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Cas:634-47-9
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Min.Order:1 Gram
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Min.Order:1 Kilogram
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Min.Order:10 Gram
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Min.Order:1 Kilogram
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High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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Min.Order:1 Metric Ton
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
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Cas:634-47-9
Min.Order:0
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Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:off-white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as prima
2-Chloro-4-methylquinoline cas 634-47-9Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Best quality with low priceAppearance:white to light yellow crystal powder Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
We are professional supplier in China for this product, we are dedicated to providing customers with the best quality, price, and service. Please feel free to send us inquiries.Appearance:Please contact us for product details Package:As per shipment
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
634-47-9 Application:intermediate
Cas:634-47-9
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Type:Lab/Research institutions
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Conditions | Yield |
---|---|
With trichlorophosphate In dichloromethane; N,N-dimethyl-formamide at 0 - 25℃; Inert atmosphere; regioselective reaction; | 81% |
2-chloro-4-methylquinoline
Conditions | Yield |
---|---|
With lithium chloride In 1,4-dioxane at 80℃; for 72h; Inert atmosphere; Sealed tube; regioselective reaction; | 32% |
Conditions | Yield |
---|---|
With phosphorus pentachloride; trichlorophosphate for 24h; Chlorination; Heating; | 96% |
With trichlorophosphate for 10h; Heating; | 82% |
With phosphorus pentachloride; trichlorophosphate |
2-Chloro-4-methylquinoline 1-oxide
2-chloro-4-methylquinoline
Conditions | Yield |
---|---|
With tris(bipyridine)ruthenium(II) dichloride hexahydrate; di-tert-butyl 1,4-dihydro-2,6-dimethyl-3,5-pyridine-dicarboxylate In acetonitrile at 20℃; for 0.0833333h; Inert atmosphere; Irradiation; chemoselective reaction; | 82% |
Conditions | Yield |
---|---|
With phosphorus pentachloride; trichlorophosphate at 135 - 140℃; | |
With phosphorus pentachloride; benzoyl chloride at 250℃; | |
With ((1,3,5-triazine-2,4,6-triyl)tris(oxy))tris(triphenylphosphonium) chloride In neat (no solvent) at 140 - 150℃; for 2h; | |
With trichlorophosphate at 120℃; for 2h; |
2-chloro-4-methylquinoline
Conditions | Yield |
---|---|
With trichlorophosphate at 80 - 85℃; |
methylmagnesium chloride
2,4-dichloroquinoline
2-chloro-4-methylquinoline
Conditions | Yield |
---|---|
With zinc dibromide In tetrahydrofuran |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sulfuric acid / 1 h / 100 °C 2: trichlorophosphate / 2 h / 120 °C View Scheme | |
Multi-step reaction with 2 steps 1: Polyphosphoric acid / 130 - 140 °C 2: trichlorophosphate; pyridine / 80 - 90 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: 0.07 h / microwave irradiation 1.2: H2SO4 / 0.08 h / microwave irradiation 2.1: 82 percent / POCl3 / 10 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 3 h / 185 °C 2: sulfuric acid / 1 h / 100 °C 3: trichlorophosphate / 2 h / 120 °C View Scheme |
2-chloro-4-methylquinoline
Conditions | Yield |
---|---|
durch Ueberfuehren in 2-Chlor-7(?)-hydrazino-4-methyl-chinolin und folgendes Kochen mit Kupfersulfat-Loesung; |
Conditions | Yield |
---|---|
at 250℃; |
2-chloro-4-methyl-7-aminoquinoline
2-chloro-4-methylquinoline
Conditions | Yield |
---|---|
Reduzieren des Reaktionsprodukts mit salzsaurer Zinnchloruer-Loesung und Kochen des entstandenen Hydrazins mit Kupfersulfat-Loesung.Diazotization; |
