As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
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inquiryName: methyl 3-(cyanomethyl)benzoate Formula: C10H9NO2 M.W.: 175.184 CAS No.: 68432-92-8 Appearance:Colorless transpare liquid Storage:Preserve in well-closed, light-resistant and airtight containers. Package:25kg/drum Application:intermediate of
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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inquiry3-CYANOMETHYLBENZOIC ACID METHYL ESTER CAS:68432-92-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high q
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inquirySuperiority We can customize and synthesize products that other suppliers may not be able to provide. Advantage cof, mof ligand manufacturer Product Detail bes
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:68432-92-8
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inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:68432-92-8
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inquiryProduct name: Methyl 3-(Cyanomethyl)Benzoate CAS No.: 68432-92-8 Molecule Formula:C10H9NO2 Molecule Weight:175.18 Purity: 95.0% Package: 200kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard
Cas:68432-92-8
Min.Order:1 Kilogram
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inquiryProduct Name: 3-CYANOMETHYLBENZOIC ACID METHYL ESTER Synonyms: 3-CYANOMETHYLBENZOIC ACID METHYL ESTER;METHYL 3-(CYANOMETHYL) BENZOATE;Methyl m-(cyanomethyl)benzoate;Benzoicacid, 3-(cyanomethyl)-, methyl ester CAS: 68432-92-8 MF: C10H9NO2
Cas:68432-92-8
Min.Order:1 Gram
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:68432-92-8
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryR & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
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inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
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inquirybest seller Application:API
Cas:68432-92-8
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inquiryzhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice.pls contact with us freely for getting detailed product spec
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China
Cas:68432-92-8
Min.Order:0
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inquirybest seller Application:API
Cas:68432-92-8
Min.Order:0
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Type:Trading Company
inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white crystalline powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use
Benzoicacid, 3-(cyanomethyl)-, methyl ester cas 68432-92-8Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Cas:68432-92-8
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Cas:68432-92-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquirytrimethylsilyl cyanide
3-methoxycarbonylbenzyl bromide
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile at 60℃; for 15h; | 98% |
With tetrabutyl ammonium fluoride In acetonitrile for 20h; Heating / reflux; | 43% |
potassium cyanide
3-methoxycarbonylbenzyl bromide
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
With 18-crown-6 ether In acetonitrile for 24h; Heating / reflux; | 96% |
With 18-crown-6 ether In acetonitrile for 24h; Ambient temperature; | 92% |
With 18-crown-6 ether In acetonitrile at 20℃; for 40h; | 91% |
In ethanol at 60℃; | 68% |
3-methoxycarbonylbenzyl bromide
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
In acetonitrile | 91% |
In dimethyl sulfoxide | |
In N,N-dimethyl-formamide |
Conditions | Yield |
---|---|
With 18-crown-6 ether In acetonitrile at 20℃; for 72h; | 91% |
With 18-crown-6 ether In acetonitrile at 20℃; for 72h; | 91% |
In methanol; water for 5h; Reflux; Inert atmosphere; | 1 g |
sodium cyanide
3-methoxycarbonylbenzyl bromide
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 20℃; | 89% |
In N,N-dimethyl-formamide at 20℃; | 89% |
In water; N,N-dimethyl-formamide at 75℃; for 5h; Inert atmosphere; | 85% |
sodium cyanide
3-methoxycarbonylbenzyl bromide
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide at 75℃; for 5h; | 70% |
In water; N,N-dimethyl-formamide at 75℃; for 5h; | 70% |
Stage #1: sodium cyanide; 3-methoxycarbonylbenzyl bromide In water; N,N-dimethyl-formamide at 75℃; for 5h; Stage #2: With water In N,N-dimethyl-formamide | 70% |
4-isoxazoleboronic acid pinacol ester
methyl 3-bromobenzoate
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
With potassium fluoride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In dimethyl sulfoxide at 130℃; for 18h; Suzuki Coupling; Inert atmosphere; Sealed tube; | 69% |
3-azido-2-methylbut-3-en-2-ol
