Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryUnique advantages for 4-Chlorobutyronitrile Cas 628-20-6 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Liquid Storage:Refrigerator Package:1kg/foil bag, 25kg/drum
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Cas:628-20-6
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Cas:628-20-6
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inquiryProduct Name: 4-Chlorobutyronitrile Synonyms: GAMMA-CHLOROPROPYL CYANIDE;4-CHLOROBUTYRONITRILE;4-CHLOROBUTANENITRILE;4-chloro-butanenitril;4-chloro-butyronitril;Butyronitrile, 4-chloro-;gamma-Chlorobutyronitrile;4-CHLOROBUTYRONITRILE 99% (GC) CAS
Cas:628-20-6
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:628-20-6
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inquirySynonyms:Gamma-chloropropyl cyanide; 4-chlorobutyronitrile; 4-chlorobutanenitrile; 4-chloro-butanenitril; 4-chloro-butyronitril; butyronitrile, 4-chloro-; gamma-chlorobutyronitrile; butanenitrile, 4-chloro-; 1-chloro-3-cyanopropane; chlorobutyronit
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Cas:628-20-6
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:628-20-6
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inquiry4-Chlorobutyronitrile CAS:628-20-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter
Cas:628-20-6
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By
Cas:628-20-6
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:628-20-6
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
4-Chlorobutyronitrile Chemical Properties Boiling point 195-197 °C (lit.) density 1.095 g/mL at 20 °C refractive index n20/D 1.442(lit.) Fp 185 °F storage temp. Refrigerator form Liquid color Clear colorless to
Cas:628-20-6
Min.Order:1 Gram
FOB Price: $66.0
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:628-20-6
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:628-20-6
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:628-20-6
Min.Order:1 Metric Ton
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inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
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GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryStock products, own laboratoryAppearance:Colorless liquid Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:628-20-6
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
4-Chlorobutyronitrile
Conditions | Yield |
---|---|
With aluminum oxide; calcium hydroxide; 2-hydroxynitrobenzene In cyclohexane at 77 - 97℃; for 5.5h; Temperature; Reflux; | 92% |
Conditions | Yield |
---|---|
With formaldehyd; formic acid; acetonitrile for 12h; Heating; | 87% |
4-Chlorobutyronitrile
Conditions | Yield |
---|---|
With N-chloro-succinimide; potassium acetate; 9-(2-mesityl)-10-methylacridinium perchlorate In acetonitrile at 20℃; for 1h; Irradiation; Sealed tube; Inert atmosphere; | 59% |
Conditions | Yield |
---|---|
With trifluoroacetic acid; trifluoroacetic anhydride; sodium nitrite at 20℃; nitrosative cleavage; | 57% |
Conditions | Yield |
---|---|
With chlorine Irradiation.mit UV-Licht; | |
With sodium persulfate; copper dichloride In water at 85 - 90℃; for 10h; Yield given. Yields of byproduct given; | |
With N-chloropiperidine; 2,2'-azobis(isobutyronitrile) In trifluoroacetic acid at 30℃; Product distribution; Rate constant; Irradiation; relative rate constants, position selectivity, substrate selectivity; |
Conditions | Yield |
---|---|
With thionyl chloride; benzene | |
With trichlorophosphate; benzene | |
With phosphorus trichloride |
