CAS No.6485-57-0,2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone Suppliers

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2,5-Cyclohexadien-1-one,2,6-bis(1,1-dimethylethyl)-4-hydroperoxy-4-methyl-

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Qingdao Beluga Import and Export Co., LTD

2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone CAS:6485-57-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, s

2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone CAS:6485-57-0

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2,5-Cyclohexadien-1-one,2,6-bis(1,1-dimethylethyl)-4-hydroperoxy-4-methyl-

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Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

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Hangzhou Fandachem Co.,Ltd

2,6-DI-TERT-BUTYL-4-HYDROPEROXY-4-METHYL-2,5-CYCLOHEXADIENONEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

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2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

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Nanjing Raymon Biotech Co., Ltd.

2,5-Cyclohexadien-1-one,2,6-bis(1,1-dimethylethyl)-4-hydroperoxy-4-methyl-Appearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical i

2,5-Cyclohexadien-1-one,2,6-bis(1,1-dimethylethyl)-4-hydroperoxy-4-methyl-

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Synthetic route

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions

Conditions	Yield
With methylene blue In methanol; water under 7500.75 Torr; for 0.266667h; Irradiation; Flow reactor;	99%
With 2,8-dibromo-5,5-difluoro-1,3,7,9-tetramethyl-10-phenyl-5H-dipyrrolo[1,2-c:2′,1′-f ][1,3,2]diazaborinin-4-ium-5-uide; oxygen In 1,4-dioxane for 6h; Irradiation;	95%
With potassium hydroxide; oxygen

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

A: 52922-83-5
1,3-di-tert-butyl-5-hydroxy-5-methyl-7-oxabicyclo[4.1.0]hept-3-en-2-one

B: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions

Conditions	Yield
With (3-)*3Et4N(1+); oxygen In N,N-dimethyl-formamide at 0℃; for 2h;	A 9% B 91%

: 67-56-1
methanol

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

: 93-55-0
1-phenyl-propan-1-one

A: 16735-22-1
3-hydroxy-2-methylpropiophenone

B: 10396-80-2
2,6-di-tert-butyl-4-hydroxy-4-methylcyclohexa-2,5-dienone

C: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions

Conditions	Yield
With 4,5,6,7-tetrachloro-2',4',5',7'-tetraiodofluorescein disodium salt; potassium carbonate In water at 20℃; for 36h; Irradiation;	A 12% B 60% C 17%

...Expand

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

A: 10396-80-2
2,6-di-tert-butyl-4-hydroxy-4-methylcyclohexa-2,5-dienone

B: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions

Conditions	Yield
With 1-([1,1'-biphenyl]-2-yl)propan-1-one; oxygen; rose bengal; potassium carbonate at 20℃; for 34h; Irradiation;	A 57% B 18%
With 9,10-Dicyanoanthracene; oxygen In acetonitrile for 55h; Rate constant; Product distribution; Mechanism; Irradiation;
With 9,10-Dicyanoanthracene; oxygen In acetonitrile for 55h; Irradiation; Yield given. Yields of byproduct given;

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

: 137-07-5
2-amino-benzenethiol

: 611-73-4
Benzoylformic acid

A: 883-93-2
2-Phenylbenzothiazole

B: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

C: C29H33NO3S

Conditions

Conditions	Yield
With dihydrogen peroxide In 1,4-dioxane; water at 20℃; for 8h; Irradiation;	A 38% B n/a C n/a

...Expand

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

A: 719-22-2
2,6-Di-tert-butyl-1,4-benzoquinone

B: 10396-80-2
2,6-di-tert-butyl-4-hydroxy-4-methylcyclohexa-2,5-dienone

C: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions

Conditions	Yield
With dihydrogen peroxide; phosphomolybdic acid In acetic acid at 30℃; for 5h; Product distribution; other heteropolyacids as catalyst;	A 4.1% B 1.7% C 34.1%

...Expand

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

A: 719-22-2
2,6-Di-tert-butyl-1,4-benzoquinone

B: 2455-14-3
3,5,3',5'-tetra-tert-butyl-4,4'-diphenoquinone

C: 10396-80-2
2,6-di-tert-butyl-4-hydroxy-4-methylcyclohexa-2,5-dienone

D: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

E: 14387-13-4
2,6-di-tert-butyl-4-(3,5-di-tert-butyl-4-hydroxyphenyl)-4-methyl-2,5-cyclohexadiene-1-one

