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inquiryCAS Number: 589-08-2 Molecular Formula: C9H13N Molecular Weight: 135.21 EINECS number: 209-632-3 Related Categories: Amines and Anilines; Amines and Anilines; Phenyls & Phenyl-Het; Phenyls & Phenyl-Het;amines
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1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re
N-butylamine
A
butyl-(3-methyl-3H-benzothiazol-2-ylidene)-amine
B
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
In dichloromethane at 25℃; for 3h; | A 95% B 85% |
N-methyl-N-(2-phenethyl)-4-methylbenzenesulfonamide
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With sodium tetrahydroborate; methoxybenzene In ethanol Irradiation; other reducing agent; | 91% |
With sodium tetrahydroborate; methoxybenzene In ethanol for 1h; Product distribution; Quantum yield; Irradiation; other solvents, reagents, reagents ratio; | 91% |
With sodium tetrahydroborate; methoxybenzene In ethanol Mechanism; Rate constant; Quantum yield; Irradiation; effect of other reducing agents, other electron donors, other solvent; | 91% |
With hydrogenchloride at 180℃; Hydrolysis; | |
With tetrabutylammonium perchlorate In N,N-dimethyl-formamide various p-tolylsulfonamides, investigation of the deprotection by cathodic cleveage; |
Conditions | Yield |
---|---|
Stage #1: 2-phenylethyl mesylate; methylamine In methanol; water at 140℃; under 15514.9 Torr; for 0.166667h; Flow reactor; Stage #2: With potassium hydroxide In water Solvent; | 90% |
N-methyl-N-(2-phenethyl)-4-methylbenzenesulfonamide
A
p-toluene sulfinic acid
B
Ethyl p-toluenesulfinate
C
methyl p-toluene sulfinate
D
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With sodium tetrahydroborate; 1,5-dimethoxynaphthalene In ethanol Irradiation; | A 71% B n/a C n/a D 89% |
Conditions | Yield |
---|---|
Stage #1: phenylacetaldehyde; methylamine With titanium(IV) isopropylate In methanol at 20℃; for 5h; Stage #2: With sodium tetrahydroborate In methanol at 20℃; for 2h; | 88% |
With alkali durch Reduktion des Kondensationsprodukts mit Natrium und Alkohol; | |
With formic acid; N-terminal His6-tagged formate dehydrogenase from Candida boidinii; Rs-amine dehydrogenase (originating from the enzyme engineeringof phenylalanine dehydrogenases from Rhodococcus sp. M4); NAD In aq. buffer at 30℃; for 48h; pH=8.5; Enzymatic reaction; |
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With potassium phosphate; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; ascorbic acid In water; acetonitrile at 20℃; for 16h; Sealed tube; Irradiation; Inert atmosphere; | 87% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate; bromine In 1,2-dimethoxyethane at -10 - 20℃; for 48h; | 82% |
With hydrogenchloride; arsenic(III) trioxide at 35 - 40℃; Electrolysis.an Bleikathoden; | |
With antimony pentoxide; sulfuric acid Electrolysis.an Bleikathoden; |
N,N-dimethyl-4-((methyl(phenethyl)amino)methyl)aniline
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With water; trifluoroacetic acid In acetonitrile at 120℃; for 5h; Sealed tube; | 75% |
methanol
phenethyl azide
A
N-Methyl-N-phenethylamine
B
N,N-dimethylphenethylamine
Conditions | Yield |
---|---|
With trans-RuCl(phenpyra-Me)(PPh3)2PF6; sodium hydroxide at 125℃; for 36h; Sealed tube; Inert atmosphere; Glovebox; | A 10 %Chromat. B 75% |
N-<1-Phenyl-2,2,2-trichlor-aethyl>-methylamin
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In diethyl ether for 10h; Heating; | 71% |
N-methyl-N-(2-phenethyl)-4-methylbenzenesulfonamide
A
ethyl ester of p-toluenesulfonic acid
B
