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inquiryItems Standard Result Appearance Colorless transparent liquid Complies Assay 99%min
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inquiryHigh purity Triisopropylsilane CAS 6485-79-6 with competitive price 1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; ...... Appeara
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inquiryProduct Name: Triisopropylsilane Synonyms: 1.2.3-Triisopropyliden-cyclopropan;hexamethyl<3>radialene;TIPS-H;Triisopropyliden-cyclopropan;Triisopropylsilylhydride;Tris-isopropyliden-cyclopropan;Tris-isopropylsilane;(ME2CH)3SIH CAS: 6485-79-6
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inquiryName: Triisopropylsilane Molecular Formula:C9H22Si Molecular Weight:158.36 CAS No.:6485-79-6 Appearance:Colorless To Slight Yellow Liquid Appearance:Colorless To Slight Yellow Liquid Storage: Preserve in well-closed, light-resistant and airtight
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inquiryBest price 6485-79-6 good producer Triisopropylsilane global trader first, the metal magnesium and 2-chloropropane were reacted to synthesize isopropyl magnesium chloride, and then in the presence of weak polar solvent, triisopropylsilane was pr
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inquiryProduct name: Triisopropylsilane CAS No.:6485-79-6 Molecule Formula:C9H22Si Molecule Weight:158.36 Purity: 99.0% Package: 170kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard
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inquiryConditions | Yield |
---|---|
With trichlorosilane; magnesium 1) THF, 2) 0 deg C, 3) 25 deg C, 3d; | 80% |
(i) Li, Na, PE, (ii) SiCl4; Multistep reaction; |
1,1,2,2-tetraisopropyl-1,2-dihydrodisilane
A
di-isopropylsilane
B
chlorotriisopropylsilane
Conditions | Yield |
---|---|
With sulfur at 320℃; for 8h; | A n/a B n/a C n/a D 69% |
Conditions | Yield |
---|---|
In benzine HSiCl3 and i-C3H7Li in benzine at -5°C;; | 64% |
In benzine HSiCl3 and i-C3H7Li in benzine at -5°C;; | 64% |
Conditions | Yield |
---|---|
58% |
Conditions | Yield |
---|---|
In not given | 37.5% |
In not given | 37.5% |
tri(iso-propyl)methoxysilane
chlorotriisopropylsilane
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; ethyl bromide; tetraoctyl ammonium bromide In benzene-d6 at 20℃; for 24h; | 32% |
3-phenyl-1-tri-tert-butylsilyl-1-triisopropylsilyl-1-silacyclopent-3-ene
A
chlorotriisopropylsilane
B
tri-t-butylsilane
Conditions | Yield |
---|---|
In various solvent(s) at 20℃; under 1 Torr; for 1h; Photolysis; Further byproducts.; | A 6.8% B 6.5% C 0.5% D 21.2% |
Conditions | Yield |
---|---|
With monosilane | |
With trichlorosilane; Petroleum ether |
1,1,1-trichloro-2-methyl-1-silapropane
isopropylmagnesium chloride
chlorotriisopropylsilane
Conditions | Yield |
---|---|
(i) Et2O, (ii) (heating); Multistep reaction; |
Conditions | Yield |
---|---|
Stage #1: oxirane; isopropylmagnesium chloride In tetrahydrofuran Stage #2: With tetrachlorosilane In tetrahydrofuran; toluene Heating; | A 47 % Chromat. B 15 % Chromat. |
methanol
isopropylmagnesium chloride
A
tri(iso-propyl)methoxysilane
B
chlorotriisopropylsilane
Conditions | Yield |
---|---|