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In acetonitrile at 20℃; for 4h; | 65% |
3-bromomethylbenzoyl chloride
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 91 percent / 18-crown-6 / acetonitrile / 40 h / 20 °C View Scheme |
3-Methylbenzoyl chloride
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: Br2 / 0.5 h / 180 °C 2: 91 percent / 18-crown-6 / acetonitrile / 40 h / 20 °C View Scheme |
1-methoxycarbonyl-3-methylbenzene
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NBS / CCl4 2: dimethylsulfoxide View Scheme | |
Multi-step reaction with 2 steps 1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 3 h / Inert atmosphere; Reflux; Irradiation 2: methanol; water / 5 h / Inert atmosphere; Reflux View Scheme | |
Multi-step reaction with 2 steps 1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 4 h / 70 °C 2: dimethyl sulfoxide / 3.25 h / 0 - 10 °C View Scheme | |
Multi-step reaction with 2 steps 1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / Inert atmosphere; Reflux 2: tetra-(n-butyl)ammonium iodide / acetonitrile / Inert atmosphere; Reflux View Scheme |
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
In methanol; dichloromethane; water; acetonitrile |
methyl 3-bromobenzoate
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: magnesium; iodine / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere 1.2: 6 h / 0 - 20 °C / Inert atmosphere 2.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium bromide; sodium hypochlorite; sodium hydrogencarbonate / acetonitrile / 2 h / 0.5 °C / pH 9-10 3.1: ammonia; thionyl chloride / 70 °C 4.1: thionyl chloride / chloroform / 8 h / Reflux View Scheme |
methyl 3-(2-amino-2-oxoethyl)benzoate
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
With thionyl chloride In chloroform for 8h; Reflux; | 32 g |
m-bromobenzoic acid
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1.1: thionyl chloride / 5 h / 70 °C 1.2: 4 h / 20 °C / Cooling with ice 2.1: magnesium; iodine / tetrahydrofuran / 2 h / 70 °C / Inert atmosphere 2.2: 6 h / 0 - 20 °C / Inert atmosphere 3.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium bromide; sodium hypochlorite; sodium hydrogencarbonate / acetonitrile / 2 h / 0.5 °C / pH 9-10 4.1: ammonia; thionyl chloride / 70 °C 5.1: thionyl chloride / chloroform / 8 h / Reflux View Scheme |
methyl 3-(2-hydroxylethyl)benzoate
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium bromide; sodium hypochlorite; sodium hydrogencarbonate / acetonitrile / 2 h / 0.5 °C / pH 9-10 2: ammonia; thionyl chloride / 70 °C 3: thionyl chloride / chloroform / 8 h / Reflux View Scheme |
m-Toluic acid
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: thionyl chloride / 4 h / Reflux 1.2: 100 °C 2.1: 40 °C 3.1: methanol / 2 h / 40 - 80 °C View Scheme |
sodium cyanide
1-methoxycarbonyl-3-methylbenzene
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
In methanol at 40 - 80℃; for 2h; |
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
With sodium hydrogen sulfide; hydrogen sulfide; acetamidine hydrochloride In water at 70℃; under 3750.38 Torr; for 4h; pH=10; Reagent/catalyst; pH-value; Pressure; Temperature; Autoclave; | 98.6% |
With sodium hydrogen sulfide; triethylamine hydrochloride In methanol at 70℃; for 7h; Concentration; Reagent/catalyst; | 95.8% |
methyl 3-cyanomethylbenzoate
2-(3-(hydroxymethyl)phenyl)acetonitrile
Conditions | Yield |
---|---|
With sodium tetrahydroborate In tetrahydrofuran; methanol at 0 - 10℃; for 16.25h; | 95% |
With lithium borohydride In tetrahydrofuran for 4h; Heating / reflux; | 41% |
methyl 3-cyanomethylbenzoate
carbonic acid dimethyl ester
2-<3-(carboxymethyl)phenyl>propionitrile
Conditions | Yield |
---|---|
With potassium carbonate at 180℃; for 8h; Product distribution; Mechanism; the course of reaction according various periods of time; | 91% |
With potassium carbonate at 180℃; for 8h; | 91% |
With potassium carbonate at 180℃; for 8h; | 91% |
methanol
methyl 3-cyanomethylbenzoate
3-methoxycarbonylphenylacetic acid methyl ester
Conditions | Yield |
---|---|
With hydrogenchloride In methanol at 20℃; for 6h; | 87% |
methyl 3-cyanomethylbenzoate
(3-(2-aminoethyl)phenyl)methanol
Conditions | Yield |
---|---|
With aluminum (III) chloride; lithium aluminium tetrahydride In tetrahydrofuran; diethyl ether at 20℃; Inert atmosphere; | 83% |
Stage #1: methyl 3-cyanomethylbenzoate With aluminum (III) chloride; lithium aluminium tetrahydride In tetrahydrofuran; diethyl ether at 20℃; Inert atmosphere; Stage #2: With sulfuric acid; water In tetrahydrofuran; diethyl ether | |