F: 1620-98-0
3,5-di-t-butyl-4-hydroxybenzaldehyde

Conditions

Conditions	Yield
With ammonia; oxygen In propan-1-ol; water at 88℃; for 1h; Product distribution; oth. time, oth. temperature;	A 3.5% B 2.1% C 14% D 17% E 8.8% F 1.5%

...Expand

: 6858-01-1, 24473-56-1
2,6-di-tert-butyl-4-methylphenoxy radical

A: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

B: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions

Conditions	Yield
With C5CoN5O2(3-)*3C36H30NP2(1+) In dichloromethane at -70℃; for 0.0833333h; starting material added in dimer form; Title compound not separated from byproducts;	A 30 % Chromat. B 70 % Chromat.

: 62926-71-0
Ethaneperoxoic acid 3,5-di-tert-butyl-1-methyl-4-oxo-cyclohexa-2,5-dienyl ester

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions

Conditions	Yield
With trifluoroacetic acid In methanol

: 99-65-0
meta-dinitrobenzene

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

oxygen: oxygen

aq.-ethanolic KOH: aq.-ethanolic KOH

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions

Conditions	Yield
at -10 - 40℃; Rate constant;

...Expand

: 61077-25-6
2,4,6-tri-tert-butyl-6-hydroperoxy-cyclohexa-2,4-dienone

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

oxygen: oxygen

aq.-ethanolic KOH: aq.-ethanolic KOH

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions

Conditions	Yield
at -10 - 40℃; Rate constant;

...Expand

: 527-17-3, 70128-24-4
Duroquinone

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

oxygen: oxygen

aq.-ethanolic KOH: aq.-ethanolic KOH

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions

Conditions	Yield
at -10 - 40℃; Rate constant;

...Expand

: 719-22-2
2,6-Di-tert-butyl-1,4-benzoquinone

: 128-37-0
2,6-di-tert-butyl-4-methyl-phenol

oxygen: oxygen

aq.-ethanolic KOH: aq.-ethanolic KOH

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

Conditions

Conditions	Yield
at -10 - 40℃; Rate constant;

...Expand

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

: 10396-80-2
2,6-di-tert-butyl-4-hydroxy-4-methylcyclohexa-2,5-dienone

Conditions

Conditions	Yield
With triphenylphosphine In dichloromethane for 3h; Heating;	100%
With sodium thiosulfate In methanol; water at 20℃;	99%
With sodium hydrogensulfite In water; acetonitrile for 0.0333333h;	90%

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

: 40056-43-7
3,5-di-tert-butyl-4-hydroxybenzoyl chloride

: 69901-39-9
1-methyl-3,5-di-tert-butyl-4-oxo-2,5-cyclohexadienyl 3,5-di-tert-butyl-4-hydroxyperbenzoate

Conditions

Conditions	Yield
With pyridine In Petroleum ether at -20℃; for 1h;	74%

: 19487-11-7
2,6-di-tert-butyl-4-chloro-4-methylcyclohexa-2,5-dien-1-one

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

: 51033-92-2
bis(1-methyl-3,5-di-tert-butyl-4-oxo-cyclohexa-2,5-dienyl) peroxide

Conditions

Conditions	Yield
With N-iodo-succinimide In acetonitrile at 35℃; for 0.0833333h;	74%
With N-iodo-succinimide In acetonitrile at 35℃; for 0.5h; Product distribution; other reagent, solvent, reaction time;	58%

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

A: 1516-94-5
1,2-bis(3,5-di-tert-butyl-4-hydroxyphenyl)ethane

B: 10396-80-2
2,6-di-tert-butyl-4-hydroxy-4-methylcyclohexa-2,5-dienone

Conditions

Conditions	Yield
With copper dichloride In acetonitrile at 20℃; for 1h;	A 70% B 28%
With copper dichloride In acetonitrile at 20℃; for 1h; Mechanism; decomposition in presence of Cu(I)Cl is also investigated;	A 70% B 28%