4-methylquinolin-2-ol
phosphorus pentachloride
2-chloro-4-methylquinoline
2-chloro-4-methylquinoline
4-trifluoromethylphenylboronic acid
4-methyl-2-(4-(trifluoromethyl)phenyl)-4-methylquinoline
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In ethanol for 4h; Heating / reflux; | 100% |
2-chloro-4-methylquinoline
4-methyl-1-naphthylboronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 24h; Suzuki Coupling; Inert atmosphere; | 99.8% |
2-chloro-4-methylquinoline
(R)-Phenylglycinol
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In isopropyl alcohol at 130℃; for 46h; | 99% |
thiophene boronic acid
2-chloro-4-methylquinoline
4-(4-methylquinolin-4-yl)-diphenylaniline
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In tetrahydrofuran; water at 80℃; for 24h; Suzuki Coupling; Inert atmosphere; | 99% |
With potassium carbonate; sodium tetrachloropalladate(II) In water; butan-1-ol at 100℃; for 12h; Suzuki cross-coupling; | 95% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In methanol; water; toluene at 85℃; for 8h; Suzuki Coupling; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
With ((C6H4)(PPh2)(NCHPhP(O)Ph2))NiCl In diethyl ether at 25℃; for 12h; Kumada cross-coupling; Inert atmosphere; | 99% |
With C32H26ClN2NiP In tetrahydrofuran at 30℃; for 12h; Kumada Cross-Coupling; Schlenk technique; Inert atmosphere; | 95% |
2-chloro-4-methylquinoline
p-tolylzinc(II) chloride
Conditions | Yield |
---|---|
With C26H24ClN2NiP*0.1C7H8 In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 80℃; for 24h; Negishi Coupling; Schlenk technique; Inert atmosphere; | 99% |
With C38H34Br2N4Ni2P2 In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 40℃; for 12h; Reagent/catalyst; Negishi Coupling; Inert atmosphere; Schlenk technique; | 99% |
With C27H22Cl2N3NiP In tetrahydrofuran; 1-methyl-pyrrolidin-2-one for 6h; Inert atmosphere; Schlenk technique; Heating; | 99% |
2-chloro-4-methylquinoline
2-methylphenylzinc chloride
Conditions | Yield |
---|---|
With C27H22Cl2N3NiP In tetrahydrofuran; 1-methyl-pyrrolidin-2-one for 24h; Inert atmosphere; Heating; Schlenk technique; | 99% |
2-chloro-4-methylquinoline
Conditions | Yield |
---|---|
With Pd-PEPPSI-IPrAn In tetrahydrofuran; 1,4-dioxane at 0 - 20℃; for 6h; Negishi Coupling; Schlenk technique; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With C32H26ClN2NiP In tetrahydrofuran at 30℃; for 12h; Kumada Cross-Coupling; Schlenk technique; Inert atmosphere; | 99% |
2-chloro-4-methylquinoline
4-dimethylaminophenylmagnesium bromide
N,N-dimethyl-4-(4-methylquinolin-2-yl)benzenamine
Conditions | Yield |
---|---|
With C32H26ClN2NiP In tetrahydrofuran at 30℃; for 24h; Time; Kumada Cross-Coupling; Schlenk technique; Inert atmosphere; | 99% |
2-chloro-4-methylquinoline
2-mesityl-4-methylquinoline
Conditions | Yield |
---|---|
With silica supported Pd-PEPPSI-IPent In tetrahydrofuran at 25℃; for 0.111667h; Negishi Coupling; Flow reactor; Inert atmosphere; | 99% |
1-methyl-piperazine
2-chloro-4-methylquinoline
4-methyl-2-(4-methylpiperazin-1-yl)quinoline
Conditions | Yield |
---|---|
at 100℃; for 16h; | 98% |
With ethanol | |
In toluene Heating; |
Conditions | Yield |
---|---|
With C48H56ClN3Pd; potassium tert-butylate In tetrahydrofuran at 70℃; for 24h; Schlenk technique; Inert atmosphere; | 98% |
In ethanol for 12h; Heating; | 74% |
In butan-1-ol Heating; | 70% |
2-chloro-4-methylquinoline
4-methyl-2-(α-pyridyl)quinoline
Conditions | Yield |
---|---|
Stage #1: 2-chloro-4-methylquinoline; pyridin-2-ylzinc(II) bromide With dichloro(1,3-bis(2,6-bis(3-pentyl)phenyl)imidazolin-2-ylidene)(3-chloropyridyl)palladium(II); zinc(II) chloride In tetrahydrofuran at 23℃; for 24h; Negishi coupling; Inert atmosphere; Stage #2: With sodium hydrogencarbonate; trisodium Edetate In tetrahydrofuran; water pH=8; | 98% |
tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 60℃; for 24h; Negishi reaction; | 92% |
Conditions | Yield |
---|---|
In dichloromethane; acetonitrile at 20℃; for 1.5h; | 98% |
