CAS No.7133-90-6,2-HYDROXY-THIOBENZAMIDE Suppliers

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Shandong Hanjiang Chemical Co., Ltd.

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

7133-90-6 CAS NO.7133-90-6

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Antimex Chemical Limied

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Febuxostat Impurity 40

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2-HYDROXYTHIOBENZAMIDEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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ZHEJIANG JIUZHOU CHEM CO.,LTD

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7133-90-6 C7H7NOS 2-HYDROXY-THIOBENZAMIDE

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Jilin haofei import and export trade Co.,Ltd

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7133-90-6 CAS NO.7133-90-6

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Finetech Industry Limited

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Debye Scientific

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2-Hydroxythiobenzamide

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Shenzhen Sumshine Biotech Co., Ltd.

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Febuxostat Impurity 40

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Ashvarsha finechemicals Private Limited

AFC-318

Benzenecarbothioamide,2-hydroxy-

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Synthetic route

: 611-20-1
salicylonitrile

: 7133-90-6
2-hydroxythiobenzamide

Conditions

Conditions	Yield
With O,S-diethyl-dithiophosphoric acid In water at 80℃; for 6h;	80%
With O,O-Diethyl hydrogen phosphorodithioate In methanol at 80℃; for 12h;	55%
With hydrogen sulfide; triethylamine In pyridine

: 611-20-1
salicylonitrile

: 298-06-6
O,O-Diethyl hydrogen phosphorodithioate

: 7133-90-6
2-hydroxythiobenzamide

Conditions

Conditions	Yield
In water at 80℃; for 6h;	80%

(EtO)2 P(S)SH: (EtO)2 P(S)SH

: 873-62-1
m-cyanophenol

: 7133-90-6
2-hydroxythiobenzamide

Conditions

Conditions	Yield
In water	57%

: 611-20-1
salicylonitrile

aq. NaCl: aq. NaCl

(EtO)2 P(S)SH: (EtO)2 P(S)SH

: 75-09-2
dichloromethane

: 7133-90-6
2-hydroxythiobenzamide

Conditions

Conditions	Yield
With sodium hydrogencarbonate In water	55%

...Expand

: 65-45-2
salicylamide

: 7133-90-6
2-hydroxythiobenzamide

Conditions

Conditions	Yield
With Lawessons reagent In tetrahydrofuran at 55℃; for 4h; Inert atmosphere;	50%
With Lawessons reagent In tetrahydrofuran	29%
With tetraphosphorus decasulfide

: 107-15-3
ethylenediamine

: 63963-47-3
6,6'-(1,2,4-Dithiazolidin-3,5-yliden)-bis-2,4-cyclohexadien-1-on

A: 1565-39-5
2-(2-imidazolinyl)phenol

B: 7133-90-6
2-hydroxythiobenzamide

Conditions

Conditions	Yield
Yields of byproduct given;	A n/a B 15%
Yield given. Yields of byproduct given;
Mechanism;

...Expand

: 79576-70-8
2-(2-Hydroxyphenyl)-1,3-benzoxazin-4-thion

: 107-15-3
ethylenediamine

A: 1565-39-5
2-(2-imidazolinyl)phenol

B: 7133-90-6
2-hydroxythiobenzamide

Conditions

Conditions	Yield
Yield given;

...Expand

: 63963-47-3
6,6'-(1,2,4-Dithiazolidin-3,5-yliden)-bis-2,4-cyclohexadien-1-on

: 7133-90-6
2-hydroxythiobenzamide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: various solvent(s) / 180 °C View Scheme

: 118-61-6
2-hydroxy-benzoic acid ethyl ester

: 7133-90-6
2-hydroxythiobenzamide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: alcohol; ammonia / 100 °C 2: P2S5 View Scheme

: 119-36-8
methyl salicylate

: 7133-90-6
2-hydroxythiobenzamide

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: alcohol; ammonia / 100 °C 2: P2S5 View Scheme