Stage #1: methanol; isopropylmagnesium chloride In tetrahydrofuran at 20℃; for 1h; Stage #2: With tetrachlorosilane In tetrahydrofuran; toluene at 70 - 95℃; for 3h; | A 59 % Chromat. B 19 % Chromat. |
Stage #1: methanol With tetrachlorosilane In tetrahydrofuran at 20℃; Stage #2: isopropylmagnesium chloride In tetrahydrofuran; toluene | A 53 % Chromat. B 4 % Chromat. |
isopropylmagnesium chloride
sodium methylate
A
tri(iso-propyl)methoxysilane
B
chlorotriisopropylsilane
Conditions | Yield |
---|---|
Stage #1: isopropylmagnesium chloride; sodium methylate In tetrahydrofuran Stage #2: With tetrachlorosilane In tetrahydrofuran; toluene Heating; | A 44 % Chromat. B 29 % Chromat. |
isopropylmagnesium chloride
A
chlorotriisopropylsilane
B
Diisopropylsilyl dichloride
Conditions | Yield |
---|---|
With tetrachlorosilane In tetrahydrofuran for 4h; Heating; | A 26 % Chromat. B 68 % Chromat. |
isopropylmagnesium chloride
magnesium methanolate
A
tri(iso-propyl)methoxysilane
B
chlorotriisopropylsilane
Conditions | Yield |
---|---|
Stage #1: isopropylmagnesium chloride; magnesium methanolate In tetrahydrofuran Stage #2: With tetrachlorosilane In tetrahydrofuran; toluene Heating; | A 51 % Chromat. B 28 % Chromat. |
isopropylmagnesium chloride
isopropyl alcohol
A
chlorotriisopropylsilane
B
Me2CHOSi(CHMe2)3
Conditions | Yield |
---|---|
Stage #1: isopropylmagnesium chloride; isopropyl alcohol In tetrahydrofuran Stage #2: With tetrachlorosilane In tetrahydrofuran; toluene Heating; | A 18 % Chromat. B 39 % Chromat. |
isopropylmagnesium chloride
tert-butyl alcohol
B
chlorotriisopropylsilane
Conditions | Yield |
---|---|
Stage #1: isopropylmagnesium chloride; tert-butyl alcohol In tetrahydrofuran Stage #2: With tetrachlorosilane In tetrahydrofuran; toluene Heating; | A 7 % Chromat. B 12 % Chromat. |
isopropylmagnesium chloride
butan-1-ol
A
chlorotriisopropylsilane
B
1-(triisopropylsilyl)oxybutane
Conditions | Yield |
---|---|
Stage #1: isopropylmagnesium chloride; butan-1-ol In tetrahydrofuran Stage #2: With tetrachlorosilane In tetrahydrofuran; toluene Heating; | A 17 % Chromat. B 51 % Chromat. |
Conditions | Yield |
---|---|
Stage #1: isopropylmagnesium chloride; hexan-1-ol In tetrahydrofuran Stage #2: With tetrachlorosilane In tetrahydrofuran; toluene Heating; | A 18 % Chromat. B 41 % Chromat. |
A
chlorotriisopropylsilane
Conditions | Yield |
---|---|
In (2)H8-toluene at 50℃; for 8h; Inert atmosphere; |
Conditions | Yield |
---|---|
With hydrogen at 90℃; under 3000.3 Torr; for 8h; |
cyclohexenone
chlorotriisopropylsilane
1-triisopropylsiloxy-1-cyclohexene
Conditions | Yield |
---|---|
platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane at 100℃; for 0.25h; | 99% |
chlorotriisopropylsilane
triisopropylsilyl chloride
Conditions | Yield |
---|---|
With hexachloroethane; palladium dichloride at 20℃; for 1h; Cooling with ice; | 99% |
With iron(III) chloride; acetyl chloride In dichloromethane | 93% |
With tert-butylhypochlorite at -10℃; Chlorination; | 9.5 g |
chlorotriisopropylsilane
triisopropylsilanol
Conditions | Yield |
---|---|
With oxygen In water; acetone at 30℃; under 760.051 Torr; for 1.33333h; | 99% |
With oxygen In tetrahydrofuran; water at 20℃; under 760.051 Torr; for 0.5h; Green chemistry; | 99% |
With water In tetrahydrofuran at 25℃; for 0.35h; | 98% |
