As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiry1H-Indene,2,3-dihydro-1,1,3-trimethyl-3-phenyl- 1-PHENYL-1,3,3-TRIMETHYLINDAN Basic information Product Name: 1-PHENYL-1,3,3-TRIMETHYLINDAN Synonyms: 1-PHENYL-1,3,3-TRIMETHYLINDAN;
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryAbout Product Details CAS: 3910-35-8 MF: C18H20
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquirygood quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg,customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran
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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:beige crystalline powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use
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1-Phenyl-1,3,3-trimethylindan cas 3910-35-8Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiry1. Timely and efficient service to ensure communication with customers2. Produce products of different specifications and sizes according to your requirements.3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures sta
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inquiry3910-35-8 Application:intermediate
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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Raw material ,higher purity, support by origional factory, fully large stock Basic information Product Name: 1-PHENYL-1,3,3-TRIMETHYLINDAN Synonyms: 1-Phenyl-1,3,3-trimethylindane;1,1,3-trimethyl-3-phenyl-2H-indene;1,3,3-TriMethyl-1-Phenyl
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inquiry1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
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inquiryConditions | Yield |
---|---|
iodine at 70℃; for 0.25h; | 100% |
With phosphotungstic acid In chloroform at 60℃; for 1.5h; | 99% |
With trifluoroacetic acid In dichloromethane | 96% |
Conditions | Yield |
---|---|
With zinc diacetate In dichloromethane for 2h; Ambient temperature; | 99% |
Multi-step reaction with 2 steps 1: CD2Cl2 / -80 °C View Scheme |
Conditions | Yield |
---|---|
With Ce3+-montmorillonite In toluene at 25℃; for 1h; | 99% |
isopropenylbenzene
A
1,1,3-trimethyl-3-phenylindane
B
2,4-diphenyl-4-methyl-pent-1-ene
C
4-methyl-2,4-diphenylpent-2-ene
Conditions | Yield |
---|---|
thiol-modified Al-loaded mesoporous silica In toluene at 120℃; for 2h; | A 97.1% B 0.7% C 1% |
thiol-modified Al-loaded mesoporous silica In toluene at 80℃; for 2h; | A 37.5% B 16.9% C 42.8% |
nafion resin; silica gel In various solvent(s) at 50℃; under 760 Torr; Product distribution; Rate constant; var. soluble liquid acids and resin-based solid acids as catalysts; var. time and solv.; |
Conditions | Yield |
---|---|
In toluene at 120℃; for 24h; Schlenk technique; Inert atmosphere; | 96% |
Conditions | Yield |
---|---|
iodine at 70℃; for 3h; | 91% |
With bismuth(III) bromide In 1,2-dichloro-ethane at 50℃; for 4h; Inert atmosphere; | 82% |
With 0.00044 wt% platinum nanoparticle supported on titanium oxide encapsulated in sulfated p-xylene polymer In nitromethane at 75℃; Irradiation; Inert atmosphere; | 76% |
Conditions | Yield |
---|---|
