Product Name:Afimoxifene CAS No.: 68392-35-8 Chemical formula: C26H29NO2 Molecular weight:387.51 Item Standard Appearance white powder Identification H-NMR
Cas:68392-35-8
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Cas:68392-35-8
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine chemicals, ph
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inquiryAfimoxifene CAS:68392-35-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediates
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquirySuperiority We can customize and synthesize products that other suppliers may not be able to provide. 1. best service, high quality and reasonable way for h
Cas:68392-35-8
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:68392-35-8
Min.Order:10 Gram
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:68392-35-8
Min.Order:100 Gram
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:68392-35-8
Min.Order:1 Kilogram
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:68392-35-8
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Cas:68392-35-8
Min.Order:1 Metric Ton
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Type:Trading Company
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Cas:68392-35-8
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inquiryR & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
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inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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Cas:68392-35-8
Min.Order:0
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:68392-35-8
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Type:Lab/Research institutions
inquiryGMP factory Packing with pallet as buyer's special request Best service after shipment with e-mail Cargos together with container sales seervice available Api, inhibitor, and fine chemicals for more than 6 years. Application:
Cas:68392-35-8
Min.Order:0 Metric Ton
Negotiable
Type:Trading Company
inquiryAfimoxifene cas 68392-35-8 Application:Afimoxifene cas 68392-35-8
Factory supply high purity low priceAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
4-hydroxytamoxifen
Conditions | Yield |
---|---|
With water In methanol for 0.0333333h; Quantum yield; Photolysis; | 73% |
(2-chloroethyl)dimethylamine hydrochloride
1,1-bis(4-hydroxyphenyl)-2-phenyl-1-butene
4-hydroxytamoxifen
Conditions | Yield |
---|---|
Stage #1: 1,1-bis(4-hydroxyphenyl)-2-phenyl-1-butene With caesium carbonate In N,N-dimethyl-formamide for 0.5h; Reflux; Stage #2: (2-chloroethyl)dimethylamine hydrochloride In N,N-dimethyl-formamide at 120℃; for 7h; | 67% |
Stage #1: 1,1-bis(4-hydroxyphenyl)-2-phenyl-1-butene With caesium carbonate In N,N-dimethyl-formamide at 70 - 80℃; for 0.166667h; Stage #2: (2-chloroethyl)dimethylamine hydrochloride In N,N-dimethyl-formamide for 1.75h; | 30% |
Stage #1: 1,1-bis(4-hydroxyphenyl)-2-phenyl-1-butene With caesium carbonate In N,N-dimethyl-formamide at 80℃; for 0.166667h; Stage #2: (2-chloroethyl)dimethylamine hydrochloride In N,N-dimethyl-formamide at 80℃; for 5.5h; | 13.6% |
Stage #1: 1,1-bis(4-hydroxyphenyl)-2-phenyl-1-butene With caesium carbonate In N,N-dimethyl-formamide at 80℃; for 0.166667h; Stage #2: (2-chloroethyl)dimethylamine hydrochloride In N,N-dimethyl-formamide at 80℃; for 5.5h; | 13.6% |
dimethyl amine
E/Z-1-[4-(2-bromoethoxy)phenyl]-1-(4-hydroxyphenyl)-2-phenylbutene
4-hydroxytamoxifen
Conditions | Yield |
---|---|
In tetrahydrofuran at 60℃; for 43h; | 31% |
1,1-bis(4-hydroxyphenyl)-2-phenyl-1-butene
2-(dimethylamino)ethyl chloride
4-hydroxytamoxifen