: 638-07-3
ethyl (2-chloroaceto)acetate

: 7133-90-6
2-hydroxythiobenzamide

: 171017-45-1
<2-(2-hydroxyphenyl)-4-thiazolyl>acetic acid ethyl ester

Conditions

Conditions	Yield
In tetrahydrofuran for 60h; Heating;	93%

: 75-09-2
dichloromethane

: 638-07-3
ethyl (2-chloroaceto)acetate

: 7133-90-6
2-hydroxythiobenzamide

: 171017-45-1
<2-(2-hydroxyphenyl)-4-thiazolyl>acetic acid ethyl ester

Conditions

Conditions	Yield
With sodium hydrogencarbonate In tetrahydrofuran	93%

...Expand

: 29310-88-1
3-bromoacetylcoumarin

: 7133-90-6
2-hydroxythiobenzamide

: 175654-92-9
2-(2-hydroxyphenyl)-4-(3-coumarinyl)thiazole

Conditions

Conditions	Yield
In ethanol for 2h; Reflux;	90%

: 7133-90-6
2-hydroxythiobenzamide

: 63963-47-3
6,6'-(1,2,4-Dithiazolidin-3,5-yliden)-bis-2,4-cyclohexadien-1-on

Conditions

Conditions	Yield
With bromine In chloroform	88%

: 31949-21-0
bromomethyl 2-methoxyphenyl ketone

: 7133-90-6
2-hydroxythiobenzamide

: C16H13NO2S

Conditions

Conditions	Yield
In ethanol for 4h; Hantzsch Thiazole Synthesis; Reflux;	88%

: 6065-32-3
4-bromocrotonic ethyl ester

: 7133-90-6
2-hydroxythiobenzamide

: C13H15NO3S

Conditions

Conditions	Yield
With 1,1,1,3',3',3'-hexafluoro-propanol; sodium acetate for 8h; Reflux;	88%

: 15057-21-3
2-bromo-1-(5-nitro-[2]furyl)-ethanone

: 7133-90-6
2-hydroxythiobenzamide

: 2-[4-(5-Nitro-furan-2-yl)-thiazol-2-yl]-phenol

Conditions

Conditions	Yield
In ethanol Heating;	85%

: 7133-90-6
2-hydroxythiobenzamide

: 70-11-1
α-bromoacetophenone

: 2-(2'-hydroxyphenyl)-4-phenylthiazole

Conditions

Conditions	Yield
In ethanol for 2h; Reflux;	84%
In ethanol at 20℃; for 5h;	84%
In ethanol Reflux;

: methanol-dichloromethane

: 7133-90-6
2-hydroxythiobenzamide

: 105-36-2
ethyl bromoacetate

: 2-ethoxycarbonylmethylthiobenzamide

Conditions

Conditions	Yield
With potassium carbonate In N-methyl-acetamide	83.4%

...Expand

: hydrotris(3,5-methylphenylpyrazolyl)boratozinc(II) hydroxide

: 7133-90-6
2-hydroxythiobenzamide

: 71-43-2
benzene

: Zn(hydrotris(3,5-phenylmethylpyrazolyl)borate)(salicylthioamide)*benzene

Conditions

Conditions	Yield
In methanol; dichloromethane Zn-complex was dissolved in CH2Cl2, ligand in MeOH was added, stirred atroom temp. overnight under N2; evapd. to dryness on rotary evaporator, dissolved in benzene, filtered, recrystd. by diffusion with pentane; elem. anal.;	81.2%

...Expand

: 7133-90-6
2-hydroxythiobenzamide

: 6305-43-7
1,4-Dibromo-butane-2,3-dione

: 1242469-32-4
C18H12N2O2S2

Conditions

Conditions	Yield
In ethanol for 12h; Hantzsch condensation; Reflux;	80%

: 638-07-3
ethyl (2-chloroaceto)acetate

: 7133-90-6
2-hydroxythiobenzamide

: 104317-54-6
3-hydroxybenzenecarbothioamide

: 171017-48-4
<2-(3-hydroxyphenyl)-4-thiazolyl>acetic acid ethyl ester

Conditions

Conditions	Yield
In tetrahydrofuran	78%

...Expand

: 70-23-5
ethyl Bromopyruvate

: 7133-90-6
2-hydroxythiobenzamide

: 27383-13-7
ethyl 2-(2-hydroxyphenyl)thiazole-4-carboxylate

Conditions

Conditions	Yield
In ethanol for 2h; Hantzsch Thiazole Synthesis; Reflux;	71%
In ethanol	52%