With nitrosonium hexachloroantimonate In dichloromethane at 23℃; for 12h; Mechanism; Quantum yield; Product distribution; Irradiation; other solvent; other reactant; without irradiation; | A 90% B 2% |
With nitrosonium hexachloroantimonate In dichloromethane at 23℃; for 12h; Irradiation; | A 90% B 2% |
2-methyl-2-phenylpropionic acid
A
1,1,3-trimethyl-3-phenylindane
B
carbon monoxide
Conditions | Yield |
---|---|
With tungsten(VI) chloride In dichloromethane at 20℃; for 168h; Inert atmosphere; Schlenk technique; | A 88% B n/a |
ethyl 3-phenylbut-2-enoate
1,1,3-trimethyl-3-phenylindane
Conditions | Yield |
---|---|
With trifluoroacetic acid at 80℃; for 24h; Reagent/catalyst; Temperature; Schlenk technique; Inert atmosphere; | 86% |
3-phenylbut-2-enoic acid
1,1,3-trimethyl-3-phenylindane
Conditions | Yield |
---|---|
With trifluoroacetic acid at 80℃; for 24h; Inert atmosphere; | 84% |
diethyl α-(1-methyl-1-phenylethyl)malonate
1,1,3-trimethyl-3-phenylindane
Conditions | Yield |
---|---|
With phosphoric acid at 90℃; for 1h; | 83% |
ethyl (Z)-3-phenylbut-2-enoate
1,1,3-trimethyl-3-phenylindane
Conditions | Yield |
---|---|
With trifluoroacetic acid at 80℃; for 24h; Schlenk technique; Inert atmosphere; | 82% |
Conditions | Yield |
---|---|
zinc(II) chloride at 50℃; for 4h; | 80% |
Conditions | Yield |
---|---|
With PPA at 90℃; for 1h; | 80% |
2-cyano-3-methyl-3-phenyl-butyric acid ethyl ester
1,1,3-trimethyl-3-phenylindane
Conditions | Yield |
---|---|
With PPA at 90℃; for 2h; | 78% |
1-methyl-1-phenylethyl alcohol
A
1,1,3-trimethyl-3-phenylindane
B
2,4-diphenyl-4-methyl-pent-1-ene
C
1,1-dimethyl-3-(2-methyl-2-phenylpropyl)-3-phenyl-2,3-dihydro-1H-indene
Conditions | Yield |
---|---|
With iron(III) chloride; 1,1,1,3',3',3'-hexafluoro-propanol; nitric acid at 20℃; for 3h; Catalytic behavior; | A 7 %Spectr. B 62% C 9 %Spectr. |
trimethylaluminum
dimethylaluminum chloride
acetophenone
A
1,1,3-trimethyl-3-phenylindane
B
isopropenylbenzene
Conditions | Yield |
---|---|
In toluene at 120℃; for 24h; Schlenk technique; Inert atmosphere; | A 34% B 57% |
1-methyl-1-phenylethyl alcohol
A
1,1,3-trimethyl-3-phenylindane
B
1,1-dimethyl-3-(2-methyl-2-phenylpropyl)-3-phenyl-2,3-dihydro-1H-indene
Conditions | Yield |
---|---|
With iron(III) chloride; 1,1,1,3',3',3'-hexafluoro-propanol; nitric acid at 20℃; for 3h; Catalytic behavior; | A 57% B 18% |
2,2-dimethyl-5-(1-methyl-1-phenylethyl)-1,3-dioxane-4,6-dione
A
1,1,3-trimethyl-3-phenylindane
B
3-methyl-3-phenylbutanoic acid
Conditions | Yield |
---|---|
With PPA at 90℃; for 2h; | A 52% B 26% |
Conditions | Yield |
---|---|
toluene-4-sulfonic acid In benzene for 18h; Heating; | 42% |
trimethylsilyl isothiocyanate
isopropenylbenzene
A
1,1,3-trimethyl-3-phenylindane
B
(1-isothiocyanato-1-methyl-ethyl)-benzene
Conditions | Yield |
---|---|
With iodine In dichloromethane | A 27% B 27% |
methoxybenzene
isopropenylbenzene
A
1,1,3-trimethyl-3-phenylindane
B
1-(2-(4-methoxyphenyl)propan-2-yl)benzene
Conditions | Yield |
---|---|
With C16H22AuClN2; potassium tetrakis(pentafluorophenyl)borate In benzene at 20℃; for 16h; Inert atmosphere; Schlenk technique; Sealed tube; | A 7% B 25% |
2-hydroxy-2-methyl-4.4-diphenyl-pentane