heptanal
chlorotriisopropylsilane
1-(1-propynyl)cyclohexene
(E)-{[1-(cyclohex-1-en-1-yl)-2-methylnon-1-en-3-yl]oxy}triisopropylsilane
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); potassium tert-butylate; 1,3-bis(mesityl)imidazolium chloride In tetrahydrofuran Inert atmosphere; regioselective reaction; | 99% |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); n-butyllithium; BF4(1-)*C29H27N2(1+) In tetrahydrofuran; hexane at 20℃; for 15h; Inert atmosphere; diastereoselective reaction; | 99% |
Conditions | Yield |
---|---|
With uranyl(VI) triflate In dichloromethane at 20℃; for 12h; Solvent; | 99% |
With [ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 In toluene at 50℃; for 24h; Inert atmosphere; | 38% |
With C48H48N2O4Ru2 In tetrahydrofuran at 20℃; for 24h; Irradiation; Inert atmosphere; chemoselective reaction; | 13 %Spectr. |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); n-butyllithium; (4R,5R)-1,3-bis(2-isopropylphenyl)-4,5-di(naphthalen-1-yl)-4,5-dihydro-1H-imidazol-3-ium tetrafluoroborate In tetrahydrofuran; hexane for 17h; Glovebox; enantioselective reaction; | A 99% B n/a |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon In N,N-dimethyl acetamide under 760.051 Torr; for 16h; Sealed tube; Heating; Schlenk technique; | 98.8% |
4,4-dimethylcyclohexenone
chlorotriisopropylsilane
4,4-dimethyl-1-triisopropylsilyl(oxy)-cyclohex-1-ene
Conditions | Yield |
---|---|
platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane at 100℃; for 0.25h; | 98% |
chlorotriisopropylsilane
(7RS)-(tert-butyldimethylsilanyloxy)-2,2-dimethyl-(7,7aRS)-dihydro-(3aSR)H-benzo[1,3]dioxol-4-one
Conditions | Yield |
---|---|
platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane at 70℃; for 1h; | 98% |
chlorotriisopropylsilane
4-(3-chloro-4-fluorophenyl)-3-(4-{[2-(tritylamino)ethyl]amino}-1,2,5-oxadiazol-3-yl)-1,2,4-oxadiazol-5(4H)-one
3-{4-[(2-aminoethyl)amino]-1,2,5-oxadiazol-3-yl}-4-(3-chloro-4-fluorophenyl)-1,2,4-oxadiazol-5(4H)-one hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; trifluoroacetic acid In 1,4-dioxane; diethyl ether | 98% |
chlorotriisopropylsilane
(1R,4S,5S,6R)-5,6-bis(methoxymethyl)bicyclo[2.2.1]hept-2-ene
benzaldehyde
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); n-butyllithium; BF4(1-)*C29H27N2(1+) In tetrahydrofuran; hexane at 20℃; for 15h; Inert atmosphere; diastereoselective reaction; | 98% |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon In N,N-dimethyl acetamide under 760.051 Torr; for 16h; Catalytic behavior; Reagent/catalyst; Solvent; Pressure; Temperature; Sealed tube; Heating; Schlenk technique; | 98% |
Conditions | Yield |
---|---|
Stage #1: chlorotriisopropylsilane With tri(phenyl)methylium closo-7,8,9,10,11,12-hexabromocarboranate In benzene at 20℃; for 0.0166667h; Glovebox; Inert atmosphere; Stage #2: 1-bromo-4-cyclopropylbenzene In benzene at 20℃; for 0.25h; Glovebox; Inert atmosphere; regioselective reaction; | 98% |
chlorotriisopropylsilane
triisopropylsilyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
at 22℃; for 16h; | 97% |
at 0 - 20℃; | |
at 0 - 20℃; for 21h; Inert atmosphere; | |
at 0 - 20℃; for 18h; Inert atmosphere; Schlenk technique; | |
In dichloromethane at 0 - 20℃; Inert atmosphere; |