Conditions | Yield |
---|---|
With caesium carbonate In N,N-dimethyl-formamide Inert atmosphere; | 24% |
Propylbenzene
4-hydroxytamoxifen
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: potassium tert-butoxide; n-butyllithium; tetramethylethylenediamine / hexane; tetrahydrofuran / 0.5 h / 20 °C 1.2: 97 percent / hexane; tetrahydrofuran / 4.5 h / -78 - 20 °C 2.1: 93 percent / aq. hydrochloric acid / ethanol; CH2Cl2 / Heating 3.1: 90 percent / aq. sodium hydroxide; tetrabutylammonium hydrogen sulfate / 18 h / 20 °C 4.1: 57 percent / boron tribromide / CH2Cl2 / 4.5 h 5.1: 31 percent / tetrahydrofuran / 43 h / 60 °C View Scheme |
4-hydroxy-4'-methoxybenzophenone
4-hydroxytamoxifen
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1.1: sodium hydride / dimethylformamide / 1 h / 0 °C 1.2: 95 percent / dimethylformamide / 2 h / 20 °C 2.1: potassium tert-butoxide; n-butyllithium; tetramethylethylenediamine / hexane; tetrahydrofuran / 0.5 h / 20 °C 2.2: 97 percent / hexane; tetrahydrofuran / 4.5 h / -78 - 20 °C 3.1: 93 percent / aq. hydrochloric acid / ethanol; CH2Cl2 / Heating 4.1: 90 percent / aq. sodium hydroxide; tetrabutylammonium hydrogen sulfate / 18 h / 20 °C 5.1: 57 percent / boron tribromide / CH2Cl2 / 4.5 h 6.1: 31 percent / tetrahydrofuran / 43 h / 60 °C View Scheme |
4-(methoxymethoxy)-4'-methoxybenzophenone
4-hydroxytamoxifen
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: potassium tert-butoxide; n-butyllithium; tetramethylethylenediamine / hexane; tetrahydrofuran / 0.5 h / 20 °C 1.2: 97 percent / hexane; tetrahydrofuran / 4.5 h / -78 - 20 °C 2.1: 93 percent / aq. hydrochloric acid / ethanol; CH2Cl2 / Heating 3.1: 90 percent / aq. sodium hydroxide; tetrabutylammonium hydrogen sulfate / 18 h / 20 °C 4.1: 57 percent / boron tribromide / CH2Cl2 / 4.5 h 5.1: 31 percent / tetrahydrofuran / 43 h / 60 °C View Scheme |
E/Z-1-(4-hydroxyphenyl)-1-(4-methoxyphenyl)-2-phenylbutene
4-hydroxytamoxifen
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 90 percent / aq. sodium hydroxide; tetrabutylammonium hydrogen sulfate / 18 h / 20 °C 2: 57 percent / boron tribromide / CH2Cl2 / 4.5 h 3: 31 percent / tetrahydrofuran / 43 h / 60 °C View Scheme |
1-(4-methoxymethoxyphenyl)-1-(4-methoxyphenyl)-2-phenylbutan-1-ol
4-hydroxytamoxifen
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 93 percent / aq. hydrochloric acid / ethanol; CH2Cl2 / Heating 2: 90 percent / aq. sodium hydroxide; tetrabutylammonium hydrogen sulfate / 18 h / 20 °C 3: 57 percent / boron tribromide / CH2Cl2 / 4.5 h 4: 31 percent / tetrahydrofuran / 43 h / 60 °C View Scheme |
E/Z-1-[4-(2-bromoethoxy)phenyl]-1-(4-methoxyphenyl)-2-phenylbut-1-ene
4-hydroxytamoxifen
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 57 percent / boron tribromide / CH2Cl2 / 4.5 h 2: 31 percent / tetrahydrofuran / 43 h / 60 °C View Scheme |
uridine 3'-(4-hydroxytamoxifen phosphate)
4-hydroxytamoxifen
Conditions | Yield |
---|---|
With sodium chloride pH=6; Mes-NaOH buffer; Enzymatic reaction; |
4,4'-Dihydroxybenzophenone
4-hydroxytamoxifen
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: titanium tetrachloride; zinc / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere; Reflux; Darkness 2.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / 70 - 80 °C 2.2: 1.75 h View Scheme | |