: 1988-75-6
4-bromo-2,4,6-tri-tert-butyl-2,5-cyclohexadiene-1-one

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

: C33H52O4

Conditions

Conditions	Yield
With N-iodo-succinimide In acetonitrile at 35℃; for 0.166667h;	58%

: 1669-36-9
4-bromo-4-methyl-2,6-di-tert-butylcyclohexa-2,5-dienone

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

: 51033-92-2
bis(1-methyl-3,5-di-tert-butyl-4-oxo-cyclohexa-2,5-dienyl) peroxide

Conditions

Conditions	Yield
With N-iodo-succinimide In acetonitrile at 35℃; for 0.0833333h;	57%

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

A: 66483-14-5
2,4-ditertiobutyl-2-(2-oxo-propyl)-2,3-dihydro-furan-3-one

B: 10396-80-2
2,6-di-tert-butyl-4-hydroxy-4-methylcyclohexa-2,5-dienone

C: 3,5-Di-tert-butyl-7-(1,5-di-tert-butyl-3-methyl-6-oxo-cyclohexa-2,4-dienyl)-7-methyl-7H-oxepin-4-one

Conditions

Conditions	Yield
With copper(l) iodide In acetonitrile at 20℃; for 1h;	A 47% B 33% C 20%

...Expand

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

: 75-65-0
tert-butyl alcohol

: 13154-57-9
2,6-di-tert-butyl-4-(tert-butylperoxy)-4-methylcyclohexa-2,5-dien-1-one

Conditions

Conditions	Yield
With sulfuric acid

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

: 79-03-8
propionyl chloride

: 62926-75-4
Propaneperoxoic acid 3,5-di-tert-butyl-1-methyl-4-oxo-cyclohexa-2,5-dienyl ester

Conditions

Conditions	Yield
With pyridine In Petroleum ether 1.) 30 min, 0 deg C, 2.) 2 h, room temp.;

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

: 3282-30-2
pivaloyl chloride

: 87100-48-9
2,2-Dimethyl-propaneperoxoic acid 3,5-di-tert-butyl-1-methyl-4-oxo-cyclohexa-2,5-dienyl ester

Conditions

Conditions	Yield
With pyridine In Petroleum ether 1.) 30 min, 0 deg C, 2.) 2 h, room temp.;

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

: 98-88-4
benzoyl chloride

: 62926-77-6
Benzenecarboperoxoic acid 3,5-di-tert-butyl-1-methyl-4-oxo-cyclohexa-2,5-dienyl ester

Conditions

Conditions	Yield
With pyridine In Petroleum ether 1.) 30 min, 0 deg C, 2.) 2 h, room temp.;

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

: 75-36-5
acetyl chloride

: 62926-71-0
Ethaneperoxoic acid 3,5-di-tert-butyl-1-methyl-4-oxo-cyclohexa-2,5-dienyl ester

Conditions

Conditions	Yield
With pyridine In Petroleum ether 1.) 30 min, 0 deg C, 2.) 2 h, room temp.;

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

: 79-30-1
isobutyryl chloride

: 62955-68-4
2-Methyl-propaneperoxoic acid 3,5-di-tert-butyl-1-methyl-4-oxo-cyclohexa-2,5-dienyl ester

Conditions

Conditions	Yield
With pyridine In Petroleum ether 1.) 30 min, 0 deg C, 2.) 2 h, room temp.;

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

: 103-80-0
phenylacetyl chloride

: 62926-76-5
Phenyl-ethaneperoxoic acid 3,5-di-tert-butyl-1-methyl-4-oxo-cyclohexa-2,5-dienyl ester

Conditions

Conditions	Yield
With pyridine In Petroleum ether 1.) 30 min, 0 deg C, 2.) 2 h, room temp.;

: 6485-57-0
2,6-di-tert-butyl-4-hydroperoxy-4-methyl-2,5-cyclohexadienone

: 809-73-4
3,3',5,5'-tetra-tert-butyl-4,4'-stilbenequinone

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 70 percent / Cu(II)Cl2 / acetonitrile / 1 h / 20 °C / decomposition in presence of Cu(I)Cl is also investigated 2: air View Scheme

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Antimex Chemical Limied

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