ethanol
sodium cyanide
1,3-chlorobromopropane
A
4-Chlorobutyronitrile
B
4-bromobutanenitrile
ethanol
potassium cyanide
1,3-chlorobromopropane
A
4-Chlorobutyronitrile
B
Glutaronitrile
sodium cyanide
1,3-chlorobromopropane
A
4-Chlorobutyronitrile
B
Glutaronitrile
Conditions | Yield |
---|---|
With methanol |
Conditions | Yield |
---|---|
With ethanol | |
With ethanol; water Alkohol abdestillieren,Wasser zum Rueckstand geben,abgeschiedene Oelschicht abheben und fraktionieren; |
Conditions | Yield |
---|---|
(i) liq. NH3, (ii) SOCl2; Multistep reaction; |
Conditions | Yield |
---|---|
In dichloromethane |
2,4-dichlorobutanenitrile
4-Chlorobutyronitrile
Conditions | Yield |
---|---|
With acetic acid; zinc for 2h; Yield given; |
propyl cyanide
chlorine
A
3-chlorobutyronitrile
B
4-Chlorobutyronitrile
Conditions | Yield |
---|---|
mit UV-Licht in der Dampfphase.Irradiation; |
propyl cyanide
chlorine
A
3-chlorobutyronitrile
B
4-Chlorobutyronitrile
C
2-chlorobutyronitrile
Conditions | Yield |
---|---|
at 450℃; Dampfphase; |
Conditions | Yield |
---|---|
With chlorine at 450℃; |
4-Chlorobutyronitrile
sodium thiomethoxide
4-(methylthio)butyronitrile
Conditions | Yield |
---|---|
In ethanol at 20℃; for 25h; Inert atmosphere; Cooling with ice; | 100% |
In ethanol | |
In ethanol at 25℃; for 15h; |
4-Chlorobutyronitrile
tert-butyl N-(benzyloxy)carbamate
4-[N-(tert-butyloxycarbonyl)benzyloxyamino]butyronitrile
Conditions | Yield |
---|---|
Stage #1: tert-butyl N-(benzyloxy)carbamate With sodium hydride In N,N-dimethyl-formamide for 0.166667h; Inert atmosphere; Stage #2: 4-Chlorobutyronitrile With sodium iodide In N,N-dimethyl-formamide at 80℃; for 6h; | 100% |
Stage #1: tert-butyl N-(benzyloxy)carbamate With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: 4-Chlorobutyronitrile With sodium iodide In N,N-dimethyl-formamide at 70℃; for 18h; Inert atmosphere; | 98% |
With sodium hydride; sodium iodide In N,N-dimethyl-formamide at 60 - 70℃; for 5h; | 80% |
Stage #1: tert-butyl N-(benzyloxy)carbamate With sodium hydride; sodium iodide In N,N-dimethyl-formamide at 0℃; Inert atmosphere; Stage #2: 4-Chlorobutyronitrile In N,N-dimethyl-formamide at 85℃; Inert atmosphere; | 70% |
With sodium hydride; potassium iodide In N,N-dimethyl-formamide |
4-Chlorobutyronitrile
(S)-(-)-[1-phenylethyl]-1H-imidazole
3-(3-cyanopropyl)-1-((1S)-1-phenylethyl)-1H-imidazol-3-ium chloride
Conditions | Yield |
---|---|
In acetonitrile Reflux; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; for 72h; | 99% |
In toluene for 7h; Reflux; | 65% |
at 20℃; | 63% |
Conditions | Yield |
---|---|
With hydrogenchloride; sodium hydroxide; sodium chloride In water; dimethyl sulfoxide | 98% |
With sodium hydride In ethylene glycol; mineral oil at 20 - 80℃; for 0.5h; Solvent; Reagent/catalyst; | 97.2% |
With potassium tert-butylate In tetrahydrofuran at -30℃; for 0.333333h; | 89% |
4-Chlorobutyronitrile
methyl N-tosylanthranilate
methyl 2-{(3-cyanopropyl)[(4-methylphenyl)sulfonyl]amino}benzoate
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In butanone for 12h; Heating; | 98% |
With potassium carbonate; potassium iodide In acetone for 168h; Heating; | 95% |
With potassium carbonate; potassium iodide In butanone for 12h; Reflux; | 80.1% |
4-Chlorobutyronitrile
[1(R)-methyl-3-[(phenylmethyl)amino]propyl]carbamic acid, 1,1-dimethylethyl ester
3-[(3-cyanopropyl)(phenylmethyl)amino-1(R)-methylpropyl]carbamic acid, 1,1-dimethylethyl ester
Conditions | Yield |
---|---|
With sodium carbonate; potassium iodide In butan-1-ol for 20h; Alkylation; Heating; | 98% |