Multi-step reaction with 2 steps 1.1: zinc; titanium tetrachloride / tetrahydrofuran / 12 h / -20 °C / Inert atmosphere; Reflux; Darkness 2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Reflux 2.2: 7 h / 120 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: titanium tetrachloride; zinc / tetrahydrofuran / 2 h / -10 - 95 °C / Inert atmosphere 1.2: 2 h / 0 - 95 °C / Inert atmosphere; Darkness 2.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / 80 °C 2.2: 5.5 h / 80 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: zinc; titanium tetrachloride / tetrahydrofuran / 2 h / Inert atmosphere; Darkness 2.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / 80 °C 2.2: 5.5 h / 80 °C View Scheme | |
Multi-step reaction with 2 steps 1: titanium tetrachloride; zinc / tetrahydrofuran / Inert atmosphere 2: caesium carbonate / N,N-dimethyl-formamide / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
With Vitamin C; Agrocybe aegerita peroxygenase; dihydrogen peroxide at 20℃; for 0.05h; pH=7; aq. phosphate buffer; Enzymatic reaction; regioselective reaction; |
1-phenyl-propan-1-one
4-hydroxytamoxifen
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: zinc; titanium tetrachloride / tetrahydrofuran / 12 h / -20 °C / Inert atmosphere; Reflux; Darkness 2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / Reflux 2.2: 7 h / 120 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: zinc; titanium tetrachloride / tetrahydrofuran / 2 h / Inert atmosphere; Darkness 2.1: caesium carbonate / N,N-dimethyl-formamide / 0.17 h / 80 °C 2.2: 5.5 h / 80 °C View Scheme | |
Multi-step reaction with 2 steps 1: titanium tetrachloride; zinc / tetrahydrofuran / Inert atmosphere 2: caesium carbonate / N,N-dimethyl-formamide / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
for 0.166667h; Quantum yield; Kinetics; Photolysis; |
Conditions | Yield |
---|---|
Claisen Rearrangement; Photolysis; |
A
4-hydroxytamoxifen
B
6-bnromo-7-hydroxy-4-(hydroxymethyl)-2H-chromen-2-one
Conditions | Yield |
---|---|
With water In methanol Quantum yield; Photolysis; |
Conditions | Yield |
---|---|
Quantum yield; Claisen Rearrangement; Photolysis; |
Conditions | Yield |
---|---|
With water In methanol for 0.0833333h; Quantum yield; Kinetics; Photolysis; |
Conditions | Yield |
---|---|
Stage #1: 2-methacryloyloxyethyl hydrogen succinate With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 0.5h; Stage #2: 4-hydroxytamoxifen In dichloromethane for 16h; | 96.02% |
Stage #1: 2-methacryloyloxyethyl hydrogen succinate With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0 - 20℃; for 0.5h; Stage #2: 4-hydroxytamoxifen In dichloromethane for 16h; | 96.02% |
trifluoromethylsulfonic anhydride
4-hydroxytamoxifen
(E,Z)-4-(1-{4-[2-(dimethylamino)ethoxy]phenyl}-2-phenylbut-1-en-1-yl)phenyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; for 1h; | 95% |
2-(dimethylamino)ethyl chloride
4-hydroxytamoxifen
Conditions | Yield |
---|---|
With sodium methylate In N,N-dimethyl-formamide; toluene for 5h; Heating; | 83% |
4-Nitrophenyl chloroformate
4-hydroxytamoxifen
Conditions | Yield |
---|---|
Stage #1: 4-Nitrophenyl chloroformate; 4-hydroxytamoxifen With pyridine In dichloromethane at 20℃; for 24h; Cooling with ice; Stage #2: N1-methyl-N1-(2-phenylcyclopropyl)ethane-1,2-diamine With triethylamine In dichloromethane at 20℃; for 22h; Cooling with ice; | 68.4% |
Conditions | Yield |
---|---|
With sodium hydroxide In chloroform for 3h; Ambient temperature; Title compound not separated from byproducts; |
acetyl chloride
4-hydroxytamoxifen
A
(E)-4-{1-[4-(2-dimethylaminoethoxy)phenyl]-2-phenylbut-1-enyl}phenyl acetate
Conditions | Yield |
---|---|
With pyridine for 1h; Friedel Crafts Acylation; Heating / reflux; |
5'-O-(4,4'-dimethoxytrityl)-2'-O-(tert-butyldimethylsilyl)uridine-3'-[(2-cyanoethyl)-(N,N-diisopropyl)]phosphoramidite
4-hydroxytamoxifen
C65H75N4O12PSi
Conditions | Yield |