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With 1,5-dimethoxynaphthalene; sodium ethanolate In ethanol Irradiation; | A 45% B 62% |
methanol
phenethyl azide
A
phenethylamine
B
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With trans-RuCl(phenpyra-Me)(PPh3)2PF6; sodium hydroxide at 125℃; for 5h; Sealed tube; Inert atmosphere; Glovebox; | A 10 %Chromat. B 60% |
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In tetrahydrofuran | 56% |
4-methoxy-7-morpholin-4-yl-benzothiazol-2-yl-amine
B
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
A 53% B n/a |
N-(2-phenylethyl)formamide
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran Reflux; | 34% |
With lithium aluminium tetrahydride; diethyl ether | |
Multi-step reaction with 2 steps 1: potassium; toluene 2: concentrated hydrochloric acid / Hydrolysis View Scheme |
Conditions | Yield |
---|---|
at 20℃; Erwaermen des Reaktionsprodukts mit Wasser; |
2-(2-phenylethyl)-1,2-benzisothiazol-3(2H)-one 1,1-dioxide
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
ueber mehrere Stufen; |
Conditions | Yield |
---|---|
beim Erhitzen ueber den Schmelzpunkt; | |
beim Erhitzen ueber den Schmelzpunkt; |
N-methyl-N-phenethylcyanamide
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With hydrogenchloride at 160℃; | |
Multi-step reaction with 2 steps 1: aqueous alcoholic sulfuric acid 2: hydrochloric acid / 160 °C View Scheme |
N-(2-bromo-2-phenylethyl)-N,4-dimethylbenzenesulfonamide
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With pentan-1-ol; sodium |
N-Methylthiophenylacetamide
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With hydrogenchloride at 30 - 40℃; Electrolysis.an Bleikathoden; | |
With sodium tetrahydroborate; triethyloxonium fluoroborate 1.) CH2Cl2, 25 deg C, 10-20 min; 2.) anhydrous methanol 2-3 h; Yield given. Multistep reaction; |
2-(3-Chlorophenyl)-N-methylethan-1-amine
A
N-methylindoline
B
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With diethyl ether; phenyllithium; diethylamine |
N-methyl-N-phenethylformamide
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With hydrogenchloride Hydrolysis; | |
With hydrogenchloride; methanol for 18h; Heating; |
N-methyl-N-phenethyl-urea
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With hydrogenchloride at 160℃; |
(E)-N-benzyl-N-methyl-2-phenylethen-1-amine
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With palladium on activated charcoal; ethanol Hydrogenation; |
Conditions | Yield |
---|---|
With ethanol at 100℃; | |
With benzene at 100℃; |
Conditions | Yield |
---|---|
nachfolgende Hydrolyse; | |
und Erwaermen des Reaktionsprodukts mit wasserhaltigem Aethanol; |
2-(2-chlorochlorophenyl)-N-methylethanamine
phenyllithium
A
N-methylindoline
B
N-Methyl-N-phenethylamine
1-phenyl-2-bromoethane
methylamine
A
N-methyl-N-phenethyl-2-phenylethan-1-amine
B
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With ethanol | |
In ethanol at 0 - 20℃; for 40h; Overall yield = 90 percent; Overall yield = 1.4 g; |
formaldehyd
phenylmagnesium bromide
methylamine
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With diethyl ether |
2-Bromoacetyl bromide
N-Methyl-N-phenethylamine
N-methyl-N-2-phenylethyl-2-bromoacetamide
Conditions | Yield |
---|---|
In dichloromethane at -25 - 20℃; | 100% |
With potassium carbonate In dichloromethane at 0 - 20℃; for 3h; |
(2R)-2-(N-(tert-butoxycarbonyl)-N-methylamino)-3-(2-naphthyl)-propionic acid
N-Methyl-N-phenethylamine
N-methyl-N-((1R)-1-(N-methyl-N-phenethylcarbamoyl)-2-(2-naphthyl)ethyl)carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
