribution; Heating; | A 4% B 93% |
3-nitrothiobenzamide
3-nitrobenzonitrile
Conditions | Yield |
---|---|
With triphenyl bismuth (2+); dichloride; triethylamine In dichloromethane at 20℃; for 0.25h; | 93% |
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 4h; Green chemistry; | 93% |
Conditions | Yield |
---|---|
With magnesium(II) perchlorate; 2-nitrobenzo[d]isothiazol-3(2H)-one 1,1-dioxide In [D3]acetonitrile at 85℃; for 5h; Inert atmosphere; Sealed tube; | 92% |
With tetrammine copper(II) sulphate; nitric acid In dichloromethane; water at 20℃; for 2.5h; regioselective reaction; | 84% |
With magnesium(II) nitrate hexahydrate; AMA at 20℃; for 24h; Neat (no solvent); | 82% |
Conditions | Yield |
---|---|
With [Ru(η6-C6Me6)Cl2(tris(dimethylamino)phosphine)]; hydroxylamine hydrochloride; sodium hydrogencarbonate In water at 100℃; for 7h; Reagent/catalyst; Inert atmosphere; Sealed tube; Green chemistry; | A n/a B 92% |
A
bis(3-cyanophenyl)diazene oxide
B
3-nitrobenzonitrile
Conditions | Yield |
---|---|
With selenium(IV) oxide; dihydrogen peroxide In methanol; water at 20℃; for 24h; | A 91% B 3% |
Conditions | Yield |
---|---|
With sodium carbonate In N,N-dimethyl-formamide at 120℃; for 12h; Inert atmosphere; Schlenk technique; | 90% |
With tris-(dibenzylideneacetone)dipalladium(0); tris(2-morpholinophenyl)phosphine; potassium carbonate In water; tert-butyl alcohol at 85℃; for 5h; Schlenk technique; Inert atmosphere; | 80% |
With palladium diacetate; sodium carbonate; 1,3-bis[(2,6-diisopropyl)phenyl]imidazolinium chloride In N,N-dimethyl acetamide at 120℃; for 11h; | 67% |
Conditions | Yield |
---|---|
at 350℃; under 48754.9 Torr; for 0.416667h; Supercritical conditions; Flow reactor; | 90% |
Conditions | Yield |
---|---|
With Aloe vera mediated silver nanoparticles In water at 50℃; for 0.75h; Green chemistry; | 90% |
Conditions | Yield |
---|---|
With diethyl chlorophosphate at 120℃; for 0.25h; Neat (no solvent); | 89% |
With di-morpholin-4-yl-phosphinic acid chloride; triethylamine In dichloromethane at 20℃; for 4h; | 72% |
With lead acetate In dichloromethane for 12h; Reflux; | 71% |
3-Methyl-4-{[1-(3-nitro-phenyl)-meth-(E)-ylidene]-amino}-4,6-dihydro-1H-cyclopenta[1,2,4]triazine-5,7-dicarboxylic acid diethyl ester
A
3-nitro-benzaldehyde
B
3-Methyl-4H-cyclopenta-1,2,4-triazin-5,7-dicarbonsaeure-diethylester
C
3-nitrobenzonitrile
Conditions | Yield |
---|---|
With ethanol Heating; | A 56% B 89% C 15% |
In ethanol Product distribution; Heating; | A 56% B 89% C 15% |
4-chlorophenyl thiocyanate
m-nitrobenzene boronic acid
3-nitrobenzonitrile
Conditions | Yield |
---|---|
With N,N,N-trimethyl-2-(sulfooxy)ethanaminium palladium(II) chloride; sodium carbonate In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; water for 2h; | 89% |
m-nitrobenzene boronic acid
2,3-dicyano-5,6-dichloro-p-benzoquinone
3-nitrobenzonitrile
Conditions | Yield |
---|---|
With silver (II) carbonate; copper(II) bis(trifluoromethanesulfonate); potassium carbonate In N,N-dimethyl-formamide at 100℃; for 20h; | 88% |
m-nitrobenzene boronic acid
ethyl (ethoxymethylene)cyanoacetate
3-nitrobenzonitrile
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; copper(l) iodide In N,N-dimethyl-formamide at 130℃; for 24h; | 88% |
3-iodobenzonitrile
3-nitrobenzonitrile
Conditions | Yield |
---|---|
With 1,10-Phenanthroline; iron(II) sulfate; potassium nitrate In dimethyl sulfoxide at 20℃; for 48h; UV-irradiation; Inert atmosphere; | 88% |
tetra-n-butylammonium cyanide
3-nitrobenzonitrile
Conditions | Yield |
---|---|
In acetonitrile at 22℃; for 0.75h; Sandmeyer Reaction; | 87% |
3-nitrobenzonitrile
5-(3-nitrophenyl)-1H-tetrazole
Conditions | Yield |
---|---|
With sodium azide; ammonium chloride In N,N-dimethyl-formamide at 120℃; for 4h; | 100% |
Stage #1: 3-nitrobenzonitrile With sodium azide In N,N-dimethyl-formamide at 120℃; for 36h; Stage #2: With hydrogenchloride In water; ethyl acetate for 0.0833333h; | 98% |
With aluminum (III) chloride; sodium azide In 1-methyl-pyrrolidin-2-one at 200℃; for 0.05h; Microwave irradiation; | 98% |
Conditions | Yield |
---|---|
With hydroxylamine In ethanol; water at 80℃; for 5h; | 100% |