---|---|
Stage #1: 5'-O-(4,4'-dimethoxytrityl)-2'-O-(tert-butyldimethylsilyl)uridine-3'-[(2-cyanoethyl)-(N,N-diisopropyl)]phosphoramidite; 4-hydroxytamoxifen With N-methylbenzimidazolium triflate In acetonitrile for 2.5h; Molecular sieve; Stage #2: With pyridine; water; iodine In tetrahydrofuran for 1h; |
4-hydroxytamoxifen
N,N-dimethyl-2-(4-(2-phenyl-1-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)but-1-en-1-yl)phenoxy)ethanamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: pyridine / dichloromethane / 1 h / 0 - 20 °C 2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 80 °C / Inert atmosphere View Scheme |
4-hydroxytamoxifen
potassium [4-(1-{4-[2-(dimethylamino)ethoxy]phenyl}-2-phenylbut-1-en-1-yl)phenyl]trifluoroboranuide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: pyridine / dichloromethane / 1 h / 0 - 20 °C 2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 80 °C / Inert atmosphere 3: potassium hydrogen difluoride / methanol; water / 0.25 h / 20 °C View Scheme |
4-hydroxytamoxifen
(4-(1-(4-(2-(dimethylamino)ethoxy)phenyl)-2-phenylbut-1-en-1-yl)phenyl)boronic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: pyridine / dichloromethane / 1 h / 0 - 20 °C 2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / 1,4-dioxane / 80 °C / Inert atmosphere 3: potassium hydrogen difluoride / methanol; water / 0.25 h / 20 °C 4: chloro-trimethyl-silane / water; acetonitrile / 1 h / 20 °C View Scheme |
4-hydroxytamoxifen
(E/Z)-4-hydroxy-N-desmethyltamoxifen hydrochloride
Conditions | Yield |
---|---|
Stage #1: 4-hydroxytamoxifen With carbonochloridic acid 1-chloro-ethyl ester; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene In dichloromethane at 0℃; for 12.5h; Reflux; Stage #2: With hydrogenchloride In methanol; water for 3h; Reflux; |
4-hydroxytamoxifen
C43H44N4O4
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: carbonochloridic acid 1-chloro-ethyl ester; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 12.5 h / 0 °C / Reflux 1.2: 3 h / Reflux 2.1: dichloromethane / 8 h / 20 °C 3.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C 3.2: 20 °C View Scheme |
4-hydroxytamoxifen
C47H52N4O6
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: carbonochloridic acid 1-chloro-ethyl ester; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 12.5 h / 0 °C / Reflux 1.2: 3 h / Reflux 2.1: dichloromethane / 8 h / 20 °C 3.1: trifluoroacetic acid / dichloromethane / 20 °C 3.2: 20 °C View Scheme |
4-hydroxytamoxifen
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: carbonochloridic acid 1-chloro-ethyl ester; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 12.5 h / 0 °C / Reflux 1.2: 3 h / Reflux 2.1: dichloromethane / 8 h / 20 °C 3.1: trifluoroacetic acid / dichloromethane / 3 h / 20 °C 3.2: 20 °C 4.1: silver nitrate / N,N-dimethyl-formamide 4.2: 120 h / -10 - 4 °C 4.3: 0.5 h / 20 °C View Scheme |
4-hydroxytamoxifen
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: carbonochloridic acid 1-chloro-ethyl ester; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 12.5 h / 0 °C / Reflux 1.2: 3 h / Reflux 2.1: dichloromethane / 8 h / 20 °C 3.1: trifluoroacetic acid / dichloromethane / 20 °C 3.2: 20 °C 4.1: silver nitrate / N,N-dimethyl-formamide 4.2: -10 - 4 °C 4.3: 20 °C View Scheme |
4-hydroxytamoxifen
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: carbonochloridic acid 1-chloro-ethyl ester; N,N,N',N'-tetramethyl-1,8-diaminonaphthalene / dichloromethane / 12.5 h / 0 °C / Reflux 1.2: 3 h / Reflux 2.1: dichloromethane / 8 h / 20 °C View Scheme |
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