Stage #1: (2R)-2-(N-(tert-butoxycarbonyl)-N-methylamino)-3-(2-naphthyl)-propionic acid With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 0℃; for 0.333333h; Addition; Stage #2: N-Methyl-N-phenethylamine In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; for 16h; Condensation; | 100% |
With 1-hydroxy-7-aza-benzotriazole; N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; for 16.3h; | 1.89 g |
N-Methyl-N-phenethylamine
(5α,7α)-17-(cyclopropylmethyl)-4,5-epoxy-3,6-dimethoxy-6,14-ethenomorphinan-7-carboxyl chloride
C34H40N2O4
Conditions | Yield |
---|---|
With triethylamine In chloroform at 20℃; | 100% |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; polymer-bound triphenylphosphine In tetrahydrofuran at 20℃; for 12h; | 99% |
Stage #1: N-Methyl-N-phenethylamine With (acryloyloxymethyl)polystyrene In N,N-dimethyl-formamide at 20℃; for 18h; Solid phase reaction; Michael addition; Stage #2: allyl bromide In N,N-dimethyl-formamide at 20℃; for 18h; Solid phase reaction; quaternization; Stage #3: With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 5h; Solid phase reaction; Hofmann elimination; | 81% |
With sodium hydrogencarbonate In N,N-dimethyl-formamide at 70℃; for 2h; | 50% |
Yield given. Multistep reaction; |
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
Stage #1: (1S,2S)-(+)-2-(methyl(phenethyl)amino)-1-phenylpropan-1-ol With methanesulfonyl chloride; triethylamine In diethyl ether at 0 - 20℃; Stage #2: With triethylamine In diethyl ether at 0 - 20℃; Stage #3: N-Methyl-N-phenethylamine In diethyl ether at 20℃; for 16h; | 99% |
Conditions | Yield |
---|---|
With sodium acetate In methanol at 20℃; Inert atmosphere; Schlenk technique; | 99% |
N,N-dimethyl-formamide
N-Methyl-N-phenethylamine
N-methyl-N-phenethylformamide
Conditions | Yield |
---|---|
at 150℃; for 96h; Sealed tube; Inert atmosphere; Green chemistry; | 99% |
at 150℃; for 96h; Inert atmosphere; Sealed tube; | 99% |
With cobalt(II) acetate at 150℃; for 3h; Inert atmosphere; Sealed tube; | 95% |
N-Methyl-N-phenethylamine
1-(2-Deoxy-β-D-erythro-pentofuranosyl)-4-(pentafluorophenyloxy)-2(1H)-pyrimidinone
Conditions | Yield |
---|---|
In 1,4-dioxane at 80℃; | 98% |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); sodium t-butanolate; 1,3-bis[2,6-bis(1-methylethyl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene monohydrochloride In toluene at 100℃; for 20h; Inert atmosphere; Schlenk technique; | 98% |
N-Methylisatoic anhydride
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With isatoic anhydride resin In dichloromethane Ambient temperature; 1.) 14 h; 2.) 90 min; | 97% |
O-benzyl-N-tert-butoxycarbonyl-L-tyrosine
N-Methyl-N-phenethylamine
N-[Boc-(O-benzyl)-L-tyrosyl]-N-methyl-2-phenylethylamine
Conditions | Yield |
---|---|
97% |
benzyl bromide
N-Methyl-N-phenethylamine
N-(2-phenethyl)benzylmethylamine
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; polymer-bound triphenylphosphine In tetrahydrofuran at 20℃; for 12h; | 97% |
Stage #1: N-Methyl-N-phenethylamine With REM resin at 20℃; for 2h; Stage #2: benzyl bromide In N,N-dimethyl-formamide for 18h; Stage #3: With N-ethyl-N,N-diisopropylamine In dichloromethane | 95% |
Stage #1: N-Methyl-N-phenethylamine With REM resin at 20℃; for 3h; Michael addition; Stage #2: benzyl bromide In N,N-dimethyl-formamide at 20℃; for 18h; Stage #3: With potassium carbonate; N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 6h; |
phenyl 1H-indazol-5-ylcarbamate
N-Methyl-N-phenethylamine
3-(1H-indazol-5-yl)-1-methyl-1-phenethylurea
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran; N,N-dimethyl-formamide at 90℃; for 14h; | 97% |
