high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:640-19-7
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With ammonia In dichloromethane at 25℃; for 10h; Solvent; Temperature; | 99.3% |
With diethyl ether; ammonia |
Conditions | Yield |
---|---|
With potassium fluoride In water at 116℃; for 3h; | 94% |
With potassium fluoride In para-xylene at 100 - 120℃; for 20h; Inert atmosphere; Schlenk technique; | 67% |
With potassium fluoride; xylene |
α-fluoro-N-bromoacetamide
A
fluoroacetamide
N-((1S,2R)-2-Bromo-cyclohexyl)-2-fluoro-acetamide
N-((1S,2S)-2-Bromo-cyclohexyl)-2-fluoro-acetamide
Conditions | Yield |
---|---|
With cyclohexene In dichloromethane at 15 - 20℃; for 1.5h; Irradiation; Yields of byproduct given; | A 30% B n/a C n/a |
α-fluoro-N-bromoacetamide
cyclohexene
A
fluoroacetamide
N-((1S,2R)-2-Bromo-cyclohexyl)-2-fluoro-acetamide
N-((1S,2S)-2-Bromo-cyclohexyl)-2-fluoro-acetamide
Conditions | Yield |
---|---|
In dichloromethane at 15 - 20℃; for 1.5h; Irradiation; Yield given. Yields of byproduct given; | A 30% B n/a C n/a |
N-Chloro-2-fluoroacetamid
A
fluoroacetamide
N-((1S,2R)-2-Chloro-cyclohexyl)-2-fluoro-acetamide
N-((1S,2S)-2-Chloro-cyclohexyl)-2-fluoro-acetamide
Conditions | Yield |
---|---|
With cyclohexene In dichloromethane at 15 - 20℃; for 2.5h; Irradiation; Yields of byproduct given; | A 7% B n/a C n/a |
N-Chloro-2-fluoroacetamid
cyclohexene
A
fluoroacetamide
N-((1S,2R)-2-Chloro-cyclohexyl)-2-fluoro-acetamide
N-((1S,2S)-2-Chloro-cyclohexyl)-2-fluoro-acetamide
Conditions | Yield |
---|---|
In dichloromethane at 15 - 20℃; for 2.5h; Irradiation; Yield given. Yields of byproduct given; | A 7% B n/a C n/a |
Conditions | Yield |
---|---|
With ammonia; water |
Conditions | Yield |
---|---|
With ammonia; water |
Conditions | Yield |
---|---|
(i) HF, Et2O, (ii) NH3, MeOH; Multistep reaction; |
Conditions | Yield |
---|---|
(i) HCl, Et2O, (ii) H2O; Multistep reaction; |
fluoroacetamide
Conditions | Yield |
---|---|
With potassium fluoride at 140 - 200℃; under 20 Torr; |
fluoroacetamide
Conditions | Yield |
---|---|
With potassium fluoride at 250℃; |
Conditions | Yield |
---|---|
at 140 - 200℃; under 20 Torr; |
Conditions | Yield |
---|---|
With copper(l) iodide; cesium fluoride; N,N`-dimethylethylenediamine In tetrahydrofuran at 25℃; for 18 - 24h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With phosphorus pentoxide at 110 - 150℃; Reagent/catalyst; | 82% |
With phosphorus pentachloride; xylene | |
With phosphorus pentoxide at 160℃; |
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; | 82% |
fluoroacetamide
2-fluorothioacetamide
Conditions | Yield |
---|---|
With Lawessons reagent In N,N,N,N,N,N-hexamethylphosphoric triamide at 80℃; for 4h; | 78% |
3-phenyl-propionaldehyde
fluoroacetamide
Benzenesulfinic acid
N-(1-benzenesulfonyl-3-phenyl-propyl)-2-fluoro-acetamide
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; | 73% |
Conditions | Yield |
---|---|
72% | |
With sulfuric acid at 95℃; |
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; | 70% |
Conditions | Yield |
---|---|
With magnesium sulfate In dichloromethane at 20℃; | 69% |
Conditions | Yield |
---|---|
at 80 - 89℃; | 65% |
Triallylborane
fluoroacetamide
4-(fluoromethyl)-1,6-heptadien-4-amine
Conditions | Yield |
---|---|
Stage #1: Triallylborane; fluoroacetamide In tetrahydrofuran for 1.5h; Reflux; Stage #2: With water; sodium hydroxide In methanol | 54% |
Stage #1: Triallylborane; fluoroacetamide In tetrahydrofuran at 65℃; Inert atmosphere; Stage #2: With methanol Stage #3: With sodium hydroxide | 54% |
Conditions | Yield |
---|---|
With sulfuric acid In acetic acid at 20℃; for 18h; | A n/a B 38% |
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