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inquiryItems Standard Result Assay (Ursolic acid) 98%min 98.22% -----------------------------------------------------------------------------------------------------------
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inquiry6362-80-7 C18H20 2,4-Diphenyl-4-methyl-1-pentene 1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:White Powder St
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inquiry2,4-Diphenyl-4-methyl-1-pentene CAS:6362-80-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality or
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inquiryAppearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:By Sea/Air/Courier Port:Qingdao
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inquiry2,4-Diphenyl-4-methyl-1-pentene Basic information Product Name: 2,4-Diphenyl-4-methyl-1-pentene Synonyms: 1,1’-(1,1-dimethyl-3-methylene-1,3-propanediyl)bis-benzen;1,1’-(1,1-dimethyl-3-methylene-1,3-propanediyl)bis-Benzene;4,4-Dimet
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inquiry2,4-Diphenyl-4-methyl-1-pentene Basic information Product Name: 2,4-Diphenyl-4-methyl-1-pentene Synonyms: Benzene,1,1'-(1,1-dimethyl-3-methylene-1,3-propanediyl)bis-;Alpha Methyls styrene diMer;2,4-Diphenyl-4-Methyl-1-pentene 97%;1,1&rsquo
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inquiryHangzhou Huarong Pharm Co., Ltd.established since 2006 , has been actively developing specialty products for Finished Dosages, APIs, Intermediates, and Fine chemicals markets in North America, Europe, Korea, Japan, Mid-East and all over the World. Hu
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inquiryName: 2,4-diphenyl-4-methyl-1-pentene CAS: 6362-80-7 Molecular Formula: C18H20 Molecular Weight: 236.351 Application:Fine chemical
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inquiryIsopropylbenzene
3-bromo-2-phenylprop-1-ene
2,4-diphenyl-4-methyl-pent-1-ene
Conditions | Yield |
---|---|
With di-tert-butyl peroxide; potassium carbonate at 120℃; for 93h; | 100% |
With di-tert-butyl peroxide; potassium carbonate at 120℃; for 93h; Degassed pressure tube; | 100% |
With triethyl borane; oxygen at 80℃; for 12h; | 35 %Chromat. |
isopropenylbenzene
A
1,1,3-trimethyl-3-phenylindane
B
2,4-diphenyl-4-methyl-pent-1-ene
C
4-methyl-2,4-diphenylpent-2-ene
Conditions | Yield |
---|---|
thiol-modified Al-loaded mesoporous silica In toluene at 120℃; for 2h; | A 97.1% B 0.7% C 1% |
thiol-modified Al-loaded mesoporous silica In toluene at 80℃; for 2h; | A 37.5% B 16.9% C 42.8% |
nafion resin; silica gel In various solvent(s) at 50℃; under 760 Torr; Product distribution; Rate constant; var. soluble liquid acids and resin-based solid acids as catalysts; var. time and solv.; |
Conditions | Yield |
---|---|
With indium(III) bromide In dichloromethane at 0℃; for 2h; | 90% |
With ruthenium trichloride In tetrahydrofuran | 78% |
With C13H17N3Ni(1+)*C32H12BF24(1-) In 1,2-dichloro-ethane at 60℃; for 4h; Inert atmosphere; | 72% |
Conditions | Yield |
---|---|
With bismuth(III) bromide In dichloromethane at -78 - 0℃; Inert atmosphere; | 88% |
With acetic anhydride; cerium triflate In acetonitrile at 20℃; for 24h; | 84% |
With iron(III) p-toluenesulfonate hexahydrate; acetic anhydride In acetonitrile | 26% |
Multi-step reaction with 2 steps 1: p-toluenesulfonic acid / benzene 2: 90 percent / InBr3 / CH2Cl2 / 2 h / 0 °C View Scheme |
Isopropylbenzene
2-((2-phenylallyl)oxy)isoindoline-1,3-dione
A
N-hydroxyphthalimide
B
2,4-diphenyl-4-methyl-pent-1-ene
Conditions | Yield |
---|---|