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In isopropyl alcohol at 100℃; | 97% |
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
at 70℃; for 2h; | 97% |
Conditions | Yield |
---|---|
With palladium 10% on activated carbon In N,N-dimethyl acetamide under 760.051 Torr; for 16h; Sealed tube; Heating; Schlenk technique; | 96.2% |
tetraethyldiborane(6)
N-Methyl-N-phenethylamine
{methyl-(2-phenylethyl)amino}diethylborane
Conditions | Yield |
---|---|
3 h at 70-100°C; | 96% |
3 h at 70-100°C; | 96% |
3-Chloropyridine
N-Methyl-N-phenethylamine
N-methyl-N-phenethylpyridin-3-amine
Conditions | Yield |
---|---|
With C43H58ClO2PPd; sodium t-butanolate; ruphos In tetrahydrofuran at 85℃; for 6h; Inert atmosphere; | 96% |
With C30H43O2P*C13H13NO3PdS; sodium t-butanolate; ruphos In tetrahydrofuran at 85℃; for 24h; | 80% |
With methanesulfonato(2-dicyclohexylphosphino-2’,6’-di-i-propoxy-1,1’-biphenyl)(2’-methylamino-1,1‘-biphenyl-2-yl)palladium(II); sodium t-butanolate; ruphos In tetrahydrofuran at 85℃; for 24h; Inert atmosphere; | 80% |
chlorosulfonyl-acetic acid methyl ester
N-Methyl-N-phenethylamine
2-[methyl(phenethyl)sulfamoyl]acetic acid methyl ester
Conditions | Yield |
---|---|
Stage #1: chlorosulfonyl-acetic acid methyl ester; N-Methyl-N-phenethylamine With triethylamine In tetrahydrofuran at 20℃; Stage #2: With hydrogenchloride In water pH=7; | 96% |
2-(Benzyloxy)-1-naphthaldehyde
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With sodium tris(acetoxy)borohydride; acetic acid In 1,2-dichloro-ethane at 20℃; for 2.5h; | 96% |
Conditions | Yield |
---|---|
With manganese(II) chloride tetrahydrate at 150℃; for 10h; Sealed tube; Microwave irradiation; Inert atmosphere; | 96% |
With cobalt(II) diacetate tetrahydrate at 150℃; for 3h; Sealed tube; Inert atmosphere; | 83% |
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane; titanium(IV) isopropylate; hydrogen; iodine; triethylamine In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane at 20℃; under 30402 Torr; for 20h; | 96% |
phenylacetylene
N-Methyl-N-phenethylamine
N-methyl-N-phenethyl-2-phenylacetamide
Conditions | Yield |
---|---|
With potassium hexafluorophosphate; 4-methylpyridine-1-oxide; chloro(cyclopentadienyl)bis(triphenylphosphine)ruthenium (II) In 1,2-dichloro-ethane at 100℃; for 24h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; Sealed tube; | 96% |
1-methyl-3-indolecarboxylic acid
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With PS-carbodiimide; benzotriazol-1-ol In 1-methyl-pyrrolidin-2-one at 100℃; for 0.0833333h; microwave irradiation; | 95% |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; polymer-bound triphenylphosphine In tetrahydrofuran at 20℃; for 12h; | 95% |
N-Methyl-N-phenethylamine
5-bromo-1H-pyrrolo[2,3-b]pyridine
N-methyl-N-phenethyl-1H-pyrrolo[2,3-b]pyridin-5-amine
Conditions | Yield |
---|---|
With RuPhos palladacycle; lithium hexamethyldisilazane; ruphos In tetrahydrofuran at 65℃; for 4h; Inert atmosphere; Sealed vial; | 95% |
Conditions | Yield |
---|---|
With manganese(II) chloride tetrahydrate at 150℃; for 10h; Sealed tube; Microwave irradiation; Inert atmosphere; | 95% |
With cobalt(II) diacetate tetrahydrate at 150℃; for 3h; Sealed tube; Inert atmosphere; | 46% |
phenyl (benzoyloxy)carbamate
N-Methyl-N-phenethylamine
Conditions | Yield |
---|---|
With 1H-imidazole In tetrahydrofuran at 100℃; for 2h; Microwave irradiation; Sealed tube; | 95% |
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; for 3h; | 95% |
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