2,4,6-Trioxaheptane Basic information Product Name: 2,4,6-Trioxaheptane Synonyms: 2,4,6-Trioxaheptane;Methoxy(MethoxyMethoxy)Methane CAS: 628-90-0 MF: C4H10O3 MW: 106.1204 EINECS: Product Categories: Mol File: 628-90-0.mol 2,4,6
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inquiry2,4,6-Trioxaheptane CAS:628-90-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
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inquiryName: 2, 4, 4, 6, 6, Trioxaheptane. Synonym: 2, 4, 4, 6, Israel, Trioxa, heptaneten, Methoxy (MChemicalbookethoxyMethoxy) Methane. CAS No: 628-90-0. Molecular formula: C4H10O3. Molecular weight: 106.1204. Appearance: colorless transparent
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inquirybis(methoxymethyl)ether Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like DHL or Fedx. Port:Shanghai/Shenzhen
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inquiry1.We have rich experience in the development and production 2.Our factory is in Shanghai of China,We have convenient traffic conditions.3.We have advanced testing equipment and shipping line. Package:5g, 10g, 50g, 100g, 2kg Application:Pharmaceutical
High purity,Competitive Price,Leading Company in the filed. Application:Pharmaceutical Intermediate
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Conditions | Yield |
---|---|
With sulfonic acid resin at 80 - 95℃; Temperature; Reagent/catalyst; | 95.5% |
With ZrO2#dotLa2O3 at 80℃; for 4h; | 6.1% |
With C16H36NO3S(1+)*CH3O4S(1-) at 125 - 130℃; under 26252.6 - 30003 Torr; Reagent/catalyst; Inert atmosphere; |
methanol
diethyl ether
bromomethylmethyl ether
bis(methoxymethyl)ether
Conditions | Yield |
---|---|
In ethyl acetate; N,N-dimethyl-formamide; mineral oil | 90% |
formaldehyd
Dimethoxymethane
A
bis-methoxymethoxy-methane
B
bis(methoxymethyl)ether
Conditions | Yield |
---|---|
With sulfuric acid at 109.99℃; under 7500.75 Torr; | A n/a B 26% |
methanol
formaldehyd
A
bis-methoxymethoxy-methane
B
bis(methoxymethyl)ether
C
POMM4
Conditions | Yield |
---|---|
With ZrO2#dotLa2O3 at 130℃; under 6000.6 Torr; for 4h; Pressure; Reagent/catalyst; | A 23% B 23.3% C 14.9% |
formaldehyd
Dimethoxymethane
A
bis-methoxymethoxy-methane
B
bis(methoxymethyl)ether
C
POMM4
Conditions | Yield |
---|---|
With La2O3 doped titania at 130℃; under 4500.45 Torr; for 4h; Reagent/catalyst; Pressure; Autoclave; | A 22.4% B 17.5% C 8.4% |
With macroporous strong acidic styrene type cation exchange resin catalyst at 100℃; under 15001.5 Torr; for 10h; Temperature; Time; Overall yield = 51.66 %; | |
With Cl -/TiO2-La2O3/SBA-15 (Si/Al=38) at 130℃; under 4500.45 Torr; for 4h; Reagent/catalyst; Temperature; Pressure; |
Conditions | Yield |
---|---|
With naphthalene; lithium In tetrahydrofuran; water |
1,3,5-Trioxan
1,1-dimethoxyethane
C
bis-methoxymethoxy-methane
D
bis(methoxymethyl)ether
E
POMM4
F
CH3-(OCH2)8-OCH3
G
Methoxymethoxymethoxymethoxymethoxy-methoxymethoxymethoxymethoxymethoxymethoxy-methane
H
POMM5
I
CH3-(OCH2)7-OCH3
J
CH3-(OCH2)6-OCH3
Conditions | Yield |
---|---|
Amberlite IR 120 at 100℃; for 24h; Product distribution / selectivity; | |
trifluorormethanesulfonic acid at 100℃; for 40h; Product distribution / selectivity; | |