With di-tert-butyl peroxide In neat (no solvent) at 120℃; for 29h; | A n/a B 76% |
Isopropylbenzene
2-((2-phenylallyl)oxy)isoindoline-1,3-dione
2,4-diphenyl-4-methyl-pent-1-ene
Conditions | Yield |
---|---|
With di-tert-butyl peroxide In neat (no solvent) at 120℃; for 29h; Sealed tube; | 76% |
With di-tert-butyl peroxide at 120℃; Temperature; Sealed tube; |
cumenyl chloride
zinc diacetate
A
1-methyl-1-phenylethyl alcohol
B
cumyl acetate
C
2,4-diphenyl-4-methyl-pent-1-ene
D
isopropenylbenzene
Conditions | Yield |
---|---|
In acetic acid at 10 - 15℃; for 2h; | A 3.4 g B 72% C 5.9 g D 2.9 g |
1-methyl-1-phenylethyl alcohol
A
1,1,3-trimethyl-3-phenylindane
B
2,4-diphenyl-4-methyl-pent-1-ene
C
1,1-dimethyl-3-(2-methyl-2-phenylpropyl)-3-phenyl-2,3-dihydro-1H-indene
Conditions | Yield |
---|---|
With iron(III) chloride; 1,1,1,3',3',3'-hexafluoro-propanol; nitric acid at 20℃; for 3h; Catalytic behavior; | A 7 %Spectr. B 62% C 9 %Spectr. |
1-methyl-1-phenylethyl alcohol
A
2,4-diphenyl-4-methyl-pent-1-ene
B
isopropenylbenzene
Conditions | Yield |
---|---|
With phosphoric acid; acetic anhydride for 48h; Ambient temperature; | A 23% B 60% |
With o-benzenedisulfonimide; acetic anhydride at 20℃; | A 45% B 31% |
Conditions | Yield |
---|---|
zinc chloride diethyl ether In dichloromethane at -78℃; for 17h; | 58% |
methanol
isopropenylbenzene
A
Cumyl methyl ether
B
2,4-diphenyl-4-methyl-pent-1-ene
Conditions | Yield |
---|---|
With silica-supported KHSO4 at 70℃; for 3h; | A 26% B 55% |
With sulfuric acid In water at 80℃; for 2.66h; | A 11.3 %Chromat. B 13.67 %Chromat. |
1-methyl-1-phenylethyl alcohol
bis-trifluoromethyl-aminooxyl
A
2,4-diphenyl-4-methyl-pent-1-ene
B
2,4-diphenyl-4-methyl-2-pentene
C
(E)-(4-methylpent-2-ene-2,4-diyl)dibenzene
Conditions | Yield |
---|---|
at 20℃; for 72h; Yields of byproduct given; | A n/a B n/a C n/a D 50% |
isopropenylbenzene
phenol
A
2,4-di-cumylphenol
B
2,4,6-tri(α,α-dimethylbenzyl)phenol
C
2,4-diphenyl-4-methyl-pent-1-ene
D
4-methyl-2,4-diphenylpent-2-ene
Conditions | Yield |
---|---|
With aluminium at 135℃; for 3h; Further byproducts given; | A 33.8% B 46.5% C 2.7% D 0.7% |
isopropenylbenzene
phenol
A
2,4-di-cumylphenol
B
2,4,6-tri(α,α-dimethylbenzyl)phenol
C
2,4-diphenyl-4-methyl-pent-1-ene
D
4-methyl-2,4-diphenylpent-2-ene
Conditions | Yield |
---|---|
With aluminium at 135℃; for 3h; Product distribution; dependence of the yield of the alkylation products on temperature, on the concentration of reagent, on the reaction time; | A 33.8% B 46.5% C 2.7% D 0.7% E n/a |
1-methyl-1-phenylethyl alcohol
methoxybenzene
A
2,4-diphenyl-4-methyl-pent-1-ene
B
1-(2-(4-methoxyphenyl)propan-2-yl)benzene
Conditions | Yield |
---|---|
With phosphoric acid at 90℃; | A 31% B 21% |
Conditions | Yield |
---|---|
With oxygen; phosphorus trichloride |
isopropenylbenzene
A
2,4-diphenyl-4-methyl-pent-1-ene
B
N-(2-Phenyl-2-propenyl)-ethylcarbamat
Conditions | Yield |
---|---|
With ethyl N-{[(4-nitrobenzene)sulfonyl]oxy}carbamate In dichloromethane |
1-methyl-1-phenylethyl alcohol
A
2,4-diphenyl-4-methyl-pent-1-ene
B
acetophenone
Conditions | Yield |
---|---|
With xenon difluoride |
Dimethoxymethane
isopropenylbenzene
A
2,4-diphenyl-4-methyl-pent-1-ene
B
4-methyl-2,4-diphenylpent-2-ene
C
1,3-dimethoxy-3-phenylbutane
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate at 25℃; for 0.5h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
With boron trifluoride diethyl etherate at 25℃; for 0.5h; Yield given. Yields of byproduct given; |
isopropenylbenzene
A
1,1,3-trimethyl-3-phenylindane
B
2,4-diphenyl-4-methyl-pent-1-ene
C