4-Chlorobutyronitrile
N-(2,4,6-trimethylphenyl)imidazole
1-(2,4,6-trimethylphenyl)-3-(butylnitrile)imidazolium chloride
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane for 72h; Reflux; Inert atmosphere; | 98% |
In 1,2-dimethoxyethane Inert atmosphere; Heating; | 98% |
4-Chlorobutyronitrile
Conditions | Yield |
---|---|
With triphenyl phosphite; bromine at 80℃; for 4h; Reagent/catalyst; | 98% |
4-Chlorobutyronitrile
dimethylsilicon dichloride
(3-cyanopropyl)dimethylsilyl chloride
Conditions | Yield |
---|---|
With magnesium; ethylene dibromide; manganese(ll) chloride In tetrahydrofuran at 65℃; for 2h; Inert atmosphere; | 96.1% |
Stage #1: 4-Chlorobutyronitrile With sodium In toluene at 108 - 110℃; for 3h; Stage #2: dimethylsilicon dichloride In toluene at 40 - 45℃; for 4h; Temperature; |
4-Chlorobutyronitrile
1-(2-Methoxyphenyl)piperazine
4‐[4‐(2‐methoxyphenyl)piperazin‐1‐yl]butannitrile
Conditions | Yield |
---|---|
With cesium hydroxide; sodium iodide at 60℃; for 1.33333h; Microwave irradiation; Neat (no solvent); chemoselective reaction; | 96% |
4-Chlorobutyronitrile
N-p-toluenesulfonyl-4-chloro-anthranilic acid methyl ester
methyl 4-chloro-2-(N-tosyl-3-cyanopropylamino)benzoate
Conditions | Yield |
---|---|
With potassium carbonate; potassium iodide In acetone for 168h; Heating; | 95% |
4-Chlorobutyronitrile
N-[N-(tert-Butyloxycarbonyl)-3-aminopropyl]benzylamine
N-[N-(tert-Butoxycarbonyl)-3-aminopropyl]-N-(3-cyanopropyl)benzylamine
Conditions | Yield |
---|---|
With sodium carbonate; potassium iodide In butan-1-ol for 48h; Heating; | 95% |
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 0 - 20℃; for 48h; Inert atmosphere; | 95% |
With triethylamine In N,N-dimethyl-formamide at 25℃; | |
With sodium methylate; sodium iodide 1.) methanol, 1 h, 2.) reflux, 12 h; Yield given. Multistep reaction; |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide for 4h; Heating; | 95% |
4-Chlorobutyronitrile
1,2,3,4-tetrahydro-4-methylspiro
N-(γ-cyanopropyl)-3,4-dihydro-4-methylspiro[quinoline-2,1'-cyclohexane]
Conditions | Yield |
---|---|
With sodium carbonate; potassium iodide In butan-1-ol Heating; | 95% |
Conditions | Yield |
---|---|
at 80℃; for 24h; | 95% |
at 70℃; for 48h; Neat (no solvent); Sealed vial; | 92% |
at 80℃; for 24h; | 82% |
Heating; | 78% |
at 79.84℃; for 48h; |
4-Chlorobutyronitrile
trans-hydridochloro-di-{1,2-bis(diphenylphosphino)ethane}iron(II)
trans-[FeH(4-chlorobutyronitrile)(dppe)2]Cl
Conditions | Yield |
---|---|
In further solvent(s) Ar-atmosphere; stirring in ClCH2CH2CH2CN for 1 h; filtration, solvent removal (vac.), washing (Et2O); elem. anal.; | 95% |
methanol
4-Chlorobutyronitrile
methyl 3-chloropropanimidate hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride In diethyl ether at 20℃; for 4h; | 94% |
With hydrogenchloride In diethyl ether at -20℃; for 24h; | 90% |
With hydrogenchloride In diethyl ether at 0℃; for 24h; | 70% |
With hydrogenchloride In diethyl ether at -20 - 0℃; for 28h; |
4-Chlorobutyronitrile
Conditions | Yield |
---|---|
With aluminum oxide; calcium hydroxide; 2-hydroxynitrobenzene In cyclohexane at 77 - 97℃; for 5.5h; Temperature; Reflux; | 92% |
Conditions | Yield |
---|---|
With formaldehyd; formic acid; acetonitrile for 12h; Heating; | 87% |
4-Chlorobutyronitrile
Conditions | Yield |
---|---|
With N-chloro-succinimide; potassium acetate; 9-(2-mesityl)-10-methylacridinium perchlorate In acetonitrile at 20℃; for 1h; Irradiation; Sealed tube; Inert atmosphere; | 59% |
Conditions | Yield |
---|---|
