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inquiryConditions | Yield |
---|---|
Stage #1: heptaethylene glycol monododecyl ether With sodium hydride In tetrahydrofuran; mineral oil for 0.5h; Inert atmosphere; Stage #2: C6H12O6S In tetrahydrofuran; mineral oil pH=2; Inert atmosphere; Stage #3: With sulfuric acid In tetrahydrofuran; water; mineral oil at 80℃; for 2h; Inert atmosphere; | 56% |
pentaethylene glycol
1-(2-{2-[2-(2-chloro-ethoxy)-ethoxy]-ethoxy}-ethoxy)-dodecane
decaethylene glycol monodecyl ether
Conditions | Yield |
---|---|
With sodium |
Conditions | Yield |
---|---|
With potassium hydroxide at 140 - 170℃; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: triethylamine; dmap; thionyl chloride / dichloromethane / 0 - 25 °C 2.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / Inert atmosphere 2.2: pH 2 / Inert atmosphere 2.3: 2 h / 80 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1.1: triethylamine; dmap; thionyl chloride / dichloromethane / 0 - 25 °C 2.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / Inert atmosphere 2.2: pH 2 / Inert atmosphere 2.3: 2 h / 80 °C / Inert atmosphere 3.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / Inert atmosphere 3.2: pH 2 / Inert atmosphere 3.3: 2 h / 80 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: triethylamine; dmap; thionyl chloride / dichloromethane / 0 - 25 °C 2.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / Inert atmosphere 2.2: pH 2 / Inert atmosphere 2.3: 2 h / 80 °C / Inert atmosphere 3.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / Inert atmosphere 3.2: pH 2 / Inert atmosphere 3.3: 2 h / 80 °C / Inert atmosphere 4.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / Inert atmosphere 4.2: pH 2 / Inert atmosphere 4.3: 2 h / 80 °C / Inert atmosphere View Scheme |
decaethylene glycol monodecyl ether
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / Inert atmosphere 1.2: pH 2 / Inert atmosphere 1.3: 2 h / 80 °C / Inert atmosphere 2.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / Inert atmosphere 2.2: pH 2 / Inert atmosphere 2.3: 2 h / 80 °C / Inert atmosphere View Scheme |
decaethylene glycol monodecyl ether
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / Inert atmosphere 1.2: pH 2 / Inert atmosphere 1.3: 2 h / 80 °C / Inert atmosphere 2.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / Inert atmosphere 2.2: pH 2 / Inert atmosphere 2.3: 2 h / 80 °C / Inert atmosphere 3.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / Inert atmosphere 3.2: pH 2 / Inert atmosphere 3.3: 2 h / 80 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / Inert atmosphere 1.2: pH 2 / Inert atmosphere 1.3: 2 h / 80 °C / Inert atmosphere 2.1: sodium hydride / mineral oil; tetrahydrofuran / 0.5 h / Inert atmosphere 2.2: pH 2 / Inert atmosphere 2.3: 2 h / 80 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Stage #1: decaethylene glycol monodecyl ether With sodium hydride In tetrahydrofuran; mineral oil for 0.5h; Inert atmosphere; Stage #2: methyl iodide In tetrahydrofuran; mineral oil Inert atmosphere; | 70% |
Conditions | Yield |
---|---|
Schotten-Baumann reaction; |
Conditions | Yield |
---|---|
Schotten-Baumann reaction; |
Conditions | Yield |
---|---|
Schotten-Baumann reaction; |
Conditions | Yield |
---|---|
In further solvent(s) surfactant C12H25O(C2H4O)10H mixed with Tb(NO3)3*6H2O (mol ratio 1:2) and to mixt. added extra H2O; XRD, IR, polarized optical microscopy (POM); |
decaethylene glycol monodecyl ether
Conditions | Yield |
---|---|
In further solvent(s) surfactant C12H25O(C2H4O)10H mixed with Tb(NO3)3*6H2O (mol ratio 1:2); XRD, IR, polarized optical microscopy (POM); |
Conditions | Yield |
---|---|
In further solvent(s) surfactant C12H25O(C2H4O)10H mixed with Tb(NO3)3*6H2O (mol ratio 1:2) and to mixt. added extra D2O; XRD, IR, polarized optical microscopy (POM); |
Conditions | Yield |
---|---|
In further solvent(s) surfactant C12H25O(C2H4O)10H mixed with Eu(NO3)3*6H2O (mol ratio 1:1) and to mixt. added extra water; XRD, IR, polarized optical microscopy (POM); |
Conditions | Yield |
---|---|
In further solvent(s) surfactant C12H25O(C2H4O)10H mixed with Eu(NO3)3*6H2O (mol ratio 1:2) and to mixt. added extra water; XRD, IR, polarized optical microscopy (POM); |
decaethylene glycol monodecyl ether
Conditions | Yield |
---|---|
In further solvent(s) surfactant C12H25O(C2H4O)10H mixed with Eu(NO3)3*6H2O (mol ratio 1:2); XRD, IR, polarized optical microscopy (POM); |
Conditions | Yield |
---|---|
In further solvent(s) surfactant C12H25O(C2H4O)10H mixed with Eu(NO3)3*6H2O (mol ratio 1:1) and to mixt. added extra D2O; XRD, IR, polarized optical microscopy (POM); |
Conditions | Yield |
---|---|
In further solvent(s) surfactant C12H25O(C2H4O)10H mixed with Eu(NO3)3*6H2O (mol ratio 1:2) and to mixt. added extra D2O; XRD, IR, polarized optical microscopy (POM); |
decaethylene glycol monodecyl ether
3-(triethoxypropyl) isocyanate
Conditions | Yield |
---|---|
With stannous octoate at 60℃; for 24h; Inert atmosphere; |
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