(E)-(4-methylpent-2-ene-2,4-diyl)dibenzene
Conditions | Yield |
---|---|
aluminum oxide; titanium(IV) oxide at 30℃; for 90h; Product distribution; Mechanism; variation of catalysts and reaction time; | |
With hydrogenchloride In cyclohexane; water at 170℃; for 12h; investigation of H-D exchange of styrenes in dilute acid at elevated temperatures; deuterium content not efficient; | |
With hydrogenchloride In cyclohexane; water at 170℃; for 12h; | A 3.7 % Chromat. B 31.7 % Chromat. C 32.6 % Chromat. |
isopropenylbenzene
A
2,4-diphenyl-4-methyl-pent-1-ene
B
(E)-(4-methylpent-2-ene-2,4-diyl)dibenzene
Conditions | Yield |
---|---|
aluminum oxide; titanium(IV) oxide at 30℃; for 90h; Yield given; | |
With In(OSO2CF3)3; 1,3-bis-(diphenylphosphino)propane; palladium diacetate In 1,4-dioxane at 20℃; for 3h; Title compound not separated from byproducts; | |
With [η5-C5Me5Ru(μ-SMe)2Ru(OH2)-η5-C5Me5](OTf)2 In 1,2-dichloro-ethane at 60℃; for 20h; Inert atmosphere; |
isopropenylbenzene
A
2,4-diphenyl-4-methyl-pent-1-ene
B
4-methyl-2,4-diphenylpent-2-ene
Conditions | Yield |
---|---|
With silica gel at 25℃; | |
With tris(2,4-dibromophenyl)aminium hexachloroantimonate In acetonitrile | A 0.112 g B n/a |
With mordenite at 30℃; for 2h; |
isopropenylbenzene
A
(3,3-dimethylbut-1-ene-1,1-diyl)dibenzene
B
1,1,3-trimethyl-3-phenylindane
C
2,4-diphenyl-2-methylpentane
D
2,4-diphenyl-4-methyl-pent-1-ene
E
4-methyl-2,4-diphenylpent-2-ene
Conditions | Yield |
---|---|
With monoaluminum phosphate; zinc(II) tetrahydroborate In 1,2-dimethoxyethane for 1.5h; Product distribution; Ambient temperature; other reagents; product selectivity; |
isopropenylbenzene
A
(3,3-dimethylbut-1-ene-1,1-diyl)dibenzene
B
1,1,3-trimethyl-3-phenylindane
C
2,4-diphenyl-4-methyl-pent-1-ene
D
4-methyl-2,4-diphenylpent-2-ene
Conditions | Yield |
---|---|
With monoaluminum phosphate In 1,2-dimethoxyethane for 1.5h; Product distribution; Mechanism; Ambient temperature; other reagents; product selectivity; |
isopropenylbenzene
A
1,1,3-trimethyl-3-phenylindane
B
2,4-diphenyl-4-methyl-pent-1-ene
Conditions | Yield |
---|---|
In toluene at 60℃; Dimerization; Intramolecular Friedel-Crafts reaction; |
isopropenylbenzene
A
1,1,3-trimethyl-3-phenylindane
B
2,4-diphenyl-4-methyl-pent-1-ene
C
(E)-(4-methylpent-2-ene-2,4-diyl)dibenzene
Conditions | Yield |
---|---|
Zeolite Y In dichloromethane at 25 - 40℃; Product distribution; Further Variations:; Catalysts; oligomerization; |
1-methyl-1-phenylethyl alcohol
A
1,1,3-trimethyl-3-phenylindane
B
2,4-diphenyl-4-methyl-pent-1-ene
Conditions | Yield |
---|---|
iodine at 70℃; for 0.0833333h; |
1-methyl-1-phenylethyl alcohol
A
2,4-diphenyl-4-methyl-pent-1-ene
B
(E)-(4-methylpent-2-ene-2,4-diyl)dibenzene
Conditions | Yield |
---|---|
With 2,4-dinitrobenzenesulfonic acid hydrate In acetonitrile at 80℃; for 12h; Title compound not separated from byproducts.; |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: diethyl ether 2: p-toluenesulfonic acid / benzene 3: 90 percent / InBr3 / CH2Cl2 / 2 h / 0 °C View Scheme |
2,4-diphenyl-4-methyl-pent-1-ene
2,4-diphenyl-2-methylpentane
Conditions | Yield |
---|---|
With hydrogen; polymer incarcerated palladium In tetrahydrofuran at 20℃; for 1h; | 100% |
With hydrogen; polymer incarcerated platinum In tetrahydrofuran at 20℃; for 1h; atmospheric pressure; | 100% |
With hydrogen; micro-encapsulated PI palladium catalyst In tetrahydrofuran at 20℃; for 0.0833333h; Product distribution / selectivity; | 100% |
Conditions | Yield |
---|---|
With 1,3-bis(tert-butyl(pyridin-2-yl)phosphanyl)propane; palladium(II) acetylacetonate; toluene-4-sulfonic acid for 20h; Sealed tube; Inert atmosphere; Autoclave; | 95% |
