As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiry622-26-4 4-Piperidineethanol Now we would like to update our product list for you, kindly check the below information: 1. Catalyst series ( such as Noble Metal Catalyst, Phosphorous ligand, etc ) 2. Pharmaceutical Intermediate
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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inquiry4-Piperidineethanol CAS:622-26-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryProduct name: 4-Piperidineethanol CAS No.:622-26-4 Molecule Formula:C7H15NO Molecule Weight:129.20 Purity: 99.0% Package: 25kg/drum Description:White powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:622-26-4
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
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4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl-amine
A
4-(2-Hydroxyethyl)piperidine
Conditions | Yield |
---|---|
A n/a B 64% |
4-piperidinylacetic acid
4-(2-Hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 25℃; Cooling with ice; Inert atmosphere; | 62.5% |
Conditions | Yield |
---|---|
With sodium; butan-1-ol und Hydrieren des vermutlich als 2-<1,2,3,6-Tetrahydro-<4>pyridyl>-aethanol C7H13NO zu formulierenden Reaktionsprodukts in Essigsaeure an Palladium; | |
With acetic acid; platinum Hydrogenation; |
pyridine-4-acetic acid
4-(2-Hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With platinum on activated charcoal; dimethylsulfide borane complex; hydrogen 2.) 1 atm; Multistep reaction; |
4-(2-Hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With ethanol; sodium |
2-(1,2,3,6-tetrahydro-[4]pyridyl)-ethanol
acetic acid
4-(2-Hydroxyethyl)piperidine
Conditions | Yield |
---|---|
Hydrogenation; |
1-t-Butoxycarbonyl-4-(methoxycarbonylmethyl)piperidine
4-(2-Hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With carbonylhydrido(tetrahydroborato)[bis(2-diphenylphosphinoethyl)-amino]ruthenium(II); hydrogen; sodium methylate In methanol at 100℃; under 38002.6 Torr; for 12h; Reagent/catalyst; |
4-(2-Hydroxyethyl)piperidine
di-tert-butyl dicarbonate
4-(2-hydroxyethyl)piperidine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With sodium hydroxide In tert-butyl alcohol at 23℃; for 30h; | 100% |
With triethylamine In chloroform at 0 - 20℃; for 1h; | 100% |
With sodium hydroxide In water; tert-butyl alcohol at 10 - 23℃; | 100% |
4-(2-Hydroxyethyl)piperidine
2-methoxy-pyridin-3-ylmethyl chloride
1-[(2-methoxy-pyridin-3-yl)methyl]-4-piperidineethanol
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 2h; | 100% |
4-(2-Hydroxyethyl)piperidine
tert-butyldicarbonate
4-(2-hydroxyethyl)piperidine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; | 100% |
In methanol at 20℃; for 2h; Inert atmosphere; | 95% |
In dichloromethane at 20℃; | 52 g |
4-(2-Hydroxyethyl)piperidine
chloroacetonitrile
2-(4-(2-hydroxyethyl)piperidin-1-yl)acetonitrile
Conditions | Yield |
---|---|
With triethylamine at 20℃; for 14h; | 100% |
4-(2-Hydroxyethyl)piperidine
2-[3-(3-chloropyrazin-2-yloxy)azetidin-1-yl]quinoline
2-(1-(3-((1-(quinolin-2-yl)azetidin-3-yl)oxy)pyrazin-2-yl)piperidin-4-yl)ethanol
Conditions | Yield |
---|---|
With potassium carbonate In water; isopropyl alcohol at 160℃; for 5h; Microwave irradiation; | 100% |
4-(2-Hydroxyethyl)piperidine
benzoyl chloride
(4-(2-hydroxyethyl)piperidin-1-yl)(phenyl)methanone
Conditions | Yield |
---|---|
With sodium hydroxide at 0℃; | 98% |
With triethylamine In dichloromethane at 20℃; |
4-(2-Hydroxyethyl)piperidine
isopropyl chloroformate
isopropyl 4-(2-hydroxyethyl)piperidine-1-carboxylate
Conditions | Yield |
---|---|
With sodium hydroxide In toluene at 20℃; for 2h; Carboxylation; | 98% |
With triethylamine In 1,2-dimethoxyethane; toluene at 20℃; | |
In dichloromethane; toluene at 20℃; for 2.5h; |
4-(2-Hydroxyethyl)piperidine
di-tert-butyl dicarbonate
2,2,2-trifluoroethyl benzoate
tert-butyl 4-(2-(benzoyloxy)ethyl)piperidine-1-carboxylate
Conditions | Yield |
---|---|
Stage #1: 4-(2-Hydroxyethyl)piperidine; 2,2,2-trifluoroethyl benzoate With (μ-oxo)bis[(1,2-ethanediamino-N,N'-bis(salicylidene))iron(III)] In toluene at 120℃; for 2h; Inert atmosphere; Schlenk technique; Stage #2: di-tert-butyl dicarbonate With triethylamine In dichloromethane at 4 - 20℃; for 4h; Inert atmosphere; Schlenk technique; chemoselective reaction; | 98% |