With trifluoroacetic acid; trifluoroacetic anhydride; sodium nitrite at 20℃; nitrosative cleavage; | 57% |
Conditions | Yield |
---|---|
With chlorine Irradiation.mit UV-Licht; | |
With sodium persulfate; copper dichloride In water at 85 - 90℃; for 10h; Yield given. Yields of byproduct given; | |
With N-chloropiperidine; 2,2'-azobis(isobutyronitrile) In trifluoroacetic acid at 30℃; Product distribution; Rate constant; Irradiation; relative rate constants, position selectivity, substrate selectivity; |
Conditions | Yield |
---|---|
With thionyl chloride; benzene | |
With trichlorophosphate; benzene | |
With phosphorus trichloride |
ethanol
sodium cyanide
1,3-chlorobromopropane
A
4-Chlorobutyronitrile
B
4-bromobutanenitrile
ethanol
potassium cyanide
1,3-chlorobromopropane
A
4-Chlorobutyronitrile
B
Glutaronitrile
sodium cyanide
1,3-chlorobromopropane
A
4-Chlorobutyronitrile
B
Glutaronitrile
Conditions | Yield |
---|---|
With methanol |
Conditions | Yield |
---|---|
With ethanol | |
With ethanol; water Alkohol abdestillieren,Wasser zum Rueckstand geben,abgeschiedene Oelschicht abheben und fraktionieren; |
Conditions | Yield |
---|---|
(i) liq. NH3, (ii) SOCl2; Multistep reaction; |
Conditions | Yield |
---|---|
In dichloromethane |
2,4-dichlorobutanenitrile
4-Chlorobutyronitrile
Conditions | Yield |
---|---|
With acetic acid; zinc for 2h; Yield given; |
propyl cyanide
chlorine
A
3-chlorobutyronitrile
B
4-Chlorobutyronitrile
Conditions | Yield |
---|---|
mit UV-Licht in der Dampfphase.Irradiation; |
propyl cyanide
chlorine
A
3-chlorobutyronitrile
B
4-Chlorobutyronitrile
C
2-chlorobutyronitrile
Conditions | Yield |
---|---|
at 450℃; Dampfphase; |
Conditions | Yield |
---|---|
With chlorine at 450℃; |
4-Chlorobutyronitrile
sodium thiomethoxide
4-(methylthio)butyronitrile
Conditions | Yield |
---|---|
In ethanol at 20℃; for 25h; Inert atmosphere; Cooling with ice; | 100% |
In ethanol | |
In ethanol at 25℃; for 15h; |
4-Chlorobutyronitrile
tert-butyl N-(benzyloxy)carbamate
4-[N-(tert-butyloxycarbonyl)benzyloxyamino]butyronitrile
Conditions | Yield |
---|---|
Stage #1: tert-butyl N-(benzyloxy)carbamate With sodium hydride In N,N-dimethyl-formamide for 0.166667h; Inert atmosphere; Stage #2: 4-Chlorobutyronitrile With sodium iodide In N,N-dimethyl-formamide at 80℃; for 6h; | 100% |
Stage #1: tert-butyl N-(benzyloxy)carbamate With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: 4-Chlorobutyronitrile With sodium iodide In N,N-dimethyl-formamide at 70℃; for 18h; Inert atmosphere; | 98% |
With sodium hydride; sodium iodide In N,N-dimethyl-formamide at 60 - 70℃; for 5h; | 80% |
Stage #1: tert-butyl N-(benzyloxy)carbamate With sodium hydride; sodium iodide In N,N-dimethyl-formamide at 0℃; Inert atmosphere; Stage #2: 4-Chlorobutyronitrile In N,N-dimethyl-formamide at 85℃; Inert atmosphere; | 70% |
With sodium hydride; potassium iodide In N,N-dimethyl-formamide |
4-Chlorobutyronitrile
(S)-(-)-[1-phenylethyl]-1H-imidazole
3-(3-cyanopropyl)-1-((1S)-1-phenylethyl)-1H-imidazol-3-ium chloride
Conditions | Yield |
---|---|
In acetonitrile Reflux; | 100% |
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 20℃; for 72h; | 99% |
In toluene for 7h; Reflux; | 65% |
at 20℃; | 63% |
Conditions | Yield |
---|---|
With hydrogenchloride; sodium hydroxide; sodium chloride In water; dimethyl sulfoxide | 98% |
With sodium hydride In ethylene glycol; mineral oil at 20 - 80℃; for 0.5h; Solvent; Reagent/catalyst; | 97.2% |
With potassium tert-butylate In tetrahydrofuran at -30℃; for 0.333333h; | 89% |
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