Multi-step reaction with 2 steps 1: sodium tetrahydroborate / tetrahydrofuran; methanol / 16.25 h / 0 - 10 °C 2: hydrogen; ammonia / Raney-Ni / methanol / 3 h / 10 °C View Scheme |
methyl 3-cyanomethylbenzoate
3-(cyanomethyl)benzoic acid
Conditions | Yield |
---|---|
With lithium hydroxide; water In tetrahydrofuran at 20 - 50℃; | 79% |
methyl 3-cyanomethylbenzoate
methyl iodide
methyl 3-(1-cyano-1-methylethyl)benzoate
Conditions | Yield |
---|---|
In dimethyl sulfoxide | 79% |
Stage #1: methyl 3-cyanomethylbenzoate With sodium hydride In dimethyl sulfoxide; mineral oil at 20 - 25℃; Stage #2: methyl iodide In dimethyl sulfoxide; mineral oil at 20℃; for 16h; | 79% |
Stage #1: methyl 3-cyanomethylbenzoate With sodium hydride In dimethyl sulfoxide; mineral oil at 20℃; for 0.333333h; Cooling with ice; Stage #2: methyl iodide In dimethyl sulfoxide; mineral oil at 20℃; for 16h; | 79% |
methyl 3-cyanomethylbenzoate
3-(2-Amino-ethyl)-benzoic acid methyl ester
Conditions | Yield |
---|---|
With hydrogenchloride; palladium 10% on activated carbon In methanol; water at 20℃; for 2h; Inert atmosphere; | 78% |
With sodium tetrahydroborate; trifluoroacetic acid In tetrahydrofuran for 4h; Ambient temperature; | |
With hydrogen; palladium on activated charcoal |
methyl 3-cyanomethylbenzoate
ethylene dibromide
methyl 3-(1-cyanocyclopropyl)benzoate
Conditions | Yield |
---|---|
With dimethyl sulfoxide | 76% |
Stage #1: methyl 3-cyanomethylbenzoate With sodium hydride In dimethyl sulfoxide; mineral oil at 20 - 25℃; Stage #2: ethylene dibromide In dimethyl sulfoxide; mineral oil at 20℃; for 10h; | 76% |
Stage #1: methyl 3-cyanomethylbenzoate With sodium hydride In dimethyl sulfoxide; mineral oil at 20℃; for 0.333333h; Cooling with ice; Stage #2: ethylene dibromide In dimethyl sulfoxide; mineral oil at 20℃; for 16h; | 76% |
Stage #1: methyl 3-cyanomethylbenzoate With sodium hydride In dimethyl sulfoxide; mineral oil at 20 - 25℃; for 0.5h; Stage #2: ethylene dibromide In dimethyl sulfoxide; mineral oil at 20℃; for 16h; |
methyl 3-cyanomethylbenzoate
methyl 3-(2-amino-2-oxoethyl)benzoate
Conditions | Yield |
---|---|
Stage #1: methyl 3-cyanomethylbenzoate With hydrogenchloride In tetrahydrofuran; water Stage #2: With sodium hydroxide In tetrahydrofuran; water | 70% |
1,5-dibromo-pentane
methyl 3-cyanomethylbenzoate
methyl 3-(1-cyanocyclohexyl)benzoate
Conditions | Yield |
---|---|
With dimethyl sulfoxide | 68% |
methyl 3-cyanomethylbenzoate
1-Bromo-2-chloroethane
methyl 3-(1-cyanocyclopropyl)benzoate
Conditions | Yield |
---|---|
Stage #1: methyl 3-cyanomethylbenzoate With sodium hydride In dimethyl sulfoxide; mineral oil Stage #2: 1-Bromo-2-chloroethane In dimethyl sulfoxide; mineral oil at 0 - 25℃; for 18h; | 68% |
With sodium hydride In dimethyl sulfoxide; mineral oil at 0 - 25℃; for 18h; | 68% |
methyl 3-cyanomethylbenzoate
3-carboxymethyl-benzoic acid
Conditions | Yield |
---|---|
With sulfuric acid; water at 160℃; for 3h; | 68% |
methyl 3-cyanomethylbenzoate
methyl 3-(1-cyano-1-methylethyl)benzoate
Conditions | Yield |
---|---|
With sodium hydride In dimethyl sulfoxide at 0 - 25℃; for 12h; | 66% |
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
With hydrogenchloride; palladium 10% on activated carbon; hydrogen In methanol; water | 63% |
With hydrogenchloride; hydrogen; palladium 10% on activated carbon In methanol; dichloromethane; water at 20℃; under 2585.81 Torr; for 10h; | |
With hydrogenchloride; hydrogen; palladium 10% on activated carbon In methanol; dichloromethane; water at 20℃; under 2585.81 Torr; for 10h; |
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
With N-Bromosuccinimide; palladium diacetate; copper(II) bis(trifluoromethanesulfonate) In 1,2-dichloro-ethane Inert atmosphere; Sealed tube; regioselective reaction; | 52% |
1,1'-oxybis(2-bromo-ethane)
methyl 3-cyanomethylbenzoate
methyl 3-(4-cyanotetrahydro-2H-pyran-4-yl)benzoate
Conditions | Yield |
---|---|
With dimethyl sulfoxide | 46% |
methyl 3-cyanomethylbenzoate
1,3-dibromo-propane
methyl 3-(1-cyanocyclobutyl)benzoate
Conditions | Yield |
---|---|
With dimethyl sulfoxide | 42% |
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
Stage #1: methyl 3-cyanomethylbenzoate With sodium tetrahydroborate In tetrahydrofuran at 80℃; Stage #2: With methanol In tetrahydrofuran at 20 - 80℃; for 16.5h; | 40% |
methyl 3-cyanomethylbenzoate
Conditions | Yield |
---|---|
With hydrogenchloride; ethanol; ammonia 1.) CH2Cl2, EtOH, 0 deg C, 6 days, 2.) MeOH, 50 deg C, 18 h; Multistep reaction; | |
With ammonia In methanol; ethanol; dichloromethane |
Conditions | Yield |
---|---|
With N-benzyl-trimethylammonium hydroxide In acetonitrile Michael reaction; Heating; |
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