Conditions | Yield |
---|---|
platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane In diethyl ether for 2h; Ambient temperature; | 97% |
chlorotriisopropylsilane
1,3-di-tert-butyl-2,3-dihydro-1H-1,3,2-diazasilol-2-ylidene
Conditions | Yield |
---|---|
Stage #1: chlorotriisopropylsilane; trityl tetrakis(pentafluorophenyl)borate In benzene at 20℃; Inert atmosphere; Stage #2: 1,3-di-tert-butyl-2,3-dihydro-1H-1,3,2-diazasilol-2-ylidene In benzene at 20℃; Inert atmosphere; | 97% |
Conditions | Yield |
---|---|
With platinum 1,3-divinyl-1,1,3,3-tetramethyldisiloxane In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene for 24h; Inert atmosphere; Reflux; | 97% |
Conditions | Yield |
---|---|
With Au97Ag3; oxygen In toluene at 80℃; for 18h; Reagent/catalyst; Solvent; chemoselective reaction; | 97% |
chlorotriisopropylsilane
4-fluoro-1-cyclopropyl-benzene
Conditions | Yield |
---|---|
Stage #1: chlorotriisopropylsilane With tri(phenyl)methylium closo-7,8,9,10,11,12-hexabromocarboranate In benzene at 20℃; for 0.0166667h; Glovebox; Inert atmosphere; Stage #2: 4-fluoro-1-cyclopropyl-benzene In benzene at 20℃; for 0.25h; Glovebox; Inert atmosphere; regioselective reaction; | 97% |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon In N,N-dimethyl acetamide at 100℃; under 7600.51 Torr; for 16h; Sealed tube; Schlenk technique; Autoclave; | 96.6% |
chlorotriisopropylsilane
carbon dioxide
methyl (2S)-2-amino-3-phenylpropanoate
N-Tsoc-phenylalanine methyl ester
Conditions | Yield |
---|---|
With palladium 10% on activated carbon In N,N-dimethyl acetamide under 760.051 Torr; for 16h; Reagent/catalyst; Pressure; Sealed tube; Heating; Schlenk technique; | 96.6% |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon In N,N-dimethyl acetamide under 760.051 Torr; for 16h; Sealed tube; Heating; Schlenk technique; | 96.2% |
chlorotriisopropylsilane
triisopropylbromosilane
Conditions | Yield |
---|---|
With ethyl tribromoacetate; palladium dichloride In tetrahydrofuran for 0.25h; Inert atmosphere; Reflux; | 96% |
With lithium nitrate; bromine In N,N-dimethyl-formamide at 25℃; Rate constant; | |
With bromine In tetrachloromethane at 25℃; Rate constant; |
chlorotriisopropylsilane
Conditions | Yield |
---|---|
With indium(III) bromide; oxygen In tetrahydrofuran at 20℃; for 24h; | 96% |
chlorotriisopropylsilane
bis(trifluoromethanesulfonyl)amide
C11H21F6NO4S2Si
Conditions | Yield |
---|---|
In 1,2-dichloro-ethane at 80℃; for 12h; Inert atmosphere; | 96% |
chlorotriisopropylsilane
4-methoxyphenylacetylen
1-(4-methoxyphenyl)-2-(triisopropylsilyl)acetylene
Conditions | Yield |
---|---|
With Au97Ag3; oxygen In toluene at 80℃; for 18h; chemoselective reaction; | 96% |
Conditions | Yield |
---|---|
With uranyl(VI) triflate In dichloromethane-d2 at 20℃; for 12h; | 96% |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon In N,N-dimethyl acetamide at 100℃; under 7600.51 Torr; for 16h; Sealed tube; Schlenk technique; Autoclave; | 95.1% |
cyclopent-2-enone
chlorotriisopropylsilane
1-triisopropylsilyl(oxy)-cyclopentene
Conditions | Yield |
---|---|
platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane at 100℃; for 0.25h; | 95% |
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