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Cas:6636-55-1
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:6636-55-1
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryProduct Description Product website: http://www.finerchem.com/pro01en/id/1184.html Product Name Methyl 6-chloro-2-pyridinecarboxylate
Cas:6636-55-1
Min.Order:1 Gram
FOB Price: $52.0
Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
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Min.Order:1 Kilogram
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Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1. Guaranteed purity; 2. Large quantity in stock; 3. Largest manufacturer; 4. Best service after shipment with email; 5. High quality & competitive price; Appearance:powder Storage:Store in sealed containers at cool & dry plac
Cas:6636-55-1
Min.Order:100 Gram
Negotiable
Type:Other
inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
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Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
Cas:6636-55-1
Min.Order:1 Kilogram
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inquiry6-CHLORO-2-PICOLINIC ACID METHYL ESTER CAS:6636-55-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high qu
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Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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Min.Order:1 Kilogram
Negotiable
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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Min.Order:10 Kilogram
Negotiable
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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Min.Order:4 Kilogram
Negotiable
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Min.Order:0 Metric Ton
Negotiable
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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Min.Order:0
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
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Min.Order:1 Gram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:6636-55-1
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryMethyl 6-chloropicolinateAppearance:white crystalline powder Storage:Shading, sealed, dry place. Package:according to customers' requirements Application:API Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF ect...)
We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
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Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry6-CHLORO-2-PICOLINIC ACID METHYL ESTER Basic information Product Name: 6-CHLORO-2-PICOLINIC ACID METHYL ESTER Synonyms: Methyl 6-Chloropyridine-2-carboxylate, 97+%;METHYL 6-CHLOROPYRIDINE-2-CARBOXYLATE;AKOS BBS-00004651;6-CHLOROPYRIDINE-2-CARB
Cas:6636-55-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
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Min.Order:0
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Cas:6636-55-1
Min.Order:1 Gram
Negotiable
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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Min.Order:1 Metric Ton
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Type:Trading Company
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Min.Order:100 Gram
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Min.Order:0
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inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Cas:6636-55-1
Min.Order:1 Kilogram
Negotiable
Type:Other
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Cas:6636-55-1
Min.Order:1 Metric Ton
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Type:Trading Company
inquiryConditions | Yield |
---|---|
With thionyl chloride at 0 - 50℃; for 6.75h; | 100% |
Stage #1: methanol; 6-chloropicolinic acid With hydrogenchloride for 15h; Heating / reflux; Stage #2: With sodium hydroxide In water | 95% |
With hydrogenchloride In water at 80℃; for 48h; | |
With hydrogenchloride In water at 80℃; for 48h; |
6-chloropicolinic acid
Methyl trichloroacetate
methyl 6-chloropicolinate
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium carbonate at 90 - 150℃; for 2h; | 83% |
2,6-dichloropyridine
methanol
carbon monoxide
A
2,6-bis(methoxycarbonyl)pyridine
B
methyl 6-chloropicolinate
Conditions | Yield |
---|---|
With triethylamine; triphenylphosphine; bis-triphenylphosphine-palladium(II) chloride at 140℃; under 37503 Torr; for 6h; methoxycarbonylation; | A 81% B n/a |
methyl 2-hydroxy-6-pyridinecarboxylate
methyl 6-chloropicolinate
Conditions | Yield |
---|---|
With trichlorophosphate at 110℃; for 14h; | 61% |
methyl pyridine-2-carboxylate
p-nitrophenyl isocyanide
A
methyl 6-chloropicolinate
Conditions | Yield |
---|---|
Stage #1: methyl pyridine-2-carboxylate With fluorine In dichloromethane at -78 - -50℃; Stage #2: p-nitrophenyl isocyanide In dichloromethane at -50 - 0℃; for 4h; | A 40% B 31% C n/a |
Conditions | Yield |
---|---|
With hydrogenchloride | |
Multi-step reaction with 2 steps 1: oxalyl dichloride / N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C 2: dichloromethane / 1.58 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 20 °C 2: 1.5 h / 20 °C View Scheme |
2,6-Dibromopyridine
methanol
carbon dioxide
A
2,6-bis(methoxycarbonyl)pyridine
B
methyl 6-chloropicolinate
Conditions | Yield |
---|---|
With hydrogenchloride; n-butyllithium Yield given. Multistep reaction. Yields of byproduct given; |
6-chloropicolinic acid
boron trifluoride methanol complex
methyl 6-chloropicolinate
Conditions | Yield |
---|---|