sulfuric acid In water at 100℃; for 12h; Product distribution / selectivity; |
1,3,5-Trioxan
1,1-dimethoxyethane
A
bis-methoxymethoxy-methane
B
bis(methoxymethyl)ether
C
POMM4
Conditions | Yield |
---|---|
sulfuric acid In water at 100℃; for 16h; Product distribution / selectivity; |
formaldehyd
1,1-dimethoxyethane
C
bis-methoxymethoxy-methane
D
bis(methoxymethyl)ether
E
POMM4
F
CH3-(OCH2)8-OCH3
G
Methoxymethoxymethoxymethoxymethoxy-methoxymethoxymethoxymethoxymethoxymethoxy-methane
H
POMM5
I
CH3-(OCH2)7-OCH3
J
CH3-(OCH2)6-OCH3
Conditions | Yield |
---|---|
Amberlite IR 120 at 100℃; for 8h; Product distribution / selectivity; |
formaldehyd
Dimethoxymethane
A
1,3,5-Trioxan
D
bis-methoxymethoxy-methane
E
bis(methoxymethyl)ether
F
POMM4
G
CH3-(OCH2)8-OCH3
H
Methoxymethoxymethoxymethoxymethoxy-methoxymethoxymethoxymethoxymethoxymethoxy-methane
I
CH3-(OCH2)7-OCH3
L
CH3-(OCH2)6-OCH3
Conditions | Yield |
---|---|
With sulfuric acid at 55 - 115℃; Inert atmosphere; |
Conditions | Yield |
---|---|
With pyridine; hydrogenchloride; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; dichloromethane; toluene |
Dimethyl ether
A
methanol
B
formaldehyd
C
methane
D
bis(methoxymethyl)ether
E
carbon monoxide
Conditions | Yield |
---|---|
With oxygen at 19.84℃; Flow reactor; Green chemistry; |
Dimethyl ether
A
methanol
B
formaldehyd
C
bis(methoxymethyl)ether
D
carbon monoxide
Conditions | Yield |
---|---|
With oxygen at 19.84℃; Flow reactor; Green chemistry; |
Dimethoxymethane
A
methanol
B
formaldehyd
C
methane
D
bis(methoxymethyl)ether
E
carbon monoxide
Conditions | Yield |
---|---|
With oxygen at 19.84℃; Flow reactor; Green chemistry; |
Dimethoxymethane
A
methanol
B
formaldehyd
C
bis(methoxymethyl)ether
D
carbon monoxide
Conditions | Yield |
---|---|
With oxygen at 19.84℃; Flow reactor; Green chemistry; |
1,3,5-Trioxan
formaldehyd
A
bis-methoxymethoxy-methane
B
bis(methoxymethyl)ether
Conditions | Yield |
---|---|
With strong acidic styrene type cation exchange resin catalyst at 100℃; under 15001.5 Torr; for 3h; Temperature; Time; Overall yield = 43.26 %; |
1,3,5-Trioxan
formaldehyd
A
bis-methoxymethoxy-methane
B
bis(methoxymethyl)ether
C
POMM4
Conditions | Yield |
---|---|
With strong acidic styrene type cation exchange resin catalyst at 80 - 100℃; under 15001.5 Torr; for 3h; Temperature; Time; Overall yield = 47.55 %; |
methanol
formaldehyd
A
Dimethoxymethane
B
bis-methoxymethoxy-methane
C
bis(methoxymethyl)ether
Conditions | Yield |
---|---|
With C16H36NO3S(1+)*CH3O4S(1-) at 125 - 130℃; under 26252.6 - 30003 Torr; Reagent/catalyst; Inert atmosphere; |
methanol
formaldehyd
A
Dimethoxymethane
B
bis-methoxymethoxy-methane
C
bis(methoxymethyl)ether
D
POMM4
Conditions | Yield |
---|---|
With C16H36NO3S(1+)*CH3O4S(1-) at 125 - 130℃; under 26252.6 - 30003 Torr; Reagent/catalyst; Inert atmosphere; |
methanol
formaldehyd
A
Dimethoxymethane
B
bis-methoxymethoxy-methane
C
bis(methoxymethyl)ether
D
POMM4
E
POMM5
Conditions | Yield |
---|---|
With C16H36NO3S(1+)*CH3O4S(1-) In water at 125 - 130℃; under 26252.6 - 30003 Torr; Reagent/catalyst; |
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