2-chloro-4-methylquinoline
2,4-difluorophenylboronic acid
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In ethanol; water; toluene at 110℃; for 16h; Suzuki-Miyaura Coupling; Inert atmosphere; | 98% |
Suzuki Coupling; Inert atmosphere; Schlenk technique; |
morpholine
2-chloro-4-methylquinoline
4-(4-methylquinolin-2-yl)morpholine
Conditions | Yield |
---|---|
With C48H56ClN3Pd; potassium tert-butylate In tetrahydrofuran at 70℃; for 24h; Schlenk technique; Inert atmosphere; | 97% |
With aluminum oxide for 0.0319444h; microwave irradiation; | 91% |
Stage #1: morpholine With C40H50BrCl2N3Pd; potassium tert-butylate at 20℃; Schlenk technique; Inert atmosphere; Stage #2: 2-chloro-4-methylquinoline In toluene at 100℃; for 24h; Schlenk technique; Inert atmosphere; | 82% |
2-chloro-4-methylquinoline
3-methyl-5-oxo-2,5-dihydro-isoxazole-4-carboxylic acid ethyl ester
ethyl 3-methyl-2-(4-methylquinolin-2-yl)-5-oxo-2,5-dihydroisoxazole-4-carboxylate
Conditions | Yield |
---|---|
In nitrobenzene at 140℃; for 0.5h; | 97% |
2-chloro-4-methylquinoline
N,N-dimethylethylenediamine
N1,N1-dimethyl-N2-(4-methylquinolin-2-yl)ethane-1,2-diamine
Conditions | Yield |
---|---|
With 2,6-di-tert-butyl-4-methyl-phenol; [1,3-bis(2,6-diisopentylphenyl)-4,5-dichloroimidazol-2-ylidene](3-chloropyridyl)palladium(II) dichloride; sodium hydride In toluene at 60℃; for 8h; Inert atmosphere; Schlenk technique; | 97% |
at 100℃; for 16h; | 69% |
Conditions | Yield |
---|---|
With copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride at 80℃; for 24h; | 97% |
2-chloro-4-methylquinoline
m-phenylenediamine
N-(4-methylquinolin-2-yl)benzene-1,3-diamine
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol; water Heating; | 97% |
Conditions | Yield |
---|---|
With C32H26ClN2NiP In tetrahydrofuran at 30℃; for 12h; Kumada Cross-Coupling; Schlenk technique; Inert atmosphere; | 97% |
2-chloro-4-methylquinoline
ethyl 5-oxo-2,5-dihydroisoxazole-4-carboxylate
ethyl 2-(4-methylquinolin-2-yl)-5-oxo-2,5-dihydroisoxazole-4-carboxylate
Conditions | Yield |
---|---|
In nitrobenzene at 140℃; for 0.0833333h; | 96% |
(2-hydroxyethyl)(methyl)amine
2-chloro-4-methylquinoline
2-[methyl-(4-methyl-quinolin-2-yl)-amino]-ethanol
Conditions | Yield |
---|---|
Heating; | 96% |
2-chloro-4-methylquinoline
m-tolylboronic acid
4-methyl-2-(m-tolyl)quinoline
Conditions | Yield |
---|---|
With sodium tetrachloropalladate(II); dicyclohexyl {2-sulfo-9-[3-(4-sulfophenyl)propyl]-9H-fluoren-9-yl}phosphonium hydrogen sulfate; potassium carbonate In water; butan-1-ol at 100℃; for 12h; Suzuki coupling; Inert atmosphere; | 96% |
2-chloro-4-methylquinoline
(meta-(trifluoromethyl)phenyl)boronic acid
4-methyl-2-(3-trifluoromethyl-phenyl)-quinoline
Conditions | Yield |
---|---|
With sodium tetrachloropalladate(II); dicyclohexyl {2-sulfo-9-[3-(4-sulfophenyl)propyl]-9H-fluoren-9-yl}phosphonium hydrogen sulfate; potassium carbonate In water; butan-1-ol at 100℃; for 12h; Suzuki coupling; Inert atmosphere; | 96% |
Suzuki Coupling; Inert atmosphere; Schlenk technique; |
2-chloro-4-methylquinoline
(2,6-dimethylphenyl)magnesium bromide
2-(2,6-dimethylphenyl)-4-methylquinoline
Conditions | Yield |
---|---|
Stage #1: (2,6-dimethylphenyl)magnesium bromide With dichloro(1,3-bis(2,6-bis(3-pentyl)phenyl)imidazolin-2-ylidene)(3-chloropyridyl)palladium(II); zinc(II) chloride In tetrahydrofuran at 23℃; for 0.333333h; Inert atmosphere; Stage #2: 2-chloro-4-methylquinoline In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 23℃; for 24h; Negishi coupling; Inert atmosphere; | 96% |
2-chloro-4-methylquinoline
2-furylzinc chloride
2-(furan-2-yl)-4-methylquinoline
Conditions | Yield |
---|---|
With C27H22Cl2N3NiP In tetrahydrofuran; 1-methyl-pyrrolidin-2-one for 2h; Inert atmosphere; Heating; Schlenk technique; | 96% |
2-chloro-4-methylquinoline
(1,1'-biphenyl)-4,4'-dithiol
2,2'-(biphenyl-4,4'-diylbissulfanediyl)bis-(4-methylquinoline)
Conditions | Yield |
---|---|
In ethanol Reflux; | 96% |
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