: 40086-66-6
2-Bromoacetylpyridine

: 7133-90-6
2-hydroxythiobenzamide

: 1191385-37-1
C14H10N2OS

Conditions

Conditions	Yield
In ethanol for 2h; Reflux;	70%

: 7133-90-6
2-hydroxythiobenzamide

: 88735-44-8
3-(2-bromoacetyl)-7-(diethylamino)-2H-chromen-2-one

: 1299474-80-8
2-(2-hydroxyphenyl)-4-[7-(diethylamino)coumarinyl]thiazole

Conditions

Conditions	Yield
In ethanol for 2h; Reflux;	68%

: 17823-58-4
ethyl 2-cyano-3,3-di(methylsulfanyl)acrylate

: 7133-90-6
2-hydroxythiobenzamide

: 5-ethoxycarbonyl-2-(2-hydroxyphenyl)-6-imino-4-methylsulfanyl-6H-1,3-thiazine hydroperchlorate

Conditions

Conditions	Yield
With perchloric acid In acetic acid at 60℃; for 0.5h;	67%

: 7133-90-6
2-hydroxythiobenzamide

: 2632-13-5
2-Bromo-4'-methoxyacetophenone

: 2–(5-(4-methoxyphenyl)thiazol-2-yl)phenol

Conditions

Conditions	Yield
In ethanol for 4h; Inert atmosphere; Reflux;	63%
In ethanol for 4h; Inert atmosphere; Reflux;

: 7133-90-6
2-hydroxythiobenzamide

: 613-54-7
2-Bromo-2'-acetonaphthone

: 2-(2-hydroxyphenyl)-4-(2-naphthyl)thiazole

Conditions

Conditions	Yield
In ethanol for 7h; Reflux;	60%

: 7133-90-6
2-hydroxythiobenzamide

: 80480-15-5
1-(bromoacetyl)pyrene

: 2-(2-hydroxyphenyl)-4-(pyren-1-yl)thiazole

Conditions

Conditions	Yield
In ethanol for 7h; Reflux;	58%

: 7520-95-8
2-bromo-1-(4-methyl-2-phenyl-1,3-thiazol-5-yl)-1-ethanone

: 7133-90-6
2-hydroxythiobenzamide

: 2-(4′-methyl-2′-phenyl-4,5′-bisthiazol-2-yl)phenol

Conditions

Conditions	Yield
In acetone at 20℃; for 24h; Hantzsch Thiazole Synthesis;	16%

: 7133-90-6
2-hydroxythiobenzamide

: 611-20-1
salicylonitrile

Conditions

Conditions	Yield
bei der Destillation unter vermindertem Druck;

: 7133-90-6
2-hydroxythiobenzamide

: 2037-95-8
1,3-benzoxazine-2,4-dione

Conditions

Conditions	Yield
With potassium hydroxide; dihydrogen peroxide

: 7133-90-6
2-hydroxythiobenzamide

: 6005-58-9
N',2-dihydroxybenzimidamide

Conditions

Conditions	Yield
With ethanol; hydroxylamine hydrochloride; sodium carbonate
Multi-step reaction with 2 steps 1: bei der Destillation unter vermindertem Druck 2: alcohol; sodium carbonate; hydroxylamine hydrochloride / 90 °C / unter Druck View Scheme

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KAISA GROUP INC

Antimex Chemical Limied

HANGZHOU TIANYE CHEMICALS CO., LTD.

Changchun Artel lmport and Export trade company

Hangzhou Fandachem Co.,Ltd

ZHEJIANG JIUZHOU CHEM CO.,LTD

HENAN SUNLAKE ENTERPRISE CORPORATION

Jilin haofei import and export trade Co.,Ltd

Finetech Industry Limited

Debye Scientific

Shenzhen Sumshine Biotech Co., Ltd.

Ashvarsha finechemicals Private Limited

Synthetic route

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