2,4-diphenyl-4-methyl-pent-1-ene
3-methyl-1,3-ddiphenylbutan-1-one
Conditions | Yield |
---|---|
Stage #1: 2,4-diphenyl-4-methyl-pent-1-ene With ozone In methanol at 25℃; Stage #2: With sodium tetrahydroborate In methanol at 25℃; | 90% |
With ozone In methanol at 20℃; for 3.63333h; | 88% |
With bismuth vanadate; oxygen In water at 20℃; Irradiation; | 80% |
2,4-diphenyl-4-methyl-pent-1-ene
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
Conditions | Yield |
---|---|
With tetrakis(trimethylphosphine)iron(0); norbornene In hexane at 50℃; for 18h; stereoselective reaction; | 84% |
2,4-diphenyl-4-methyl-pent-1-ene
(trifluoromethyl)trimethylsilane
(2,2-difluoro-1-(2-methyl-2-phenylpropyl)cyclopropyl)benzene
Conditions | Yield |
---|---|
With sodium iodide In tetrahydrofuran at 65℃; for 2h; Inert atmosphere; | 83% |
diethyl bromomethylmalonate
2,4-diphenyl-4-methyl-pent-1-ene
diethyl 2-(2-phenyl-2-propenyl)-2-methylmalonate
Conditions | Yield |
---|---|
With pentamethylcyclopentadienyl bis(triphenylphosphine)ruthenium(II) chloride; N-ethyl-N,N-diisopropylamine In tetrahydrofuran at 100℃; for 24h; Inert atmosphere; | 76% |
Conditions | Yield |
---|---|
With copper(l) iodide; tris[(2-pyridylmethyl)amine]; N-ethyl-N,N-diisopropylamine In 1,2-dimethoxyethane; acetonitrile at 100℃; for 20h; Catalytic behavior; Inert atmosphere; | 73% |
methanol
carbon monoxide
2,4-diphenyl-4-methyl-pent-1-ene
methyl (E)-5-methyl-3,5-diphenyl-3-hexenoate
Conditions | Yield |
---|---|
With palladium diacetate; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile at 50℃; under 760.051 Torr; for 24h; regioselective reaction; | 68% |
Conditions | Yield |
---|---|
With Selectfluor In 1,2-dichloro-ethane at 20℃; for 12h; regioselective reaction; | 66% |
(4-methoxybenzoyl)(pyridin-1-ium-1-yl)amide
2,4-diphenyl-4-methyl-pent-1-ene
Conditions | Yield |
---|---|
Stage #1: (4-methoxybenzoyl)(pyridin-1-ium-1-yl)amide; 2,4-diphenyl-4-methyl-pent-1-ene With 9-mesityl-2,7-dimethyl-10-phenylacridin-10-ium tetrafluoroborate In dichloromethane for 0.00277778h; Sonication; Sealed tube; Inert atmosphere; Green chemistry; Stage #2: In dichloromethane at 20℃; for 22h; Irradiation; Sealed tube; Inert atmosphere; Green chemistry; | 63% |
2,4-diphenyl-4-methyl-pent-1-ene
N-((fluoromethyl)(oxo)(phenyl)-λ6-sulfaneylidene)-4-methylbenzenesulfonamide
Conditions | Yield |
---|---|
With 1,4-bis(diphenylamino)naphthalene; water In acetone at 20℃; for 18h; Irradiation; | 61% |
2,4-diphenyl-4-methyl-pent-1-ene
N-methyl-2-iodoaniline
Conditions | Yield |
---|---|
With dipotassium hydrogenphosphate In dimethyl sulfoxide at 20℃; Inert atmosphere; UV-irradiation; Green chemistry; regioselective reaction; | 61% |
Conditions | Yield |
---|---|
With 2-Adamantanone In para-xylene at 130℃; under 760.051 Torr; for 20h; Inert atmosphere; regioselective reaction; | A 60% B 87 %Spectr. |
Conditions | Yield |
---|---|
With dimethyl sulfoxide; potassium hydroxide at 120℃; for 24h; | 60% |
Conditions | Yield |
---|---|
With 1-hydroxytetraphenylcyclopentadienyl(tetraphenyl-2,4-cyclopentadien-1-one)-μ-hydrotetracarbonyldiruthenium(II); dicarbonylacetylacetonatorhodium(I); tris[(R)-2’-(benzyloxy)-1,1’-binaphthyl-2-yl]phosphite; hydrogen In toluene at 120℃; under 30003 Torr; for 20h; Autoclave; | A 43% B 54% |
Conditions | Yield |
---|---|
With 2-Adamantanone In para-xylene at 130℃; under 760.051 Torr; for 64h; Inert atmosphere; regioselective reaction; | 48% |
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