1,1,3-trimethyl-3-phenylindane
Conditions | Yield |
---|---|
With hydrogenchloride; tin(IV) chloride; benzene |
1,1,3-trimethyl-3-phenylindane
Conditions | Yield |
---|---|
With sulfuric acid |
Conditions | Yield |
---|---|
at 130 - 150℃; for 24h; |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In benzene for 1.5h; Ambient temperature; | 0.98 g |
With bismuth(III) bromide In 1,2-dichloro-ethane at 50℃; Inert atmosphere; |
azocumene
A
Isopropylbenzene
B
dicumene
C
1,1,3-trimethyl-3-phenylindane
D
p-cumylcumene
E
2-(Isopropyl-phenyl)-2-phenyl-propan
F
isopropenylbenzene
Conditions | Yield |
---|---|
With silica surface at 55℃; Kinetics; Mechanism; Rate constant; energy data (ΔH(excit.), ΔS(excit.)); also photolysis at 25 deg C; labeling studies; |
2-nitropropane
benzene
A
Isopropylbenzene
B
1,1,3-trimethylindene
C
1,1,3-trimethyl-3-phenylindane
D
2,2-diphenylpropane
E
3,3,3',3'-tetramethyl-1,1'-spiro-biindane
F
1',3,3,3',3'-pentamethyl-1-(1'-indanyl-methylene)-indane
Conditions | Yield |
---|---|
With aluminium trichloride Product distribution; Mechanism; 2 h, room temp., 55 deg C, various periods of time; |
isopropenylbenzene
A
1,1,3-trimethyl-3-phenylindane
B
2,4-diphenyl-4-methyl-pent-1-ene
C
(E)-(4-methylpent-2-ene-2,4-diyl)dibenzene
Conditions | Yield |
---|---|
aluminum oxide; titanium(IV) oxide at 30℃; for 90h; Product distribution; Mechanism; variation of catalysts and reaction time; | |
With hydrogenchloride In cyclohexane; water at 170℃; for 12h; investigation of H-D exchange of styrenes in dilute acid at elevated temperatures; deuterium content not efficient; | |
With hydrogenchloride In cyclohexane; water at 170℃; for 12h; | A 3.7 % Chromat. B 31.7 % Chromat. C 32.6 % Chromat. |
isopropenylbenzene
A
1,1,3-trimethyl-3-phenylindane
B
1-phenyl-3-(2-phenyl-2-methylpropyl)-1,3-dimethylindan
Conditions | Yield |
---|---|
x In nitromethane at 25℃; for 0.0833333h; Yield given; | |
(BF4)2 In nitromethane at 25℃; for 1h; Yield given; |
1,1,3-trimethyl-3-phenylindane
1,3,3-trimethyl-5-nitro-1-(4-nitrophenyl)-2,3-dihydro-1H-indene
Conditions | Yield |
---|---|
With sulfuric acid; nitric acid In dichloromethane at 0 - 5℃; | 83% |
1,1,3-trimethyl-3-phenylindane
A
1,3,3-trimethyl-5-nitro-1-(4-nitrophenyl)-2,3-dihydro-1H-indene
B
1,3,3-trimethyl-6-nitro-1-(4-nitrophenyl)-2,3-dihydro-1H-indene
Conditions | Yield |
---|---|
With nitric acid at 60℃; for 6h; Reagent/catalyst; Temperature; Autoclave; Overall yield = 88.7 percent; | A 31% B 69% |
With sulfuric acid; nitric acid In chloroform at 2 - 8℃; Temperature; Overall yield = 77.3 %; Overall yield = 25.2 g; | A 16.8 g B 8.4 g |
1,1,3-trimethyl-3-phenylindane
B
6-amino-1-(4'-aminophenyl)-1,3,3-trimethylindane
Conditions | Yield |
---|---|
Stage #1: 1,1,3-trimethyl-3-phenylindane With nitric acid at 60℃; for 6h; Stage #2: With palladium 10% on activated carbon; hydrogen at 70℃; under 12001.2 - 15001.5 Torr; for 8h; Reagent/catalyst; Temperature; Pressure; Overall yield = 84 percent; | A 31% B 69% |
1,1,3-trimethyl-3-phenylindane
3,3,3',3'-tetramethyl-1,1'-spiro-biindane
Conditions | Yield |
---|---|
With aluminium trichloride |
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