4-(2-Hydroxyethyl)piperidine
5-((tert-butyl)sulfanyl)-6-chloropyrazine-2,3-dicarbonitrile
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide | 97% |
4-(2-Hydroxyethyl)piperidine
tert-butyldimethylsilyl chloride
Conditions | Yield |
---|---|
With 1H-imidazole In dichloromethane at 20℃; for 18h; | 97% |
Stage #1: tert-butyldimethylsilyl chloride With 1H-imidazole In N,N-dimethyl-formamide at 25℃; for 1h; Stage #2: 4-(2-Hydroxyethyl)piperidine In N,N-dimethyl-formamide at 25℃; for 8h; | 82.45% |
4-(2-Hydroxyethyl)piperidine
2-chloro-5-ethylpyrimidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dimethyl sulfoxide at 110℃; | 97% |
4-(2-Hydroxyethyl)piperidine
Methyl formate
N-formyl-4-(2-hydroxyethyl)piperidine
Conditions | Yield |
---|---|
at 0 - 20℃; for 1h; | 95% |
With sodium hydroxide In methanol |
4-(2-Hydroxyethyl)piperidine
2,3-dichloro-5,6-dicyanopyrazine
Conditions | Yield |
---|---|
In tetrahydrofuran at 0℃; for 1h; Cooling with ice; | 95% |
In tetrahydrofuran at 0℃; | 95% |
4-(2-Hydroxyethyl)piperidine
4-(2-hydroxyethyl)piperidine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
In ethanol for 1h; Reflux; | 95% |
4-(2-Hydroxyethyl)piperidine
5-chloro-6-(diethylamino)pyrazine-2,3-dicarbonitrile
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 1.5h; | 95% |
4-(2-Hydroxyethyl)piperidine
benzoic acid methyl ester
2-(piperidine-4-yl)ethyl benzoate
Conditions | Yield |
---|---|
With tetramethylammonium methyl carbonate In toluene for 3h; Molecular sieve; Reflux; Green chemistry; | 94% |
4-(2-Hydroxyethyl)piperidine
2,6-bis(3-chloropropionamido)anthracene-9,10-dione
2,6-bis<3-<4-(2-hydroxyethyl)piperidino>propionamido>anthracene-9,10-dione
Conditions | Yield |
---|---|
In ethanol for 5h; Heating; | 93% |
4-(2-Hydroxyethyl)piperidine
benzoic acid methyl ester
A
2-(piperidine-4-yl)ethyl benzoate
B
N-benzoylpiperidine-4-ylethyl benzoate
Conditions | Yield |
---|---|
Zn4(OCOCF3)6O In toluene for 18h; Inert atmosphere; Reflux; | A 92% B 7% |
4-(2-Hydroxyethyl)piperidine
tert-butyl (2-{[3-(2-chloropyrimidin-5-yl)benzyl](methyl)amino}-2-oxoethyl)carbamate
tert-butyl {2-[(3-{2-[4-(2-hydroxyethyl)piperidin-1-yl]pyrimidin-5-yl}benzyl)(methyl)amino]-2-oxoethyl}carbamate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; | 92% |
4-(2-Hydroxyethyl)piperidine
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 1h; Cooling with ice; | 91% |
In tetrahydrofuran at 20℃; | 91% |
4-(2-Hydroxyethyl)piperidine
6,7-dimethoxy-4-chloroquinazoline
Conditions | Yield |
---|---|
In isopropyl alcohol at 100℃; for 16h; Sealed tube; | 91% |
4-(2-Hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In butan-1-ol at 200℃; for 4h; Sealed tube; | 91% |
4-(2-Hydroxyethyl)piperidine
6,7-dimethoxy-4-chloroquinazoline
Conditions | Yield |
---|---|
In isopropyl alcohol at 100℃; for 16h; Sealed tube; | 91% |
4-(2-Hydroxyethyl)piperidine
(3,4-Dimethoxyphenyl)acetic acid
2-(3,4-dimethoxyphenyl)-1-[4-(2-hydroxyethyl)piperidin-1-yl]ethanone
Conditions | Yield |
---|---|
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 5h; | 90% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 5h; | 90% |
4-(2-Hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 2h; | 90% |
2-(6-bromo-1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)-N,N-dimethylethanamine
4-(2-Hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In 2-methoxy-ethanol at 120℃; for 24h; Inert atmosphere; | 89% |
4-(2-Hydroxyethyl)piperidine
2-bromomethyl-2,3-dihydro-2,4,6,7-tetramethyl-5-benzofuranamine
Conditions | Yield |
---|---|
88% |
4-(2-Hydroxyethyl)piperidine
benzyl chloroformate
1-(Benzyloxycarbonyl)-4-(2-hydroxyethyl)piperidine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In water; acetonitrile at 25℃; for 12h; Inert atmosphere; | 86% |
With sodium carbonate In dichloromethane; water at 0 - 25℃; for 6h; Inert atmosphere; | 82% |
With triethylamine In acetonitrile at 20℃; | 81% |
4-(2-Hydroxyethyl)piperidine
Conditions | Yield |
---|---|
In tetrahydrofuran at 70℃; for 4h; | 86% |
Conditions | Yield |
---|---|
With potassium carbonate In ethanol at 80℃; for 12h; Inert atmosphere; | 86% |
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