at 110℃; for 0.25h; |
1-oxy-pyridine-2-carboxylic acid methyl ester
A
methyl 6-chloropicolinate
B
4-Chloro-pyridine-2-carboxylic acid methyl ester
Conditions | Yield |
---|---|
With trichlorophosphate at 80℃; for 17h; Yield given. Yields of byproduct given; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: mCPBA / CH2Cl2 / 48 h / Ambient temperature 2: POCl3 / 17 h / 80 °C View Scheme |
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1.58333h; | |
at 20℃; for 1.5h; |
methyl 6-chloropicolinate
2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)-5-(tributylstannyl)oxazole
methyl 6-(2-(1-(tert-butyldimethylsilyloxy)-3-(4-(phenoxymethyl)phenyl)propyl)oxazol-5-yl)pyridine-2-carboxylate
Conditions | Yield |
---|---|
tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane for 3h; Stille coupling; Heating; | 95% |
Conditions | Yield |
---|---|
With 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; potassium carbonate In N,N-dimethyl-formamide at 120℃; for 7h; Schlenk technique; Inert atmosphere; | 92% |
methyl 6-chloropicolinate
6-chloro-2-pyridinemethanol
Conditions | Yield |
---|---|
Stage #1: methyl 6-chloropicolinate With lithium aluminium tetrahydride In tetrahydrofuran at -45 - 0℃; for 1.5h; Stage #2: With sodium hydroxide; water In tetrahydrofuran | 91% |
With sodium tetrahydroborate In ethanol at 15 - 30℃; for 6h; Inert atmosphere; |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,4-dioxane at 80℃; Inert atmosphere; Sealed tube; | 83% |
methyl 6-chloropicolinate
2-(3-(biphenyl-4-yl)-1-(tert-butyldimethylsilyloxy)propyl)-5-(tributylstannyl)oxazole
methyl 6-(2-(3-(biphenyl-4-yl)-1-(tert-butyldimethylsilyloxy)propyl)oxazol-5-yl)picolinate
Conditions | Yield |
---|---|
tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane for 24h; Stille coupling; Heating; | 81% |
Conditions | Yield |
---|---|
With sodiumsulfide nonahydrate; sodium acetate In N,N-dimethyl-formamide at 70℃; for 12h; | 78% |
methyl 6-chloropicolinate
2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)-5-(tributylstannyl)oxazole
methyl 6-(2-(1-(tert-butyldimethylsilyloxy)-3-(4-phenoxyphenyl)propyl)oxazol-5-yl)pyridine-2-carboxylate
Conditions | Yield |
---|---|
tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane for 18h; Stille coupling; Heating; | 77% |
methyl 6-chloropicolinate
sodium thiomethoxide
methyl 6-(methylthio)picolinate
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; for 0.5h; | 72% |
methyl 6-chloropicolinate
2-(3-(biphenyl-4-yl)propyl)-5-(tributylstannyl)oxazole
C25H22N2O3
Conditions | Yield |
---|---|
tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane for 24h; Stille coupling; Heating; | 66% |
methyl 6-chloropicolinate
6-chloro-pyridine-2-carboxylic acid hydrazide
Conditions | Yield |
---|---|
With hydrazine hydrate In methanol at 20℃; for 0.333333h; | 65% |
With ethanol; hydrazine |
methyl 6-chloropicolinate
2-trimethylstannylpyridine
2,2'-dipyridyl-6-carboximidic acid methyl ester
Conditions | Yield |
---|---|
bis-triphenylphosphine-palladium(II) chloride In N,N-dimethyl-formamide at 130℃; for 12h; Condensation; | 61% |
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; caesium carbonate In toluene at 100℃; Inert atmosphere; | 57% |
Conditions | Yield |
---|---|
With (1,2-dimethoxyethane)dichloronickel(II); [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; caesium carbonate; 4,4'-di-tert-butyl-2,2'-bipyridine In N,N-dimethyl-formamide at 25 - 27℃; for 21h; Reagent/catalyst; Inert atmosphere; Irradiation; | 57% |
methyl 6-chloropicolinate
Conditions | Yield |
---|---|
Stage #1: [5-methyl-2-phenyl-1,3-oxazol-4-yl]methanol With sodium hydride In tetrahydrofuran at 1 - 30℃; Stage #2: methyl 6-chloropicolinate In tetrahydrofuran at 1 - 40℃; for 5h; | 51% |
[5-methyl-2-phenyl-1,3-oxazol-4-yl]methanol
methyl 6-chloropicolinate
Conditions | Yield |
---|---|
Stage #1: [5-methyl-2-phenyl-1,3-oxazol-4-yl]methanol With sodium hydride In tetrahydrofuran at 0 - 20℃; for 0.25h; Stage #2: methyl 6-chloropicolinate In tetrahydrofuran at 40℃; for 5h; | 51% |
methyl 6-chloropicolinate
2-fluoropyrazine
(6-chloropyridin-2-yl)(3-fluoropyrazin-2-yl)methanone
Conditions | Yield |
---|---|
Stage #1: 2-fluoropyrazine With 2,2,6,6-tetramethyl-piperidine; n-butyllithium In tetrahydrofuran at -78 - 0℃; Inert atmosphere; Stage #2: methyl 6-chloropicolinate In tetrahydrofuran at -78 - -70℃; | 46% |
Conditions | Yield |
---|---|
With potassium tert-butylate at 20 - 50℃; for 43h; | 41.6% |
methyl 6-chloropicolinate
acetonitrile
3-(6-chloro-pyridin-2-yl)-3-oxo-propionitrile
Conditions | Yield |
---|---|
With sodium hydride In toluene; mineral oil at 65℃; for 24h; Inert atmosphere; | 40% |
With sodium hydride In toluene; mineral oil at 65℃; for 24h; Inert atmosphere; | 40% |
methyl 6-chloropicolinate
butan-1-ol
6-n-butoxy-2-pyridinecarboxylic acid
Conditions | Yield |
---|---|
Stage #1: methyl 6-chloropicolinate; butan-1-ol With sodium hexamethyldisilazane at 130℃; for 48h; Heating / reflux; Stage #2: With hydrogenchloride; water at 0℃; |
1-[(tert-butyldimethylsilyl)oxy]-1-(oxazol-2-yl)-7-phenylheptane
methyl 6-chloropicolinate
methyl 6-(2-(1-(tert-butyldimethylsilyloxy)-7-phenylheptyl)oxazol-5-yl)picolinate
Conditions | Yield |
---|---|
Stage #1: 1-[(tert-butyldimethylsilyl)oxy]-1-(oxazol-2-yl)-7-phenylheptane With tert.-butyl lithium Stage #2: With tributyltin chloride Stage #3: methyl 6-chloropicolinate; tetrakis(triphenylphosphine) palladium(0) In 1,4-dioxane for 24h; Stille coupling; Heating; Further stages.; | 975 mg |
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