With hydroxylamine hydrochloride; sodium carbonate In ethanol; water at 85℃; for 2h; Inert atmosphere; | 99% |
With hydroxylamine hydrochloride; triethylamine In methanol at 20℃; Reflux; | 93% |
3-nitrobenzonitrile
5-(3-nitrophenyl)-2H-tetrazole
Conditions | Yield |
---|---|
With aluminum (III) chloride; sodium azide In 1-methyl-pyrrolidin-2-one at 200℃; for 0.0833333h; Microwave irradiation; | 100% |
With sodium azide; ammonium chloride In N,N-dimethyl-formamide at 16℃; Reflux; | 97% |
With sodium azide; zinc dibromide In water for 51h; Reflux; | 94% |
Conditions | Yield |
---|---|
With indium; acetic acid In methanol at 20℃; for 1.5h; | 100% |
Conditions | Yield |
---|---|
With iron(III)-acetylacetonate; hydrazine hydrate In methanol at 150℃; Microwave irradiation; Green chemistry; | 99% |
With iron(III)-acetylacetonate; hydrazine hydrate In methanol at 150℃; for 0.0333333h; Microwave irradiation; chemoselective reaction; | 99% |
With maghemite; methylhydrazine In ethanol at 60℃; for 0.2h; Sealed tube; Inert atmosphere; chemoselective reaction; | 99% |
Conditions | Yield |
---|---|
With cobalt(II,III) oxide; water at 140℃; for 24h; | 99% |
With potassium tert-butylate In tert-butyl alcohol at 20℃; for 12h; Solvent; Temperature; Inert atmosphere; | 99% |
With manganese(IV) oxide; water In isopropyl alcohol at 100℃; under 5171.62 Torr; for 0.25h; | 98% |
Cysteamine
3-nitrobenzonitrile
2-(3-nitrophenyl)-4,5-dihydro-1,3-thiazole
Conditions | Yield |
---|---|
With trichloroisocyanuric acid In neat (no solvent) at 110℃; for 0.0333333h; chemoselective reaction; | 98% |
With 1-butyl-3-methylimidazolium tribromide at 100℃; for 0.1h; | 88% |
With tribromomelamine at 100℃; for 0.0833333h; Neat (no solvent); | 87% |
In ethanol for 5h; Heating; | 63% |
ethanol
3-nitrobenzonitrile
3-nitrobenzenecarboximidic acid ethyl ester monohydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol | 98% |
With hydrogenchloride In benzene Cooling with ice; | |
With hydrogenchloride In 1,4-dioxane |
3-nitrobenzonitrile
5-(3-hydroxyphenyl)-1H-tetrazole
Conditions | Yield |
---|---|
With sodium azide at 120℃; for 2.16667h; Suzuki Coupling; | 97% |
Conditions | Yield |
---|---|
With caesium carbonate In toluene at 150℃; for 24h; Inert atmosphere; Sealed tube; | 96% |
Conditions | Yield |
---|---|
With sodium sulfide In methanol for 8h; Reflux; | 95.3% |
With sodium monohydrogen sulfide x-hydrate at 110℃; for 48h; | 60% |
With sulfur In methanol at 67℃; for 24h; Large scale; |
3-nitrobenzonitrile
3-(hydroxyamino)benzonitrile
Conditions | Yield |
---|---|
With ammonium formate; zinc In acetonitrile at 25 - 30℃; for 1.66667h; sonification; | 95% |
With methyldiazene In acetonitrile at 28℃; for 1.66667h; Irradiation; Sealed tube; Inert atmosphere; | 93% |
With sulfuric acid In ethanol at 20℃; (electrochemical reduction); | |
With ammonium chloride; zinc at 60 - 80℃; | |
With ammonium chloride; zinc In ethanol |
3-nitrobenzonitrile
3-fluoro-5-nitrobenzonitrile
Conditions | Yield |
---|---|
With fluorine In acetonitrile at 0 - 10℃; | 95% |
With fluorine In acetonitrile at 90℃; under 1500.15 Torr; for 1h; Sealed tube; | 345 g |
3-nitrobenzonitrile
N-Cyan-(3-nitro-benzamidin)
Conditions | Yield |
---|---|
Stage #1: 3-nitrobenzonitrile With sodium methylate In methanol at 20℃; for 4h; Stage #2: With CYANAMID In methanol at 20℃; | 95% |
3-nitrobenzonitrile
3-nitrothiobenzamide
Conditions | Yield |
---|---|
With diammonium sulfide; 1,6-bis(3-methylimidazolium-1-yl)hexane dichloride at 70℃; for 0.1h; | 94% |
Stage #1: 3-nitrobenzonitrile With Lawessons reagent; boron trifluoride diethyl etherate In diethyl ether; toluene at 50℃; for 14h; Inert atmosphere; Stage #2: With sodium hydrogencarbonate In diethyl ether; toluene at 20℃; for 0.333333h; Inert atmosphere; | 88% |
With triethanolamine; hydrogen sulfide In ethanol |
Conditions | Yield |
---|---|
With zinc(II) chloride In chlorobenzene for 21h; Inert atmosphere; Reflux; | 94% |
(4S)-1-benzyl-4,5-dihydroxypyrrolidin-2-one
3-nitrobenzonitrile
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate at 20℃; Ritter Amidation; Inert atmosphere; diastereoselective reaction; | 94% |