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inquiryphosgene
2-methyl-2-propyl-1,3-propanediol
5-Methyl-5-n-propyl-1,3-dioxan-2-one
Conditions | Yield |
---|---|
With antipyrine; chloroform |
2-methyl-2-propyl-1,3-propanediol
Diethyl carbonate
5-Methyl-5-n-propyl-1,3-dioxan-2-one
Conditions | Yield |
---|---|
With sodium methylate Entfernen des entstehenden Aethanols; | |
With sodium 1.) toluene, 90 deg C, 30 min, 2.) toluene, 88-110 deg C; Yield given. Multistep reaction; |
2-methyl-2-propyl-1,3-propanediol
bis(trichloromethyl) carbonate
5-Methyl-5-n-propyl-1,3-dioxan-2-one
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at -78 - 20℃; for 16h; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: p-toluenesulfonyl chloride; n-butyllithium 1.2: 0 - 60 °C 2.1: C49H74AlNO4; bis(triphenylphosphoranylidene)ammonium iodide / butanone / 24 h / 110 °C / 7500.75 Torr / Autoclave; Sealed tube View Scheme |
3-methyl 3-n-propyl oxetane
carbon dioxide
5-Methyl-5-n-propyl-1,3-dioxan-2-one
Conditions | Yield |
---|---|
With C49H74AlNO4; bis(triphenylphosphoranylidene)ammonium iodide In butanone at 110℃; under 7500.75 Torr; for 24h; Autoclave; Sealed tube; |
5-Methyl-5-n-propyl-1,3-dioxan-2-one
A
methanol
B
2-methyl-2-propyl-1,3-propanediol
Conditions | Yield |
---|---|
With [Mn(HN(C2H4PiPr2)2)(CO)2Br]; hydrogen; sodium t-butanolate In tetrahydrofuran at 120℃; under 22502.3 Torr; for 26h; Schlenk technique; Glovebox; Autoclave; | A 94% B 98% |
Conditions | Yield |
---|---|
With ammonia |
morpholine
5-Methyl-5-n-propyl-1,3-dioxan-2-one
morpholine-4-carboxylic acid 2-hydroxymethyl-2-methyl-pentyl ester
methamphetamin
5-Methyl-5-n-propyl-1,3-dioxan-2-one
2-Methyl-2-propyl-3--propanol-(1)
5-Methyl-5-n-propyl-1,3-dioxan-2-one
1-amino-3-methylbutane
2-Methyl-2-propyl-3-<(3-methyl-butyl)-carbamoyl-oxy>-propanol-(1)
5-Methyl-5-n-propyl-1,3-dioxan-2-one
4-amino-benzoic acid
2-Methyl-2-propyl-3-<(p-carboxy-phenyl)-carbamoyloxy>-propanol-(1)
5-Methyl-5-n-propyl-1,3-dioxan-2-one
1-pentanamine
2-Methyl-2-propyl-3-pentyl-carbamoyloxy-propanol-(1)
5-Methyl-5-n-propyl-1,3-dioxan-2-one
dibutylamine
2-Methyl-2-propyl-3-dibutylcarbamoyloxy-propanol-(1)
5-Methyl-5-n-propyl-1,3-dioxan-2-one
isopropylamine
N-Mono-isopropyl-2-methyl-2-n-propylpropane-1,3-diol carbamate
5-Methyl-5-n-propyl-1,3-dioxan-2-one
diethylamine
2-Methyl-2-propyl-3-diethylcarbamoyloxy-propanol-(1)
5-Methyl-5-n-propyl-1,3-dioxan-2-one
N-butylamine
N-Butyl-carbaminsaeure-(3-hydroxy-2-methyl-2-propyl-propylester)
5-Methyl-5-n-propyl-1,3-dioxan-2-one
methylamine
2-Methyl-2-propyl-3-methylcarbamoyloxy-propanol-(1)
5-Methyl-5-n-propyl-1,3-dioxan-2-one
benzylamine
2-Methyl-2-propyl-3-benzylcarbamoyloxy-propanol-(1)
5-Methyl-5-n-propyl-1,3-dioxan-2-one
2-methylallylamin
2-Methyl-2-propyl-3-<(2-methyl-allyl)-carbamoyloxy>-propanol-(1)
5-Methyl-5-n-propyl-1,3-dioxan-2-one
2-Methyl-2-propyl-3-aminocarbamoyl-oxy-propanol-(1)
Conditions | Yield |
---|---|
With hydrazine hydrate |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 5 h / Heating 2: 80 percent / HCl / CH2Cl2 / 10 h / -2 - 2 °C View Scheme | |
Multi-step reaction with 2 steps 2: (i) PhNMe2, (ii) NH3 View Scheme |
5-Methyl-5-n-propyl-1,3-dioxan-2-one
morpholine-4-carboxylic acid 2-carbamoyloxymethyl-2-methyl-pentyl ester
5-Methyl-5-n-propyl-1,3-dioxan-2-one
2-Methyl-2-propyl-3-isopropylaminocarbamoyloxy-propanol-(1)
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. N2H4 2: (i), (ii) (catalytic hydrogenation) View Scheme |
5-Methyl-5-n-propyl-1,3-dioxan-2-one
N.N.-Diethyl-2-methyl-2-propyl-1.3-dicarbamoyloxy-propan
5-Methyl-5-n-propyl-1,3-dioxan-2-one
N-Isopropylamino-2-methyl-2-propyl-1,3-dicarbamoyloxy-propan
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aq. N2H4 2: (i), (ii) (catalytic hydrogenation) 3: HCl / CHCl3 View Scheme |
5-Methyl-5-n-propyl-1,3-dioxan-2-one
N,N-Diaethyl-N',2-dipropyl-2-methyl-1,3-dicarbamoyloxy-propan
5-Methyl-5-n-propyl-1,3-dioxan-2-one
N-Butyl-N'-(3-methyl-butyl)-2-methyl-2-propyl-1,3-dicarbamoyl-propan
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: (i) PhNMe2, (ii) NH3 View Scheme |
5-Methyl-5-n-propyl-1,3-dioxan-2-one
N-Methyl-N'-isopropyl-2-methyl-2-propyl-propandiol-(1.3)-dicarbamat
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: (i) PhNMe2, (ii) /BRN= 741851/ View Scheme |
5-Methyl-5-n-propyl-1,3-dioxan-2-one
N-Methyl-N'-butyl-2-methyl-2-propyl-propandiol-(1,3)-dicarbamat
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: (i) PhNMe2, (ii) /BRN= 741851/ View Scheme |
5-Methyl-5-n-propyl-1,3-dioxan-2-one
N,N-Dimethyl-N'-isopropyl-2-methyl-2-propyl-propandiol-(1.3)-dicarbamat
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: (i) PhNMe2, (ii) /BRN= 605257/ View Scheme |
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